Dectris PILATUS3 R Bedienungsanleitung

DECTRIS Ltd.

5400 Baden

Switzerland

www.dectris.com

User Manual

PILATUS3

This user manual is valid for the following PILATUS detectors:

PILATUS3 6M | PILATUS3 2M | PILATUS3 1M

PILATUS3 300K | PILATUS3 300K-W | PILATUS3 200K

Version:

V2.1

User Manual. PILATUS3. Version: V2.1 2/62

Table of Contents

1. Document History 4

1.1. Current document 4

1.2. Changes 4

2. How to use this Manual 5

2.1. Address and Support 5

2.2. Explanation of Symbols 6

2.3. Convention for Commands 6

2.4. Disclaimer 7

3. Warnings 8

4. System Description 9

4.1. Overview 9

4.2. Hardware 10

4.3. Software 14

4.3.1. Overview of Camserver 14

4.3.2. Description of the File Structure and Configuration Files on the

PILATUS3 Detector Server 14

4.3.3. Overview of TVX 15

4.3.4. Configuration Files for TVX 15

5. Quick Start Guide 16

6. Control the Detector 18

6.1. From the Detector Server 18

6.2. From a Specific Environment 19

6.2.1. Steps to Bring Up a PILATUS3 Detector in a New Environment 19

6.2.2. Testclients 20

7. How to use the PILATUS3 Detector through Camserver 21

7.1. Main Commands 21

7.1.1. Variables 22

7.2. Image formats 23

7.3. External Triggering 25

7.3.1. External Trigger Mode 25

7.3.2. External Multi Trigger Mode 27

7.3.3. External Enable Mode 28

7.3.4. Multiple Exposure Mode 30

8. Trimming the Detector 31

8.1. Principle 31

8.2. Trimming Method 31

8.3. Set the Threshold with more Control 32

9. Bad Pixel Mask and Module Gaps 34

9.1. Using the Bad Pixel Mask 34

9.1.1. Adding new Bad Pixels to the Mask 34

9.1.2. Make a new Bad Pixel Mask from an Uniform Illumination 35

9.2. Flag the Module Gaps 36

10.Adjust Crystallography Parameters 37

11.Flat Field Image 38

11.1.Using the Flat Field Correction Image in Camserver 38

12.How to Use the PILATUS3 Detector through TVX 39

12.1.Description of the Image Display 42

12.2.Analysis commands 46

12.3.Mask files 48

12.4.User defined commands 49

12.5.Glossary files 50

12.6.Example 50

13.Factory Calibration and Correction 51

14.Camserver Commands 52

15.Camserver Test Client 61

User Manual. PILATUS3. Version: V2.1 4/62

1. Document History

1.1. Current document

Version

Date

status

prepared

checked

released

2.1

20.06.2014

released

SB, LK

1.2. Changes

Version

Date

Changes

1.0

01.05.2013

First version

1.1.1

12.06.2013

Adapted CD

2.0

14.02.2014

Complete revision, final CD

2.1

20.06.2014

Moved system specific information to Technical

Specifications. Minor changes.

2. How to use this Manual

Before you start to operate the PILATUS3 detector system please read the User Manual and

the Technical Documentation included in the documentation package carefully.

This document has been designed for the PILATUS3 detector systems.

2.1. Address and Support

DECTRIS Ltd.

Neuenhoferstrasse 107

5400 Baden

Switzerland

Phone: +41 56 500 21 02

Fax: + 41 56 500 21 01

Website:

www.dectris.com →support →Technical Notes →PILATUS

www.dectris.com →support →FAQ

www.dectris.com →support →Problem Report

Email:

[email protected]

Should you have questions concerning the system or its use, please contact us via phone,

mail or fax.

Do not ship the system back before you receive the necessary

transport and shipping information!

User Manual. PILATUS3. Version: V2.1 6/62

2.2. Explanation of Symbols

Symbol

Description

Important or helpful notice

Caution.

Please follow the instructions carefully to prevent

equipment damage or personal injury.

2.3. Convention for Commands

Example

Description

cd ..

Shell commands are written in blue and italic

ExpTime

Camserver commands are in written italic

Disp

TVX commands are written in bold italic

exposem

TVX macros are written in underlined, bold, italic

2.4. Disclaimer

DECTRIS Ltd. has carefully compiled the contents on this manual according to the current

state of knowledge. Damage and warranty claims arising from missing or incorrect data are

excluded.

DECTRIS Ltd. bears no responsibility or liability for damage of any kind, also for indirect or

consequential damage resulting from the use of this system.

DECTRIS Ltd. is the sole owner of all user rights related to the contents of the manual (in

particular information, images or materials), unless otherwise indicated. Without the written

permission of DECTRIS Ltd. it is prohibited to integrate the protected contents published in

these applications into other programs or other Web sites or to use them by any other means.

DECTRIS Ltd. reserves the right, at its own discretion and without liability or prior notice, to

modify and/or discontinue this application in whole or in part at any time, and is not obliged to

update the contents of the manual.

User Manual. PILATUS3. Version: V2.1 8/62

3. Warnings

Please read these warnings before operating the detector system.

Before turning the power supply on, check the supply voltage against the label on the

power supply. Using an improper main voltage will destroy the power supply and

damage the detector.

Power down the detector system before connecting or disconnecting any cable.

Make sure the cables are connected and properly secured.

Avoid pressure or tension on the cables.

The detector system should have enough space for proper ventilation. Operating the

detector outside the specified ambient conditions could damage the system.

The detector is not specified to withstand direct beam at a synchrotron. Such

exposure will damage the exposed pixels.

Place the protective cover on the detector when it is not in use.

Opening the detector or the power supply housing without explicit instructions from

DECTRIS Ltd. will void the warranty.

DO NOT INSTALL ADDITIONAL SOFTWARE OR CHANGE THE OPERATING

SYSTEM on the detector server except for necessary network configurations.

DO NOT TOUCH THE ENTRANCE WINDOW OF THE DETECTOR.

4. System Description

4.1. Overview

A PILATUS3 detector system consists of the following components:

Detector

Detector server

Cooling unit

PILATUS Processing Unit (depending on the system)

High-bandwidth connection

PILATUS

Detector Cooling

Unit

(optional)

Detector

Server

PILATUS

Processing

Unit (PPU)

(optional)

TCP/IP

Client

(local or remote)

TCP/IP

Client

(local or remote)

10 Gbit Ethernet point-to-point connection

Closed circuit

Max. 3 bar, 23°C

User Manual. PILATUS3. Version: V2.1 10/62

4.2. Hardware

DECTRIS X-ray detector systems operate in "single photon counting" mode and are based on

the newly developed CMOS hybrid pixel technology. The main difference with respect to

existing detectors is that the X-rays are directly transformed into electric charge (Figure 1)

and processed in the CMOS readout chips. This new design has no dark current or readout

noise, a high dynamic range of 20 bits (0:1'048'573), a read out time of less than a 1 ms, a

frame rate of up to 500 images/s and an excellent point spread function of 1 pixel. The

quantum efficiency depends on the silicon sensor thickness; however the detectors can be

used for energies of up to 36 keV or more. The count rate is greater than 1x107/s/pixel,

enough to perform many experiments using the high flux of modern synchrotron light sources.

However, the detector cannot withstand a direct synchrotron beam.

Figure 1. Principle of direct detection.

A DECTRIS Ltd. hybrid pixel detector is composed of a silicon sensor, which is a two-

dimensional array of pn-diodes processed in high-resistivity silicon, connected to an array of

readout channels designed with advanced CMOS technology (Figure 2). Each readout

channel is connected to its corresponding detecting element through a microscopic indium

ball, with a typical diameter of 18 m. This connection process is called ‘bump-bonding’.

Figure 2. The detector module, the basic element of all DECTRIS Ltd. area detector systems

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