Gilson 155 Bedienungsanleitung
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Find the Gilson 100326 at our website: Click HERE
Gilson 155/156
UV/VIS Detectors
User’s Guide
LT1034/©2004 Gilson, Inc. All rights reserved March 2004
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Table of Contents
Declaration of Conformity
1 Introduction
Description ............................................................................ 1-1
Optics .............................................................................. 1-2
Display ............................................................................ 1-2
Features ........................................................................... 1-2
Unpacking............................................................................. 1-3
Customer Service ................................................................. 1-4
Technical Specifications ..................................................... 1-5
Modes and Their Parameters ............................................ 1-9
Single Wavelength Mode ............................................. 1-9
Dual Wavelength Mode ...............................................1-9
Scan Wavelength Mode ............................................... 1-9
Status Mode .................................................................... 1-9
Setup Mode .................................................................... 1-9
File Mode ........................................................................ 1-9
2 Installation
Operating Environment ..................................................... 2-1
Temperature ................................................................... 2-1
Contaminants ................................................................ 2-1
Ventilation ...................................................................... 2-1
Condensation ................................................................. 2-1
Electrical Setup..................................................................... 2-2
Rear Panel Diagram ..................................................... 2-3
Essential Setup ............................................................... 2-4
Optional Connections .................................................. 2-6
Unit ID and Baud Rate Selection ............................... 2-10
Unit ID ............................................................................ 2-10
Baud Rate ....................................................................... 2-11
Plumbing Setup .................................................................... 2-12
Inlet Tubing .................................................................... 2-12
Outlet Tubing .................................................................2-13
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3 Operation
Operation Flowchart........................................................... 3-2
Front Panel Diagram ........................................................... 3-4
Software Structure .............................................................. 3-6
Mode Selection ............................................................... 3-6
Parameter List ................................................................ 3-6
Start Up ................................................................................. 3-12
Wake-Up Displays ........................................................ 3-12
Selecting the Mode ........................................................3-14
Error Messages ............................................................... 3-15
Detector Setup Parameters ................................................ 3-16
First Display For Setup Mode ..................................... 3-16
Second Display For Setup Mode ................................ 3-17
Third Display For Setup Mode ................................... 3-18
Fourth Display For Setup Mode .................................3-19
Single Wavelength Mode ................................................... 3-20
Display For Single Wavelength Mode .......................3-20
Output Channels........................................................... 3-22
Example Run .................................................................. 3-23
Dual Wavelength Mode ..................................................... 3-25
First Display for Dual Wavelength Mode................. 3-26
Second Display for Dual Wavelength Mode ...........3-27
Output Channels........................................................... 3-29
Example Run .................................................................. 3-29
Scan Wavelength Mode ...................................................... 3-32
First Display for Scan Wavelength Mode ................. 3-33
Second Display for Scan Wavelength Mode ............ 3-35
Third Display for Scan Wavelength Mode ............... 3-36
Output Channels........................................................... 3-36
Remote Event/Zero ...................................................... 3-37
Scan Mode Event Marker ............................................ 3-37
Zero Scan ........................................................................ 3-37
Discrete Sample Scan ................................................... 3-38
Example Run .................................................................. 3-39
Programming the Detector ................................................ 3-42
Remote Event ................................................................. 3-43
Remote Zero ................................................................... 3-43
Programming Tools ...................................................... 3-44
Example 1: Startup File ................................................3-45
Example 2: Programmed Run .................................... 3-48
Example 3: Linking to Another File ........................... 3-56
Mobile Phase Tips ................................................................ 3-57
Degas Solvents and Buffers ......................................... 3-57
Check UV and Visible Absorbance of Solvents ....... 3-57
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4 Maintenance
Flow Cell Maintenance ....................................................... 4-2
Cleaning the Inside of the Flow Cell (Analytical,
Preparative, Microbore, and SFC only) .................... 4-2
Unclogging the Flow Cell ............................................ 4-5
Replacing Tubing and/or the Flow Cell ................... 4-5
Lamp Maintenance ............................................................. 4-22
UV Lamp Maintenance ............................................... 4-22
Visible Lamp Maintenance .......................................... 4-29
Fuse Replacement ................................................................ 4-35
5 Troubleshooting
Troubleshooting ................................................................... 5-2
Detector Not Functioning ............................................ 5-2
A Lamp Fails to Ignite/A Lamp Fails While On..... 5-2
Status Lights Blinking/Screen Blank or Dark ......... 5-2
Baseline Spikes ............................................................... 5-3
Baseline Noise ................................................................ 5-4
Baseline Drift .................................................................. 5-5
Autozero Out of Range ................................................ 5-6
Out of Range .................................................................. 5-6
Peaks Too Broad ............................................................ 5-7
Decreased Response to Known Sample .................... 5-7
Abnormally High System Pressure ............................ 5-7
Diagnostics ............................................................................ 5-8
Numeric Analyses on the 155 Detector .................... 5-8
Repair and Return Policies ................................................ 5-10
Telephone Numbers ...................................................... 5-10
Before Calling Us ........................................................... 5-10
Warranty Repair ........................................................... 5-10
Non-Warranty Repair .................................................. 5-10
Rebuilt Exchange ........................................................... 5-11
Return Procedure .......................................................... 5-11
AppendixA Defaults and Limits
Setup Mode ........................................................................... A-1
Single Wavelength Mode ................................................... A-1
Dual Wavelength Mode ..................................................... A-2
Scan Mode............................................................................. A-2
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Appendix B Mode-Specific Functions
Mode-Specific Output Channels ...................................... B-1
Mode-Specific Remote Event and
Autozero Functions ............................................................. B-1
Appendix C Sensitivity
Appendix D GSIOC Control
GSIOC Commands .............................................................. D-2
FIFO Commands .................................................................. D-2
GSIOC Command List ........................................................ D-2
FIFO Command List ............................................................ D-11
Appendix E Replacement Parts
Lamp Assemblies ................................................................. E-1
Cell/Accessory Kits ............................................................. E-1
Flow Cell Assemblies ........................................................... E-2
Inlet and Outlet Tubing ...................................................... E-2
Miscellaneous ....................................................................... E-4
Appendix F DisplayAdjustment
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Application of Council Directives:
89/336/EEC, 73/23/EEC
Standards to which Conformity is Declared:
EN61326, EN61000-3-3, EN61000-3-2, EN61010-1:2001
Manufacturer’s Name ........................................... Gilson, Inc.
Manufacturer’s Address ....................................... 3000 W. Beltline Highway
Middleton, WI 53562
EC Office Address .................................................. Gilson S.A.S.
19 Avenue des Entrepreneurs, B.P. 145
F-95400 Villiers-le-Bel, France
Type of Equipment ................................................. Laboratory Equipment
Model. ....................................................................... 155 UV/VIS Detector
Beginning with Serial Number: 109F8G001
Month and Year of Manufacture: June 1998
Place: Middleton, WI (USA) Michael Jacquart
Issue Date: August 1998 Senior Vice President
Corporate Technology Development
I, the undersigned, hereby declare that the equipment
specified above conforms to the above Directives and Standards.
Declaration of Conformity
Artisan Technology Group - Quality Instrumentation ... Guaranteed | (888) 88-SOURCE | www.artisantg.com
Application of Council Directives:
89/336/EEC, 73/23/EEC
Standards to which Conformity is Declared:
EN61326, EN61000-3-3, EN61000-3-2, EN61010-1:2001
Manufacturer’s Name ........................................... Gilson, Inc.
Manufacturer’s Address ....................................... 3000 W. Beltline Highway
Middleton, WI 53562
EC Office Address .................................................. Gilson S.A.S.
19 Avenue des Entrepreneurs, B.P. 145
F-95400 Villiers-le-Bel, France
Type of Equipment ................................................. Laboratory Equipment
Model. ....................................................................... 156 UV/VIS Detector
Beginning with Serial Number: 109C9H001
Month and Year of Manufacture: March 1999
Place: Middleton, WI (USA) Michael Jacquart
Issue Date: April 1999 Senior Vice President
Corporate Technology Development
I, the undersigned, hereby declare that the equipment
specified above conforms to the above Directives and Standards.
Declaration of Conformity
Artisan Technology Group - Quality Instrumentation ... Guaranteed | (888) 88-SOURCE | www.artisantg.com
1-1
1
Introduction
Description
The Gilson 155 and 156 UV/VIS Detectors are microprocessor-controlled absorbance
detectors that provide dual wavelength detection. Both detector models are compatible
components of a Gilson modular HPLC system. And, the 155 Detector with its front panel
control is also compatible with other commercially available HPLC systems.
The 155 Detector can be controlled via its front panel or via external software, such as
Gilson UniPoint™ System Software. The 156 Detector must be controlled via external
software since it does not have an integral front panel display. For information on how to
control the 156 Detector, refer to the user’s guide for the controlling software.
Gilson 155 UV/VIS Detector
Artisan Technology Group - Quality Instrumentation ... Guaranteed | (888) 88-SOURCE | www.artisantg.com
Dieses Handbuch passt für folgende Modelle
1
Inhaltsverzeichnis
Andere Gilson Sicherheitssensor Handbücher
