Koehler K87100 Leitfaden

Koehler Instrument Company, Inc.

1595 Sycamore Avenue • Bohemia, New York 11716-1796 • USA

Toll Free: 1-800-878-9070 (US only) • Tel: +1 631 589 3800 • Fax: +1 631 589 3815

http://www.koehlerinstrument.com • e-mail: [email protected]

Petroleum Testing & Analysis Instrumentation • Custom Design & Manufacturing

MAINTENANCE AND USER’S MANUAL

PENSKY MARTENS

FLASH POINT TESTER

K87100 / K87190

EN 22719 – ISO 2719

ASTM D 93

IP 34

Koehler Instrument Company, Inc.

1595 Sycamore Avenue • Bohemia, New York 11716-1796 • USA

Toll Free: 1-800-878-9070 (US only) • Tel: +1 631 589 3800 • Fax: +1 631 589 3815

http://www.koehlerinstrument.com • e-mail: [email protected]

Petroleum Testing & Analysis Instrumentation • Custom Design & Manufacturing

Table of contents

I – INTRODUCTION Page 5

- 1.1 – Safety instructions Page 5

- 1.2 – Operation instructions Page 5

- 1.3 – Installation instructions Page 6

- 1.4 – Checks out when delivered Page 6

II – TECHNICAL FEATURES Page6–7

III – INSTRUMENT DESCRIPTION Page 8

- 3.1 – Presentation Page 8

- 3.1.1 – Control Panel

Page 8

- 3.1.2 – Front side middle Page 8

- 3.1.3 – Front side low Page 8

- 3.1.4 – Back side Page 8

- 3.1.5 – Working area Page 9

- 3.1.6 – Right side Page 9

- 3.1.7 – Schemas

Page 10-11

IV – SUPPLIED ACCESSORIES Page 13

- 4.1 – Options Page 12

- 4.2 – Accessories Page14-17

V – METHODS AND STARTING-UP Page 18

- 5.1 – Standards Page 18

- 5.2 – Methods Page 19

- 5.3 – Starting-up Page 20

- 5.3.1 – Rear panel connections Page 20

- 5.3.2 – Front panel connections Page 21

- 5.3.3 – Power supply connection Page 21

VI – SOFTWARE DESCIPTION Page 22

- 6.1 – Waiting screen Page 22

- 6.2 – Access to functions Page22-25

VII – RUNNING A TEST Page 25

- 7.1 - Test process (included method for bitumen) Page 25-28

Koehler Instrument Company, Inc.

1595 Sycamore Avenue • Bohemia, New York 11716-1796 • USA

Toll Free: 1-800-878-9070 (US only) • Tel: +1 631 589 3800 • Fax: +1 631 589 3815

http://www.koehlerinstrument.com • e-mail: [email protected]

Petroleum Testing & Analysis Instrumentation • Custom Design & Manufacturing

- 7.2 - Unknown product quick search Page 27

- 7.3 - Quick A Method Page 27

VIII – PRINTING Page 28

- 8.1 – Types of printer Page 28

- 8.2 – Printing current results Page 28

- 8.3 – Printing previous test results Page 28

- 8.4 – Printing temperature slope Page 28

- 8.5 – Print out examples Page 28

- 8.6 – Lock book print out Page 29

IX – SAFETIES Page 29

- 9.1 – Pt 100 probe absence Page 30

- 9.2 – Default in sample temperature increase Page 30

- 9.3 – Electric safety Page 30

- 9.4 – Sample temperature safety Page 30

- 9.5 – Gas safety Page 31

X – INSTALLATION OF SOFTWARE UPDATE Page 32

XI – FEATURES Page 33

- 11.1 – Password (new password) Page 33

- 11.2 – Software options Page 34

- 11.2.1 – Result correction Page 34

- 11.2.2 – Stop of block cooling Page 34

- 11.2.3 – Safety stop Page 34

- 11.2.4 – Introduction of expected temperature Page 34

- 11.2.5 – Barometric pressure Page 34

- 11.2.6 – Buzzer Page 35

- 11.2.7 – New software release Page 35

- 11.2.8 – New password Page 35

- 11.2.9 – Temperature slope print out Page 35

- 11.2.10 – To quit the configuration process Page 35

- 11.3 – Hardware configuration Page 36

- 11.3.1 – Languages Page 36

- 11.3.2 – Units Page 36

- 11.3.3 – Calibration Page 36

Koehler Instrument Company, Inc.

1595 Sycamore Avenue • Bohemia, New York 11716-1796 • USA

Toll Free: 1-800-878-9070 (US only) • Tel: +1 631 589 3800 • Fax: +1 631 589 3815

http://www.koehlerinstrument.com • e-mail: [email protected]

Petroleum Testing & Analysis Instrumentation • Custom Design & Manufacturing

- 11.3.3.A – Sample probe Page 37

- * - Physical calibration Page 38

- * - Display probe calibration values Page 38

- * - Point calibration Page 38

- 11.3.3.B – Barometric pressure Page 38

- * - Physical calibration Page 38

- * - Display calibration value Page 39

- * - Point calibration Page 39

- 11.3.3.C – Pre test steps Page 39

- * - Step calibration Page 39

- * - Step display Page 39

- 11.3.3.D – Electrical supply regulation Page 40

- * - Physical calibration Page 40

- * - Display of calibration point Page 40

- * - Point calibration Page 40

- 11.3.4 – Controls Page 41

- 11.3.4.A – Analogic readings Page 41

- 11.3.4.B – Logic I/O checks Page 41

- 11.3.4.C – Autodiagnostic Page 41

- 11.3.4.D – Lock book print out Page 41

XII – INCIDENTS Page 42

XIII – MAINTENANCE Page 43

- 13.1 – Calibration Page 43

- 13.2 – Controls Page 43

- 13.3 – Cooling system scaling Page 43

XIV – ACCESSORIES AND REFERENCES Page 44

- 14.1 – Accessory parts Page 45

- 14.2 – Optional accessories Page 45

XV – KEY CONTACT Page 45

Koehler Instrument Company, Inc.

1595 Sycamore Avenue • Bohemia, New York 11716-1796 • USA

Toll Free: 1-800-878-9070 (US only) • Tel: +1 631 589 3800 • Fax: +1 631 589 3815

http://www.koehlerinstrument.com • e-mail: [email protected]

Petroleum Testing & Analysis Instrumentation • Custom Design & Manufacturing

I - INTRODUCTION

- 1.1 – SAFETY INSTRUCTIONS

For any use of the instrument, operators must have the following expertise:

A good knowledge of manual petroleum testing methods and the experience of performing flash

point tests,

A good understanding of the risks associated with product and sample manipulation.

Manipulations of hot cup and cover are prohibited. In case of absolute necessity, manipulations

have to be realized with utmost care. In every case, operators have to wear gloves, glasses and

protective safety clothes.

- 1.2 – OPERATION INSTRUCTIONS

Tests have to be exclusively performed:

according to the methods described in the user’s manual,

with the accessories delivered and recommended in the user’s manual,

according the testing process and starting up procedures described in the manual.

Testing processes have to be permanently watched.

The instrument has to be located under a fume hood equipped with a vapor extractor and the

working space has to be sufficiently ventilated.

Water and gas supplies have to be controlled at least once a month in order to verify the good

condition of pipes and fastenings. Gas pipes have to be replaced prior to the expiration date.

If an incident occurs (gas cut off, overheating of the instrument, leakage) which could damage the

instrument or components, an internal and external check up has to be carried out by a person with

the adequate technical level.

Only skilled technicians are allowed to perform maintenance on the instrument which has to be

back at ambient T°, and unplugged from electric supply - excepted for calibration purpose - water

and gas supplies.

Maintenance functions described as in the user’s manual should only be performed by a qualified

technician.

Koehler Instrument Company, Inc.

1595 Sycamore Avenue • Bohemia, New York 11716-1796 • USA

Toll Free: 1-800-878-9070 (US only) • Tel: +1 631 589 3800 • Fax: +1 631 589 3815

http://www.koehlerinstrument.com • e-mail: [email protected]

Petroleum Testing & Analysis Instrumentation • Custom Design & Manufacturing

Prior to using the instrument, operators have to take knowledge of keyboard function keys

described in the user’s manual.

- 1.3 – INSTALLATION INSTRUCTIONS

- The cooling circuit of the instrument must be connected to a max 5 psi pressure water supply.

- The water connections must be done with the delivered tubes and clamp collars.

- The gas circuit of the instrument must be connected to a max 50 mbar pressure gas supply with

the tubes and clamp collars delivered in accessories or to a removable gas cartridge delivered in

option with its connecting accessories.

- The instrument has to be located on a stable and strong table or laboratory bench.

- Electric supply has to be in accordance with the one described on the identification tag and the

instrument has to be connected to the earth.

- The instrument has to be located under a fume hood equipped with a vapor extractor and the

working space has to be sufficiently ventilated.

- 1.4 – CHECK WHEN DELIVERED

Packaging should not be damaged. If so, the necessary claims have to be made to the carrier.

Compare the content of the packing with the provided list of accessories.

Control accessory identification and quality.

II – TECHNICAL FEATURES

Determination of the Closed Cup Flash Point according to the following standards:

EN 22719

ISO 2719

ASTM D93

IP 34

Koehler Instrument Company, Inc.

1595 Sycamore Avenue • Bohemia, New York 11716-1796 • USA

Toll Free: 1-800-878-9070 (US only) • Tel: +1 631 589 3800 • Fax: +1 631 589 3815

http://www.koehlerinstrument.com • e-mail: [email protected]

Petroleum Testing & Analysis Instrumentation • Custom Design & Manufacturing

Ambient working temperature 15°C to 30°C

Working temperature range -20 °C to 400 °C

Detection temperature range -70 °C to 700 °C

Sample temperature measurement 4-wired glass Pt100 probe,

accuracy

0,1°C

Flash point detection Ionization and or thermocouple

Flame dipping Automatic with gas or electrical

Test electric spark Electrical supply potentiometric tune

Stirring 2 speeds : 90 to 120 rpm,

240 to 260 rpm

Cooling of heating block Air ventilation and/or refrigerant

Gas supply Gas network (50 mbar max),

optional gas cartridge (about 8H of

autonomy)

Water supply Water network (5 psi max)

Connection : ext. diameter 12,5 mm

Pilot and test flame Adjustable by valves

Safety of heating Hard heating cut-off at 550°C

Measured in the heating block,

Independently of the

microprocessor,

With sound alarm

Safety on samples Cut-off of on-going test with sound

alarm ; programmable safety from

15°C to 99°C above expected

temperature

Probe safety Faulty probe ; abnormal

temperature

reading

Gas safety Optical detection of flame absence

with sound alarm and automatic

gas

cut-off after 30" and test

termination

Apparatus management Carte 386SX

Programming through tactile keyboard with

membrane Automatic barometric correction :

with manual registration of the

atmospheric pressure or by

pressure transducer

Selection of the units : °C, °F,

mbar, mm Hg

Koehler Instrument Company, Inc.

1595 Sycamore Avenue • Bohemia, New York 11716-1796 • USA

Toll Free: 1-800-878-9070 (US only) • Tel: +1 631 589 3800 • Fax: +1 631 589 3815

http://www.koehlerinstrument.com • e-mail: [email protected]

Petroleum Testing & Analysis Instrumentation • Custom Design & Manufacturing

Calibration of the temperature

measurement (regulated bath or

resistance box)

Obliteration or preservation of the

presumed temperature after each

test

Buzzer (continuous or 3 minutes)

Stop temperature of the cooling

heating block

Correction of temperature deviation

on result : +/- 9,9°C

Safety on sample from 15°C to

99°C above ambient temperature

Alarm sounds at safety

temperature

-15°C

Instrument piloting Waterproof tactile screen, liquid

Crystal backlit graphic display,

256x128 pixels

Printing of configuration report

Printing of results 80 column printer or ticket printer

(supplied)

Maintenance function For logic I/O

Back up of programmed parameters Flash Eprom

Software up dating Through teleloading

Recording of previous 100 results

Size LxHxW (mm) 270 x 550 x 550

Weight 20 kgs

Power supply 115 or 230 V 10 % - 50/60 HZ

Koehler Instrument Company, Inc.

1595 Sycamore Avenue • Bohemia, New York 11716-1796 • USA

Toll Free: 1-800-878-9070 (US only) • Tel: +1 631 589 3800 • Fax: +1 631 589 3815

http://www.koehlerinstrument.com • e-mail: [email protected]

Petroleum Testing & Analysis Instrumentation • Custom Design & Manufacturing

III – INSTRUMENT DESCRIPTION

- 3.1 - PRESENTATION

3.1.1 – Control panel

1 waterproof tactile keyboard (1)

1 backlit liquid crystal graphic display 256x128 pixels (2)

3.1.2. Front panel (middle)

thermocouple connector for the flash point detector (3)

cable connector for ionization detection (4)

sample Pt100 probe connector (5)

gas connections for the pilot (6) and the test flame (7)

3.1.3 – Front panel (bottom)

pilot flame needle valve (8), test flame needle valve (9)

light indicators for heating (10) and cooling (11) of the heating block

electrical supply potentiometer of the lighting spark (28)

3.1.4 – Rear panel

general power supply switch with fuses (12)

RS232 port for PC connection (13)

printer connector (14)

gas inlet (15)

inlet (16) and outlet (17) connections of the cooling circuit

gas cartridge fastenings (18)

pressure generator connection for pressure sensor calibration (19)

electrical regulator connection for pressure sensor calibration (30)

Koehler Instrument Company, Inc.

1595 Sycamore Avenue • Bohemia, New York 11716-1796 • USA

Toll Free: 1-800-878-9070 (US only) • Tel: +1 631 589 3800 • Fax: +1 631 589 3815

http://www.koehlerinstrument.com • e-mail: [email protected]

Petroleum Testing & Analysis Instrumentation • Custom Design & Manufacturing

3.1.5 – Working space

electrical spark connections (20)

cup container when no test is under way (21)

heating block (22)

flame dipper (23) or electrical spark

pilot flame (24)

arm for controlling the flame presentation traps (25)

connection axis of the stirring (26)

flexible stirrer (27)

3.1.6 – Right side

Identification tag (29)

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