Sabio 2010D Bedienungsanleitung

MODEL 2010D

GAS DILUTION CALIBRATOR

OPERATIONS MANUAL

I N S T R U M E N T S

MODEL 2010D OPERATIONS MANUAL

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reserved. However, any part of this document may be reproduced

for Sabio Instruments, Inc. customer usage with Sabio

Instruments, Inc. cited as the source.

NOTICE TO USER

The information in this manual has been carefully checked and is

believed to be accurate. However, Sabio Instruments, Inc.

assumes no responsibility for any inaccuracies that may be

contained in this manual. In no event will Sabio Engineering,

Inc. be liable for direct, indirect, special, incidental or

consequential damages resulting from any defect or omission in

this manual, even if advised of the possibility of such damages.

The contents of this manual and the specifications herein may

change without notice or obligation.

GOVERNING LAW

Laws of the state of Texas, USA govern this agreement.

The information presented in this manual is for reference only.

This manual may contain or reference information and products

that may be protected by copyrights and/or patents. No license

is conveyed under the rights of Sabio Instruments, Inc. or

others.

Table of Contents

Section 1 Introduction.................................... 1-1

User Benefits .......................................... 1-1

Standard Features ....................................... 1-3

Optional Features ....................................... 1-3

Model 2010D Gas Dilution Calibrator Specifications ....... 1-4

Section 2 Getting Started ................................ 2-1

Unpacking and Power Application ......................... 2-1

Start-Up ................................................ 2-1

Standby Operation Upon Power Up ......................... 2-1

User Interface .......................................... 2-1

Initial Configuration of the Model 2010D ................. 2-3

System Operation and Maintenance Precautions ............ 2-3

Section 3 System Operations .............................. 3-1

Front Panel Guide ....................................... 3-1

Main Screen Layout ...................................... 3-8

Main Menu Topics ........................................ 3-11

Using the 2010D Screens .................................. 3-12

Edit Screens ............................................ 3-13

Section 4 Installation.................................... 4-1

Placement ............................................... 4-1

Environment ............................................. 4-1

Source Gas Cylinder Selection ........................... 4-2

Diluent Selection ....................................... 4-4

Source and Diluent Port Usage ........................... 4-4

Dilution Calibrator Pneumatic Connections ............... 4-5

Power ................................................... 4-7

Parallel Printer Data Port .............................. 4-7

Keyboard Port ........................................... 4-9

RS-232 Serial Communications Port 1 ..................... 4-9

RS-232 Serial Communications Port 2 ..................... 4-10

RS-232 Serial Communications Cable, Model 2010D to PC..... 4-10

RS-232 Serial Communications Cable, Model 2010D to Modem . 4-11

Status Input/Output Port ................................ 4-12

Instrument Audit Analog Input/Output Port ............... 4-13

Air Source Activation Port .............................. 4-14

Ethernet Port ........................................... 4-15

USB Host Port ........................................... 4-15

Section 5 Operation ...................................... 5-1

Performing Automatic Calibrations ....................... 5-1

Calibrating Multiple Analyzers in One Calibration ....... 5-1

Performing Manual Calibrations .......................... 5-2

Predefined Operator Stepped Manual Calibration .......... 5-2

Timer Stepped Manual Calibration ........................ 5-4

Viewing Calibration Status .............................. 5-5

Performing Manual Calibrations using the Status Screen 5-7

Viewing Diagnostic Information ........................ 5-10

The Analog Input Screen ................................. 5-10

The Analog Output Screen ............................... 5-11

The Internal Control Outputs and User Digital I/O Bits .. 5-11

Section 6 Model 2010D Calibration Set-Up .................. 6-1

Set Up Gases ............................................ 6-2

Set Up Gas Standards ................................... 6-3

Diluent and Source Port Assignments .................... 6-4

Introduction to Initializing Calibration Sequences ...... 6-6

Defining Calibration Sequences .......................... 6-8

Setting up Sequence Points for Single-Gas Sequences

(Page 2 and 3) .......................................... 6-11

Setting up Sequence Points for Multi-Gas Sequences

(Page 2 and 5) .......................................... 6-14

Auto Calibration Set-up ................................. 6-19

Scheduling Automatic Calibrations ....................... 6-20

Digital I/O Group Set-up ................................ 6-21

Assigning Sequence Start Patterns ....................... 6-24

Assigning Point Start Patterns .......................... 6-25

Setting the Time and Date ............................... 6-27

Section 7 Serial Communications........................... 7-1

Operating Modes ........................................ 7-1

Prerequisites ........................................... 7-2

Configuring the Modem ................................... 7-3

Setting Up the Com Ports ................................ 7-4

Setting Up the Remote Terminal .......................... 7-6

Setting Up the Command Protocol ......................... 7-7

Configuring the Computer for Terminal Mode............... 7-9

Operating the Model 2010D Remotely using Terminal Mode.... 7-11

Disconnecting ........................................... 7-12

Operating the Model 2010D Remotely using Command Mode..... 7-13

The Monitor Labs Protocol ............................... 7-13

Number Representation (Floating Point) .................. 7-14

Digital Word Representation ............................. 7-14

Command Structure ....................................... 7-15

Starting and Ending Commands ............................ 7-15

Command Words ........................................... 7-15

Calibrator Address ...................................... 7-16

Data Fields ............................................. 7-16

Data Verification Fields ................................ 7-16

Response Structure ...................................... 7-18

Commands ................................................ 7-19

Monitor Labs Commands ................................... 7-19

Common Data and Parameter Fields for Commands ........... 7-19

Command Summary.......................................... 7-20

Error Codes ............................................. 7-20

Stop (S) ................................................ 7-21

Purge (P) ............................................... 7-21

Timed Sequence (TS) ..................................... 7-23

Manual Sequence (MS)..................................... 7-23

Get Status (GS) ......................................... 7-24

Section 8 Internal Calibrations............................ 8-1

Viewing Calibration Data ................................ 8-5

Manually Entering Polynomial Coefficients ............... 8-5

Manually Entering a Calibration Table ................... 8-6

Performing an Interactive Calibration ................. 8-7

Editing Calibration Data ................................ 8-8

Selecting Device Parameters ............................ 8-9

Interactively Calibrating Mass Flow Controllers ......... 8-9

Interactively Calibrating the Ozone Generator ........... 8-11

Section 9 Internal UV Ozone Photometer..................... 9-1

Description ............................................. 9-1

Theory of Operation ..................................... 9-1

Installation ............................................ 9-3

Operation ............................................... 9-3

Setup Options ........................................... 9-9

Photometer Calibration .................................. 9-17

Ozone Servo Control Adjustments ........................ 9-19

Routine Maintenance ..................................... 9-21

Leak Check .............................................. 9-22

Photometer Flow Check / Adjustment ...................... 9-23

Schematics

Flow Diagram ............................................ S-1

Warranty

List of Figures

2-1 Main Menu .......................................... 2-2

3-1 The Model 2010DFront Panel ......................... 3-2

3-2 The Main Screen .................................... 3-8

3-3 External Keyboard Shortcuts in Terminal Mode ....... 3-9

3-4 Examples of Data Entry Fields ...................... 3-13

4-1 Rear Panel ......................................... 4-6

5-1 Manual Sequence Selection Menu ..................... 5-3

5-2 The "Select a Point to Run" Screen ................. 5-3

5-3 The Sequence Status Screen ......................... 5-4

5-4 The Idle Status Screen ............................. 5-6

5-5 The Dilution Status Screen ......................... 5-6

5-6 The Ozone Status Screen ............................ 5-7

5-7 The GPT Status Screen .............................. 5-7

5-8 The Analog Input Diagnostic Screen ................. 5-10

5-9 The Analog Output Diagnostic Screen ................ 5-11

5-10 The Internal Control Outputs Diagnostic Screen ..... 5-12

5-11 The User Digital I/O Bits Diagnostic Screen ........ 5-12

6-1 New Gas Screen ..................................... 6-2

6-2 New Gas Standard Screen ............................ 6-3

6-3 Edit Port Assignments Screen ....................... 6-5

6-4 New Sequence Screen, Page 1 ....................... 6-8

6-5 New Sequence Screen (Single Gas, Page 2 of 3) ...... 6-11

6-6 New Sequence Screen (Multi-gas, Page 2 of 5) ....... 6-14

6-7 New Sequence Screen (Multi-gas, Page 3 of 5) ....... 6-17

6-8 The Edit Sequence Schedules Screen ................. 6-20

6-9 The Edit Digital I/O Group Assignments Screen ...... 6-23

6-10 Sequence Start Remote Activation Patterns Screen ... 6-24

6-11 Point Start Remote Activation Patterns Screen ...... 6-26

6-12 Set System Clock Screen ............................ 6-27

7-1 Port Set-up Screen ................................. 7-5

7-2 Remote Terminal Setup Screen ....................... 7-7

7-3 Command Model Setup Screen ......................... 7-7

7-4 File Transfer Status Screen ........................ 7-12

8-1 Comparison of Linearization Methods ................ 8-4

8-2 Calibration Menu ................................... 8-5

8-3 New Calibration Coefficients ....................... 8-6

8-4 New Calibration Table .............................. 8-6

8-5 Interactive Calibration ............................ 8-8

8-6 Device Parameters .................................. 8-9

8-7 Interactive Ozone Calibration ...................... 8-13

9-1 The Ozone Status Screen ............................ 9-4

9-2 The Photometer Diagnostic Screen, General .......... 9-6

9-3 The Photometer Diagnostic Screen, Detailed ......... 9-8

9-1 Ozone Status Screen ............................... 9-4

9-2 Photometer Diagnostics Screen, General ............ 9-6

9-3 Photometer Diagnostics Screen, Detailed ........... 9-8

9-4 Photometer Parameters, Page 1 of 3 ................ 9-10

9-5 Photometer Parameters, Page 2 of 3 ................. 9-13

9-6 Photometer Parameters, Page 3 of 3 ............... 9-15

9-7 Photometer, Edit Calibration Table ................. 9-17

9-8 Photometer, Interactive Calibration ................ 9-17

9-9 Photometer, Leak Check Setup ....................... 9-23

9-10 Photometer, Flow Check / Adjustment ................ 9-24

List of Tables

4-2 Parallel Printer Port Connections .................. 4-8

4-3 External Keyboard Port Connections ............. ... 4-9

4-4 Communications Port 1 Connections .................. 4-9

4-5 Communications Port 2 Connections .................. 4-10

4-6 Model 2010D to PC Connections ....................... 4-11

4-7 Model 2010D to Modem Connections .................... 4-11

4-8 Status Input/Output Port Connections ............... 4-12

4-9 Audit Port Connections ............................. 4-13

4-10 Air Source Activation Port Connections ............. 4-14

7-1 PC Keyboard Model 2010D Key Mapping ............... 7-11

Introduction Page 1-

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Section 1 Introduction

Users can easily perform gas dilution, ozone, and GPT

calibrations with Sabio Instruments Inc.'s intelligent Model

2010D gas dilution calibrator. The Model 2010D was designed to

set a new government and industry standard of quality and

performance for gas calibrations. Enhanced with the latest

technology, Sabio's Model 2010D Gas Dilution Calibrator is an

uncomplicated and effective way to precisely control the

dilution of gas standards for calibration of ambient air and

source monitoring analyzers.

An easy-to-read display, with touch panel operation, user-

friendly menu software and sturdy hardware amenities make the

Model 2010D both highly practical and easy to operate. Each

Model 2010D component was selected or designed with great care to

meet Sabio's quality performance standards and government

environmental agency goals and requirements.

User Benefits

Quality Construction. Sabio selected very high quality, inert valves

for the source, permeation and dilution streams. The source and

permeation oven valves wetted surfaces are manufactured with inert

materials. To ensure the manifolds do not react with the gases, the

manifolds are made of inert materials. Sabio minimized dead space

in the valves and manifolds to assure fast rise times. A source

purge-valve is standard for sweeping trapped gas out of the source

manifold. Static mixers enhance homogeneous blending of diluent and

source gases and the reaction chamber meets EPA requirements.

Mass-flow controllers precisely meter all gas streams.

Modern technology means precision calibration. In combining superior

software, components and materials, Sabio's Model 2010D is

setting a new benchmark for precisely diluting gas standards.

Elemental design means no lengthy training period required. The design of

the Model calibrator makes it easy for non-technical personnel with

little or no specialized training to perform precise calibrations

of gas analyzers.

Introduction Page 1-

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A complete calibration system. The Model 2010D Calibration System

makes use of embedded microprocessor technology to enhance the

accuracy and control features of the calibration system. The

Model 2010D is designed to be used manually, automatically or

semi-automatically by remote control to conduct calibrations.

The unit features an optional internal ozone generator. An

optional permeation oven and UV absorption photometer are also

available.

Versatile programming options. The calibrator has the capability to

produce and store in memory 20 calibration sequences, with up to 20

levels of source/dilution in each sequence. Users employ the front

panel membrane keypad or serial port to input calibration parameters.

A bright, easy-to-read, 25-line x 80-character display shows

calibration and system configuration information.

Additional features include continually updated display of dilution

and source information, local and remote calibration control,

eight-port output manifold with port connections for up to seven gas

analyzers, and portable and 19-inch rack mounting options.

The Model 2010D's precision ozone generator is suitable for use

as a transfer standard for ozone calibrations or can be used for

performing nitrogen dioxide calibrations by means of gas phase

titration (GPT). The ozone generator eliminates the need for an

additional ozone transfer standard to conduct audits or perform

calibrations.

The Model 2010D's ozone generator's advanced electronic

circuitry and propriety photo detector enable the ozone

generator output to be so stable and accurate that the need for

a photometer is eliminated.

The internal UV absorption photometer option is a complete UV ozone

analyzer that can be used independently for monitoring ozone

production.

The Model 2010D external permeation oven option is an effective

tool for generating precise gas concentrations for calibrating a

wide range of gas analyzers. The large oven capacity

accommodates many types and sizes of permeation devices. An

internal clean air supply, precise mass flow controller and

temperature controller ensures a highly accurate gas

concentration process.

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