Barnstead|Thermolyne D11911 Bedienungsanleitung
BARNSTEAD|THERMOLYNE
NANOpure®DIamond™
UV
ultrapure water system
Operation Manual
Series 1191
Model No. Voltage
D11911 100V - 240V
LT1191X1 • 6/22/00
Safety Information ..........................................................................................................................................................................................3
Alert Signals............................................................................................................................................................................................3
Warnings ................................................................................................................................................................................................3
Introduction ....................................................................................................................................................................................................5
General Usage........................................................................................................................................................................................5
General Specifications....................................................................................................................................................................................6
Environmental Conditions ......................................................................................................................................................................7
Declaration of Conformity ......................................................................................................................................................................7
Unpacking ......................................................................................................................................................................................................8
Installation ......................................................................................................................................................................................................9
Choosing a Site ......................................................................................................................................................................................9
Other Accessories ........................................................................................................................................................................................10
UV Lamp Installation ............................................................................................................................................................................11
Bench Mounting....................................................................................................................................................................................12
Wall Mounting ......................................................................................................................................................................................12
Installing the Control Panel in a Remote Location ..............................................................................................................................13
Water Connections ..............................................................................................................................................................................14
Controls ........................................................................................................................................................................................................15
Main Power Switch ..............................................................................................................................................................................15
Control Panel........................................................................................................................................................................................15
Switches................................................................................................................................................................................................16
Initial Operation ............................................................................................................................................................................................17
Cartridge Pack Installation....................................................................................................................................................................17
Initial Rinse ..........................................................................................................................................................................................18
System Sanitization Procedure ............................................................................................................................................................19
Normal Operation..........................................................................................................................................................................................21
Dispensing Water..........................................................................................................................................................................................21
Automatic Dispensing ..................................................................................................................................................................................21
User Settings ................................................................................................................................................................................................22
Adjusting Display Brightness................................................................................................................................................................22
Setting the Displayed Language ..........................................................................................................................................................22
Setting the Date and Time....................................................................................................................................................................22
Setting the Cell Constant......................................................................................................................................................................23
Use of Standby Mode ..........................................................................................................................................................................25
Selecting the Set Point ........................................................................................................................................................................25
Resetting the Sanitization Timer ..........................................................................................................................................................26
Resetting the UV Timer ........................................................................................................................................................................26
Setting Volumetric Dispensing..............................................................................................................................................................27
Setting Timed Dispensing ....................................................................................................................................................................28
Performing a System Flush ..................................................................................................................................................................28
Changing Purity Units ..........................................................................................................................................................................28
Temperature Compensation..................................................................................................................................................................29
Installing Float or Pressure Switch ..............................................................................................................................................................30
N.I.S.T. Calibration Module ..........................................................................................................................................................................31
Performing an Electronic Calibration Using the Optional N.I.S.T. Calibration Module ........................................................................31
Remote Dispenser................................................................................................................................................................................32
Computer/Printer Setup................................................................................................................................................................................33
Connecting NANOpure DIamond to Computer and Communicating Through the RS-232 Port Using Hyperterminal or Procomm ..33
Connecting and Starting the Printer ....................................................................................................................................................35
Printer Setup ........................................................................................................................................................................................36
Maintenance and Servicing ..........................................................................................................................................................................38
General Cleaning Instructions ..............................................................................................................................................................38
Cell Cleaning ........................................................................................................................................................................................38
System Sanitization ..............................................................................................................................................................................38
System Depressurization......................................................................................................................................................................40
Cartridge Pack Replacement................................................................................................................................................................41
0.2 Micron Filter Replacement..............................................................................................................................................................42
UV Lamp Replacement ........................................................................................................................................................................43
Fuse Replacement................................................................................................................................................................................44
Shutdown..............................................................................................................................................................................................44
Troubleshooting ............................................................................................................................................................................................45
Replacement Parts ......................................................................................................................................................................................48
Flow Chart Operational Overview)................................................................................................................................................................50
Wiring Diagram ............................................................................................................................................................................................51
Ordering Procedures ....................................................................................................................................................................................52
One Year Limited Warranty ..........................................................................................................................................................................53
2
Table of Contents
Your Barnstead|Thermolyne NANOpure DIamond UV
ultrapure water system has been designed with function,
reliability, and safety in mind. It is your responsibility to
install it in conformance with local electrical codes. This
manual contains important safety information. You must
carefully read and understand the contents of this manual
prior to the use of this equipment. For safe operation,
please pay attention to the alert signals throughout the
manual.
Water purification technology employs one or more of the
following: chemicals, electrical devices, mercury vapor
lamps, steam and heated vessels. Care should be taken
when installing, operating or servicing Barnstead
products. The specific safety notes pertinent to this
Barnstead product are listed below.
Warnings
To avoid electrical shock, always:
1. Use a properly grounded electrical outlet of
correct voltage and current handling capacity.
2. Do not locate the NANOpure DIamond UV di-
rectly over equipment that requires electrical
service. Routine maintenance of this unit may
involve water spillage and subsequent electrical
shock hazard if improperly located.
3. Replace fuses with those of the same type and
rating.
4. Disconnect from the power supply prior to main-
tenance and servicing.
To avoid personal injury:
1. Do not use in the presence of flammable or
combustible materials; fire or explosion may
result. This device contains components which
may ignite such materials.
2. This device is to be used with water feeds only.
Sanitizing/cleaning agents must be used in com-
pliance with instructions in this manual. Failure
to comply with the above could result in
explosion and personal injury.
3
Safety Information
Caution
Cautions alert you to a possibility of
damage to the equipment.
Warning
Warnings alert you to a possibility of
personal injury.
Note
Notes alert you to pertinent facts and
conditions.
Alert Signals
Note
The UV lamp contains mercury. If bro-
ken or no longer needed, do not dis-
pose of the UV lamp in the trash.
Recycle or dispose of the UV lamp as
hazardous waste.
3. Avoid splashing disinfecting solutions on
clothing or skin.
4. Ensure all piping connections are tight to avoid
chemical leakage.
5. Ensure adequate ventilation.
6. Carefully follow manufacturer’s safety
instructions on labels of chemical containers and
material safety data sheets.
7. Depressurize system prior to removing the
cartridge pack.
8. This unit is equipped with an ultraviolet lamp.
Ultraviolet radiation is harmful to the eyes and
skin. Do not attempt to observe the lamp
directly.
9. Refer servicing to qualified personnel.
10. A full cartridge pack may weigh about 20 lbs.
4
SAFETY INFORMATION
Congratulations on your purchase of a Barnstead|
Thermolyne NANOpure DIamond UV ultrapure water sys-
tem. This water purification system is designed to provide
low TOC, high resistivity, reagent grade water that
exceeds ASTM Type I, CAP and NCCLS Type I stan-
dards. It uses a four-stage deionization process combined
with a UV lamp, and a 0.2 micron filter to polish suitable
feed water (distilled, deionized, or reverse osmosis) to
produce low TOC (<3.0 ppb) water with a resistivity of up
to 18.2 megohm-cm. Water resistivity is continuously
monitored by a resistivity cell and displayed on a digital
display.
The electronics can be verified and calibrated utilizing a
N.I.S.T. Traceable Calibration module. See accessory
ordering information.
Please read the instructions carefully to ensure that you
receive maximum benefit from the NANOpure DIamond
UV. Also, please fill out and return the enclosed warranty
registration card as it will help us assure you of proper
warranty coverage.
General Usage
Do not use this product for anything other than its intend-
ed usage.
5
Introduction
Dimensions and Clearance Requirements
Dimensions
13.4” W x 19.5” H x 16.9” D (34.0 x 49.5 x 42.8 cm)
Clearances
Sides - 9” (22.9 cm) minimum for servicing.
Above - 3” (7.6 cm) minimum for removal of the top cover.
Front - 4.75” (12.1 cm) minimum for opening the front door.
Feed Water Requirements
Types RO, DI, distilled.
TOC Less than 1.0 ppm.
Turbidity 1.0 N.T.U. maximum.
Pressure Range Gravity feed to 100 psig (7kg/cm2) maximum.
Temperature Range 4°C - 40°C (40-104°F)
TDS (CaCO3) < 70 ppm
Silica < 1 ppm
Silt < 5% SDI
Product Water
Water Quality
Resistivity > 18.0 mΩ-cm
TOC Less than 3.0 ppb
Flow Rate
1.5 lpm maximum at minimum inlet feed water pressure 10 PSIG with a new final filter.
Volumetric Dispense
Accuracy: ± 5%
Repeatability: ± 3%
Electrical Requirements
The NANOpure DIamond UV is equipped with 2 power cords to be plugged into an electrical outlet of the
appropriate voltage.
Voltage and Frequency (Nominal)
Model D11911 100-240 VAC, 47-63 Hz, 1 phase
6
General Specifications
Environmental Conditions
Operating: 4°C - 49°C; 20% to 80% relative humidity, non-condensing. Installation
Category II (over-voltage) in accordance with IEC 664. Pollution Degree 2 in
accordance with IEC 664.
Altitude limit: 3,500 meters.
Storage: -25°C to 65°C; 10% to 85% relative humidity.
Declaration of Conformity
Barnstead|Thermolyne hereby declares under its sole responsibility that this product conforms with the
technical requirements of the following standards:
EMC: EN 61000-3-2 Limits for Harmonic Current Emissions
EN 61000-3-3 Limits for Voltage Fluctuations and Flicker
EN 61326-1 Electrical Equipment for Measurement, Control, and Laboratory Use; Part I:
General Requirements
Safety: EN 61010-1 Safety Requirements for Electrical Equipment for Measurement, Control and
Laboratory Use; Part I: General Requirements
per the provisions of the Low Voltage Directive 73/23/EEC, as amended by 93/68/EEC.
The authorized representative located within the European Community is:
Electrothermal Engineering, Ltd.
419 Sutton Road
Southend On Sea
Essex SS2 5PH
United Kingdom
Copies of the Declaration of Conformity are available upon request.
7
GENERAL SPECIFICATIONS
1. Remove the unit from its shipping container.
Remove all contents carefully. Ensure that the
UV lamp, feed and drain tubing, sanitization
cartridge, wall bracket, accessory parts bag
and power cords (see list below) are re-
moved from the packaging materials before
discarding. Put the NANOpure DIamond UV on
a bench.
UV Lamp LMX13
Sanitization Cartridge CMX25
Wall Bracket (Unit)
Wall Bracket (Remote Display) BC1190X10
Accessory Parts Bag Includes:
Feed Water Tube, 3/8” O.D.
Drain Tube, 1/4” O.D.
240 V Power Cord w/Fuses CRX70 (2, FZX54)
120 V Power Cord w/Fuses CRX72 (2, FZX47)
Display Cable WHX20
Blank Display
Plug Adapter CEX42
Also required for installation:
* Customer Supplied Fasteners to mount unit and remote
display.
8
Unpacking
9
Choosing a Site
The NANOpure DIamond UV features a removable con-
trol panel display which allows the system to be mounted
almost anywhere within the laboratory. Use the wall
bracket for wall mounted systems as a template to drill
mounting holes. (The NANOpure DIamond UV does not
include screws and fasteners for mounting.) Please refer
to the “General Specifications” section for clearance
requirements.
Installation
NOTE
The outlet of a gravity feed storage
reservoir must be above or at the
same level as the inlet of the
NANOpure DIamond UV.
********************
************************
Caution
Wall composition, condition and
construction as well as fastener type
must be considered when mounting
this unit. The mounting surface and
fasteners selected must be capable of
supporting a minimum of 150 lbs. (68
kg). Inadequate support and/or fasten-
ers may result in damage to mounting
surface and/or equipment. If you are
unsure of mounting surface
composition, condition and construc-
tion or correct fasteners, consult your
building maintenance group or
contractor.
Warning
Do not locate the NANOpure DIamond
UV directly over equipment that
requires electrical service. Routine
maintenance of this unit may involve
water spillage and subsequent electri-
cal shock hazard if improperly located.
Do not use in the presence of
flammable materials; fire or explosion
may result. This device contains
components which may ignite such
materials.
Other Accessories
Optional accessories for this unit include a float switch,
low pressure switch, N.I.S.T. Traceable Calibration
Module, remote dispenser, and printer. Installation proce-
dures for these accessories are explained in later sec-
tions of this manual.
INSTALLATION
10
Dieses Handbuch passt für folgende Modelle
2
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