Barnstead D14031 Bedienungsanleitung

DIamond™TII
Type II water system
Operation Manual
Model No. Description Voltage
D14031 12 LPH 100V - 240V
D14041 24 LPH 100V - 240V
LT1403X8 • 10/05/06

Safety Information ..................................................................................................................................................................4
Alert Signals ....................................................................................................................................................................4
Warnings..........................................................................................................................................................................4
Introduction ..........................................................................................................................................................................6
Product Overview ............................................................................................................................................................6
General Usage ................................................................................................................................................................6
General Specifications............................................................................................................................................................7
Dimensions and Clearance Requirements......................................................................................................................7
Electrical Requirements ..................................................................................................................................................7
Feedwater Requirements ................................................................................................................................................7
DI Product Water ............................................................................................................................................................7
RO System ......................................................................................................................................................................8
RO Membrane Performance ..........................................................................................................................................8
Environmental Conditions................................................................................................................................................9
Declaration of Conformity................................................................................................................................................9
Unpacking ........................................................................................................................................................................10
Installation ........................................................................................................................................................................11
Locating Unit..................................................................................................................................................................11
Bench Mounting......................................................................................................................................................11
Wall Mounting ........................................................................................................................................................11
Installing the Control Panel in a Remote Location ........................................................................................................12
Component Installation..................................................................................................................................................13
UV Lamp Installation ..............................................................................................................................................13
Water Connection Details..............................................................................................................................................14
Push-to-Connect Fitting Tubing Installation ..........................................................................................................14
Push-to-Connect Fitting Tubing Removal ..............................................................................................................14
Tubing Adapter Fittings ..........................................................................................................................................15
Quick Disconnect Fittings ......................................................................................................................................16
Cartridge and Membrane Installation ............................................................................................................................17
Prefilter Installation..........................................................................................................................................17
MPS Cartridge Installation ..............................................................................................................................17
Carbon Filter Installation ................................................................................................................................18
RO Membrane Installation ..............................................................................................................................18
Cartridge Pack Installation ..............................................................................................................................20
Water Service Connections ..........................................................................................................................................21
Feedwater Connection ..........................................................................................................................................21
Atmospheric Drain..................................................................................................................................................21
Reservoir Connection ............................................................................................................................................21
Power Connections ......................................................................................................................................................22
Optional Accessories ....................................................................................................................................................22
Dispense Overflow Cutoff Float ............................................................................................................................23
Performing an Electronic Calibration Using the Optional N.I.S.T. Calibration Module ..........................................24
Manual Remote Dispenser and Accu DIspense™ Volumetric Remote Dispenser................................................24
Controls ................................................................................................................................................................................25
Control Panel ................................................................................................................................................................25
Buttons ........................................................................................................................................................................25
Initial Operation ....................................................................................................................................................................27
RO Membrane Rinse Up ..............................................................................................................................................27
System Sanitization Procedure ....................................................................................................................................27
Cartridge Pack Rinse Up ..............................................................................................................................................29
Operational Modes ........................................................................................................................................................29
Idle Mode................................................................................................................................................................29
Run Mode ..............................................................................................................................................................29
Standby Mode ........................................................................................................................................................30
2
Table of Contents

Flush Mode ............................................................................................................................................................30
Automatic Flush (RO Membrane) ..................................................................................................................30
Manual Flush (RO Membrane) ......................................................................................................................30
Normal Operation ..........................................................................................................................................................31
Dispensing Water ..........................................................................................................................................................31
Automatic Dispensing....................................................................................................................................................32
Reservoir Replenishment ..............................................................................................................................................32
User Settings ................................................................................................................................................................33
Setting the Displayed Language ............................................................................................................................33
Setting the Time and Date ....................................................................................................................................33
Setting the Low Product Purity Alarm ....................................................................................................................33
Setting the RO % Reject Alarm..............................................................................................................................34
Setting the Feedwater Chlorine Level....................................................................................................................34
Setting System Options ................................................................................................................................................35
Auto Standby Timer................................................................................................................................................35
Unit Under Counter ................................................................................................................................................35
Display Contrast ....................................................................................................................................................35
Set Units ................................................................................................................................................................36
Printer Attached......................................................................................................................................................36
Reservoir Type ......................................................................................................................................................37
Computer/Printer Setup ........................................................................................................................................................37
Connecting DIamond TII to Computer and Communicating Through the RS-232 Port Using Hyperterminal or Procomm ....37
Hyperterminal....................................................................................................................................................................37
Procomm ..........................................................................................................................................................................38
Connecting and Starting the Printer ........................................................................................................................................40
Maintenance and Servicing ..................................................................................................................................................40
System Sanitization ......................................................................................................................................................40
Prefilter Replacement ....................................................................................................................................................40
MPS Replacement ........................................................................................................................................................40
Carbon Replacement ....................................................................................................................................................41
Cartridge Pack Replacement ........................................................................................................................................41
RO Membrane Replacement ........................................................................................................................................42
0.2 Micron Final Filter Replacement ............................................................................................................................43
Fuse Replacement ........................................................................................................................................................44
UV Lamp Replacement ................................................................................................................................................44
Resetting Routine Timers ..............................................................................................................................................45
Prefilter, MPS, Carbon, Membrane and Cartridge Pack Timers ............................................................................45
Reservoir Vent Timer..............................................................................................................................................45
System UV Timer ..................................................................................................................................................46
Reservoir UV Timer................................................................................................................................................46
Sanitization Timer ..................................................................................................................................................46
Shutdown ......................................................................................................................................................................46
General Cleaning Instructions ......................................................................................................................................46
Troubleshooting ....................................................................................................................................................................47
System Alarms ..............................................................................................................................................................49
Routine Care ................................................................................................................................................................54
Replacement Parts ..............................................................................................................................................................55
Consumables ................................................................................................................................................................55
General Maintenance ....................................................................................................................................................56
Safety Stock ..................................................................................................................................................................56
Wiring Diagrams ..................................................................................................................................................................57
Ordering Procedures ............................................................................................................................................................59
One Year Limited Warranty ..................................................................................................................................................60
3
TABLE OF CONTENTS

Your Barnstead International DIamond TII Type II water
system has been designed with function, reliability, and
safety in mind. It is your responsibility to install it in con-
formance with local electrical codes. This manual con-
tains important safety information. You must carefully read
and understand the contents of this manual prior to the
use of this equipment. For safe operation, please pay
attention to the alert signals throughout the manual.
Water purification technology employs one or more of the
following: chemicals, electrical devices, mercury vapor
lamps, steam and heated vessels. Care should be taken
when installing, operating or servicing Barnstead
products. The specific safety notes pertinent to this
Barnstead product are listed below.
Warnings
To avoid electrical shock, always:
1. Use a properly grounded electrical outlet of
correct voltage and current handling capacity.
2. Do not locate the DIamond TII directly over
equipment that requires electrical service.
Routine maintenance of this unit may involve
water spillage and subsequent electrical shock
hazard if improperly located.
3. Replace fuses with those of the same type and
rating.
4. Do not disassemble water lines or remove car-
tridges where spilled water could contact
equipment that requires electrical service.
Electrical shock hazard could result.
5. Power unit OFF before plugging in or unplug-
ging unit.
6. Disconnect from the power supply prior to main-
tenance and servicing.
To avoid personal injury:
1. Do not use in the presence of flammable or
combustible materials; fire or explosion may
result. This device contains components which
may ignite such materials.
4
Safety Information
Caution
Cautions alert you to a possibility of
damage to the equipment.
Warning
Warnings alert you to a possibility of
personal injury.
Note
Notes alert you to pertinent facts and
conditions.
Alert Signals
Note
The UV lamp contains mercury. If bro-
ken or no longer needed, do not dis-
pose of the UV lamp in the trash.
Recycle or dispose of the UV lamp as
hazardous waste.

2. Do not use in the presence of highly corrosive
substances such as bleach or acid baths; fire
may result.
3. This device is to be used with water feeds only.
Sanitizing agents must be used in compliance
with instructions in this manual. Failure to com-
ply with the above could result in explosion and
personal injury.
4. Avoid splashing cleaning solutions on clothing or
skin.
5. Ensure all piping connections are tight to avoid
chemical leakage.
6. Ensure adequate ventilation.
7. Carefully follow manufacturer’s safety
instructions on labels of chemical containers and
material safety data sheets.
8. This unit is equipped with an ultraviolet lamp.
Ultraviolet radiation is harmful to the eyes and
skin. Do not attempt to observe the lamp
directly.
9. Refer servicing to qualified personnel.
5
SAFETY INFORMATION

6
Introduction
Product Overview
The Barnstead DIamond TII is a tap-fed water purification
system designed to be simple to use and to provide
reagent grade water that exceeds ASTM Type II, and
NCCLS/CAP Type I standards. It uses a thin film compos-
ite reverse osmosis membrane with pretreatment to pro-
duce RO water that is then polished using a two-stage
deionization process combined with UV oxidation and a
0.2 micron final filter.
The % of the rejection between incoming and reverse
osmosis product water is monitored and an indication is
provided to the user if the RO water quality is unaccept-
able. Incoming and RO pressure are provided by pres-
sure sensors located inside the unit. The DI water purity
is continuously sensed by a resistivity cell and displayed
on a graphical display.
RO operation is automatic and works independently of the
DI system to fill the external reservoir as determined by
sensors in the reservoir.
The DIamond TII is not shipped with pretreatment and DI
polishing cartridges or a final filter. These must be
ordered separately. The start-up kit containing these
components can be ordered using part number D502138
for all units.
The electronics can be verified and calibrated utilizing a
N.I.S.T. Traceable Calibration Module. See accessory
ordering information.
Please read the instructions carefully to ensure that you
receive maximum benefit from the DIamond TII. Also,
please fill out and return the enclosed warranty registra-
tion card as it will help us assure you of proper warranty
coverage.
General Usage
Do not use this product for anything other than its intend-
ed usage. If the equipment is used in a manner not speci-
fied by the manufacturer, the protection provided by the
equipment may be impaired.

7
Dimensions and Clearance Requirements
DIamond TII dimensions - 13.5" W X 18.5" D X 19.5" H (34.3 cm X 47.0 cm X 49.5 cm)
Clearances:
Sides - 9" (22.9 cm) minimum to allow for servicing
Above - 3" (7.6 cm) minimum for removal of top cover
Front - 4.75" (12.1 cm) minimum for opening front door
Electrical Requirements
The DIamond TII is equipped with two power cords and corresponding fuses taped to each power cord to be
plugged into a grounded electrical outlet of the appropriate voltage.
All models: 100-240 VAC +5% -10%, 47-63 Hz.
Feedwater Requirements1
Types1Tap (Potable)
Turbidity 1.0 N.T.U. maximum
Pressure Range 2 bar (30 psig) to 6.9 bar (100 psig)
Temperature Range 4-40°C (39-104°F)
Minimum Inlet Flow Requirements 100 lph
pH 3-10
TDS 600 (max. ppm as CaCO3)
Silt Density Index <5%
Free Chlorine <3 ppm
Langlier Saturation Index <1
Iron (total as Fe) <0.5 ppm
Silica <30 ppm
DI Product Water
Quality
Resistivity: ASTM Type II, NCCLS Type I >15 megohm/cm
TOC: <15 PPB
Flow Rate: up to 1 LPM with a new D3750 final filter
Bacteria: Less than 1 CFU/ml
Volumetric Dispense:
Accuracy: ±5%
Repeatability: ±3%
Feedwater suitability must be determined by a water analysis
General Specifications
1500 ppm NaCl feedwater solution @ 25°C
(77°F), @ 4.5 bar (65 psig), 15% recovery.
Flow rate and recovery will decrease with
lower water temperature and pressure.
Barnstead recommends the use of a hot
water mixing valve before the RO system for
water cooler than 15°C (59°F).

8
RO System
Model RO Product Flow Rate Recovery
D14031 12 lph ±15% (3.2 gph) 10-20%
D14041 24 lph ±15% (6.3 gph) 20-40%
RO Membrane Performance1
Rejection
Inorganic (minimum) >90%
Inorganic (typical) >95%
Particles >99%
Bacteria >99%
Organics (>300 MW) >99%
1500 ppm NaCl feedwater solution @ 25°C (77°F), @ 4.5 bar (65 psig), 15% recovery. Flow rate and recov-
ery will decrease with lower water temperature and pressure. Barnstead recommends the use of a hot water
mixing valve before the RO system for water cooler than 15°C (59°F).
GENERAL SPECIFICATIONS

9
Environmental Conditions
Operating: 15°C - 30°C; 20% - 80% relative humidity, non-condensing. Installation Category II
(overvoltage) in accordance with IEC 664. Pollution Degree 2 in accordance with IEC 664.
Altitude limit: 2,000 meters.
Storage: -25°C - 65°C; 10% to 85% relative humidity.
Declaration of Conformity
Barnstead International hereby declares under its sole responsibility that this product conforms with the tech-
nical requirements of the following standards:
EMC: EN 61000-3-2 Limits for harmonic current emissions
EN 61000-3-3 Limits for voltage fluctuations and flicker
EN 61326-1 Electrical equipment for measurement, control, and
laboratory use - EMC requirements; Part I: General
Requirements
Safety: EN 61010-1 Safety requirements for electrical equipment for
measurement, control, and laboratory use;
Part I: General Requirements
per the provisions of the Electromagnetic Compatibility Directive 89/336/EEC, as amended by 92/31/EEC and
93/68/EEC, and per the provisions of the Low Voltage Directive 73/23/EEC, as amended by 93/68/EEC.
The authorized representative located within the European Community is:
Electrothermal Engineering Ltd.
419 Sutton Road
Southend On Sea
Essex SS2 5PH
United Kingdom
Copies of the Declaration of Conformity are available upon request.
GENERAL SPECIFICATIONS

10
Unpacking
Remove the unit from its shipping container and ensure that the
following items are removed from the packaging materials
before discarding:
1) DIamond TII unit
2) Approximately 6 ft. (1.83 m) of 1/4” (0.64 cm) O.D.
drain tubing (TU1190X12) with a 1/4” NPT fitting at one
end
3) Approximately 10 ft. (3.05 m) of 3/8” (0.95 cm) O.D.
feedwater tubing provided with a quick disconnect
insert on one end and a 1/4” NPT fitting on other end
(TU1119X7)
4) Two approximately 10 ft. of 3/8” O.D. tubes for fluidical-
ly connecting the unit to the storage reservoir. One tube
will have an integral shut-off connection (see Quick
Disconnect Fittings section of this manual)
5) For Model D14041 only: Membrane Reject 1 to
Membrane Feed 2 tube
6) North American power cord with attached (1.6 amp)
fuse bag (CRX72)
7) European power cord with attached (0.63 amp) fuse
bag (CRX70)
8) UV lamp (LMX13)
9) Hose barb fitting (05930BI) – Attached to unit dispens-
ing valve
10) Tube removal tool (AYX23)
11)Wall Bracket - Unit (BC1190X12)
12) Wall Bracket - Remote Display (BC1190X10)
13) Display Cable (WH1403X4)
14) Blank Display (DL1190X18)
15) Plug Adapter (CEX42)
16) If a DIamond TII storage reservoir (D14061, D14062,
D14063, D14064, D14071, D14072, D14073 or
D14074) is also purchased, see contents in separate
box.
Also required for installation: Customer-supplied fasteners to
mount unit and remote display.
Dieses Handbuch passt für folgende Modelle
3
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