Teledyne Cetac Technologies SPM-700 Bedienungsanleitung
SPM-700 Syringe Pump Module
Manual Part Number 610108 Rev 0
Installation Guide
COPYRIGHT
© 2018 Teledyne CETAC Technologies
610108 Rev 0 , December, 2018
Teledyne CETAC Technologies authorizes its
customers to reproduce, transmit, or store
this document in its entirety, including this
page, for the express purpose of installing,
operating, or maintaining the product
described herein.
Teledyne CETAC Technologies
Customer Service & Support
14306 Industrial Road
Omaha, Nebraska 68144, USA
Phone (800) 369-2822 (USA only)
Phone (402) 733-2829
E-mail cetacservice@teledyne.com
REVISIONS
Teledyne CETAC Technologies strives to
provide the scientific community with an
unparalleled combination of effective
technology and continuing value. Modular
upgrades for existing instruments will
continue to be a prime consideration as
designs progress.
Teledyne CETAC Technologies reserves the
right to revise this document and/or improve
products described herein at any time without
notice or obligation.
TRADEMARK ACKNOWLEDGEMENTS
Windows is a registered trademark of
Microsoft Corporation in the United States and
other countries.
PharMed and Tygon are registered
trademarks of Saint-Gobain Performance
Plastics.
DuPont™ and Viton® are trademarks or
registered trademarks of E.I. du Pont de
Nemours and Company.
Superthane is a registered trademark of
NewAge Industries, Inc.
KIMWIPES is a registered trademark and
KIMTECH SCIENCE is a trademark of
Kimberly-Clark Worldwide, Inc
All other marks are the property of their
respective owners.
3
Contents
1Introduction ..............................................................................................................4
Overview.................................................................................................................................... 4
Chemical Compatibility....................................................................................................... 4
Operator Qualifications....................................................................................................... 5
Choosing a Location for Installation ............................................................................. 5
Proximity to the Instrumentation ........................................................................... 5
Space Requirements...................................................................................................... 6
Power Requirements..................................................................................................... 6
Unpacking the Syringe Pump Module .......................................................................... 6
2Installing the Syringe Module.............................................................................7
Installing the Accessory Module Mounting Blocks................................................. 7
Mounting the Syringe Pump Modules .......................................................................... 9
Connecting the Tubing ......................................................................................................10
Connecting the Power Supply ........................................................................................11
Connecting the Syringe Module to the Autosampler ...........................................11
Connecting the Syringe Module Directly to the Host PC ....................................12
Connecting a USB Cable ............................................................................................12
Connecting a Serial Cable.........................................................................................13
Installing a Syringe..............................................................................................................13
Starting the Pump................................................................................................................14
Shutting Down the Pump .................................................................................................15
3Maintaining and Troubleshooting the Product......................................... 16
Cleaning the Syringe Module..........................................................................................16
Cleaning the Syringe...........................................................................................................16
Returning the Product to CETAC for Service...........................................................18
Shipping the Product..................................................................................................18
Product Warranty Statement .................................................................................18
4Safety and Regulatory Information ............................................................... 19
Safety Characteristics ........................................................................................................19
Environmental Characteristics...............................................................................19
Electrical Characteristics..........................................................................................20
Safety Notices ........................................................................................................................20
Power Cord Set Requirements and Maintenance............................................20
Mains Disconnect .........................................................................................................21
Mechanical Hazards ...................................................................................................21
Operating Environment.............................................................................................21
Explanation of Caution and Warning Notices..................................................22
Electromagnetic Interference ........................................................................................22
Explanation of Regulatory Marks.................................................................................23
4
1Introduction
Overview
FIGURE 1-1 Front and Back Views.
The color and branding of the module may vary from what is shown here.
Chemical Compatibility
The syringe module is intended for use with sample matrices with the
following characteristics:
low-acid aqueous solutions (up to 1% HNO3 or HCl)
low-viscosity oils
low to high dissolved solids
The system is not suitable for high viscosity samples.
NOTICE
Avoid use with chemicals which are likely to precipitate or form deposits on
the internal surfaces, such as silver chloride. Samples which contain AgCl may
contaminate the internal surfaces and require the replacement of the tubing.
Wetted components are made of Polyetherimide (PEI) and
Polytetrafluoroethylene (PTFE). When these inert, non-metallic materials are
Power Switch
Serial Port
USB Port
RS-485 Ports
Power Connector
Valve with Input
and Output Ports
Syringe
Plunger
Thumbscrew
5
used at temperatures less than 135°C, they can withstand repeated exposure
to the following substances:
Predominantly aqueous solutions of acids (less than 10%), including HNO3
and HCl.
Predominantly aqueous solutions of strong bases (less than 10%)
Common organic solvents such as acetone, alcohols, ethyl acetate,
Methylethylketone (MEK), petroleum oils and derived fuels,
tetrachloroethylene, toluene, kerosene and xylene.
NOTICE
DAMAGE FROM CHEMICAL EXPOSURE
Prolonged or repeated exposure to temperatures greater than 135°C and to
the following substances can cause failure of the wetted components:
Acids greater than 10%.
Hydrofluoric acid (HF).
Solutions of concentrated bases (greater than 10% potassium,
ammonium, or sodium hydroxides).
Partially halogenated hydrocarbons or extremely aggressive organic
solvents (chloroform, methylene dichloride, 1,1,2-trichloroethane).
Operator Qualifications
To use this product, you should have a working knowledge of the equipment
with which the syringe module will be used.
WARNING
CHEMICAL INJURY HAZARD
Make sure you know the hazards associated with all of the chemicals you
are using, and take the appropriate precautions. Exposure to laboratory
chemicals may result in serious injury.
Choosing a Location for Installation
Proximity to the Instrumentation
Tubing length affects the time it takes for fluid to reach its destination and the
volume of fluid required. When introducing very small sample volumes (flow
rates less than 50 µL min-1), minimize the length of the connecting sample
tubing. For the introduction of sample volumes to analytical instrumentation
such as ICP-MS, where flow rates of greater than 50 µL min-1 will be employed,
the length of connecting sample tubing between the syringe pump and a
nebulizer is less critical. The syringe module can be mounted on either side of
the autosampler or it may be placed on the workbench.
6
Space Requirements
You will need easy access to the back of the syringe module to reach the power
switch. As a minimum, allow at least 5 cm behind the syringe module for cable
egress, ventilation, and access to the power switch. Always position the
equipment so that it is easy to disconnect the power cord.
Power Requirements
The syringe module receives power through the connection to the external
desktop “brick” power supply. Place the module within 1.2 meters of a power
outlet.
WARNING
SHOCK AND FIRE HAZARD
Use only the provided power supply. The power supply must be plugged into
an outlet which has a protective ground connection.
The power supply must be connected to an AC power source that will not
apply more than 240VAC between the supply conductors and ground. A
protective ground connection is required for safe operation.
Ensure that you position the syringe module so that the plug is easily
accessible (is not blocked) and can be quickly disconnected if needed. In case
of hazard, the power cord should be disconnected from the wall socket. Do not
plug in the power supply until ready to operate the pump.
Unpacking the Syringe Pump Module
Inspect external packaging upon receipt for signs of shipping damage. Inspect
all items during unpacking and notify the carrier immediately of any concealed
damage.
If the system is shipped or removed from storage during cold weather, allow
the equipment to equilibrate to room temperature before opening and
exposing to warm, humid air.
CAUTION
EQUIPMENT DAMAGE FROM CONDENSATION
If condensation forms on or inside the pump module, allow it to dry
thoroughly before connecting it to a power source and operating it. Failure to
do so may cause equipment damage.
NOTE
Keep the factory packaging for use in case the product ever needs to be
returned or shipped to another location.
7
2Installing the Syringe
Module
The syringe pump module may be placed on the workbench, or it can be
attached to the autosampler using an optional mounting block.
Installing the Accessory Module Mounting Blocks
The syringe pump module can be mounted on an accessory mounting block,
and the mounting block can be installed on either side of the autosampler.
There are two types of mounting blocks. An inside mounting block is designed
to attach directly to the autosampler. An outside mounting block is designed to
attach to an inside mounting block.
FIGURE 2-1 Mounting Blocks.
You will need a Philips head screwdriver and a set of Allen (hex) wrenches.
1Turn the power switches on the power supply, autosampler, and syringe pump
module OFF.
2Place an inside mounting block next to the autosampler on the side where you
want it.
Inside Block
Outside Block
Syringe Pump Module Installation Guide
Chapter 2: Installing the Syringe Module
8
3Check that the black pin is in the position toward the front of the autosampler.
If necessary, turn the block over and move the pin to the other hole.
FIGURE 2-2 Position of Pin on Mounting Block (Bottom View).
4Use four hex-head screws to attach the mounting block to the frame of the
autosampler.
FIGURE 2-3 Attaching the Mounting Block.
The installed mounting block should look like this:
FIGURE 2-4 Inside Mounting Block After Installation.
5If more than one module is needed on one side of the autosampler, then an
outside mounting block needs to be fitted to accommodate that module. The
outside mounting block can be fitted by positioning the white mounting pins
on the side of the block (as shown in FIGURE 2-1) into the spaces in the side of
the inside mounting block (as can be seen in FIGURE 2-4) and pushing the
outside mounting block down until it is flush with the inside mounting block.
Front
Back
Syringe Pump Module Installation Guide
Chapter 2: Installing the Syringe Module
9
Mounting the Syringe Pump Modules
1Place the syringe pump on the mounting block. The black pin on the block fits
into the hole on the underside of the module.
2Push the module back until the front is flush with the front of the autosampler.
FIGURE 2-5 Mounting the Syringe Pump
NOTE
To remove the pump from its mounting block, slide it forward as far as it will
go, then slide it back about 1 mm before lifting it.
Syringe Pump Module Installation Guide
Chapter 2: Installing the Syringe Module
10
Connecting the Tubing
NOTICE
Tighten the fittings using only your fingers. Turn the fittings slowly at first,
making sure they are not cross-threaded. Using excessive force will damage
both the fittings and the valve.
The direction of liquid flow through the valve at the top of the syringe is set by
software.
FIGURE 2-6 Liquid Flow When Output Is Set To the Right Side
1Place a connector and ferrule on the free end of the input tubing. Do the same
for the output tubing.
FIGURE 2-7 Installing the Connector and Ferrule
2Connect the tubing to the valve at the top of the syringe pump. Tighten the
connectors using your fingers.
NOTE
The tubing and connectors may vary by application.
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