Agilent Technologies SD-1 Bedienungsanleitung

Agilent Technologies

Agilent SD-1 Isocratic

Solvent Delivery Module

User Manual

SD-1 Solvent Delivery - User Manual

Notices

No part of this manual may be reproduced

in any form or by any means (including elec-

tronic storage and retrieval or translation

into a foreign language) without prior agree-

ment and written consent from Agilent

Technologies, Inc. as go v e r n e d b y U n i t e d

States and international copyright laws.

Manual Part Number

G9302-90001

Edition

01/2013

Printed in Germany

Agilent Technologies

Hewlett-Packard-Strasse 8

76337 Waldbronn

This product may be used as a com-

ponent of an in vitro diagnostic sys-

tem if the system is registered with

the appropriate authorities and com-

plies with the relevant regulations.

Otherwise, it is intended only for gen-

eral laboratory use.

Warranty

The material contained in this docu-

ment is provided “as is,” and is sub-

ject to being changed, without notice,

in future editions. Further, to the max-

imum extent permitted by applicable

law, Agilent disclaims all warranties,

either express or implied, with regard

to this manual and any information

contained herein, including but not

limited to the implied warranties of

merchantability and fitness for a par-

ticular purpose. Agilent shall not be

liable for errors or for incidental or

consequential damages in connection

with the furnishing, use, or perfor-

mance of this document or of any

information contained herein. Should

Agilent and the user have a separate

written agreement with warranty

terms covering the material in this

document that conflict with these

terms, the warranty terms in the sep-

arate agreement shall control.

Technology Licenses

The hardware and/or software described in

this document are furnished under a license

and may be used or copied only in accor-

dance with the terms of such license.

Restricted Rights Legend

If software is for use in the performance of a

U.S. Government prime contract or subcon-

tract, Software is delivered and licensed as

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defined in DFAR 252.227-7014 (June 1995),

or as a “commercial item” as defined in FAR

2.101(a) or as “Restricted computer soft-

ware” as defined in FAR 52.227-19 (June

1987) or any equivalent agency regulation

or contract clause. Use, duplication or dis-

closure of Software is subject to Agilent

Technologies’ standard commercial license

terms, and non-DOD Departments and

Agencies of the U.S. Government will

receive no greater than Restricted Rights as

defined in FAR 52.227-19(c)(1-2) (June

1987). U.S. Government users will receive

no greater than Limited Rights as defined in

FAR 52.227-14 (June 1987) or DFAR

252.227-7015 (b)(2) (November 1995), as

applicable in any technical data.

Safety Notices

CAUTION

A CAUTION notice denotes a

hazard. It calls attention to an

operating procedure, practice, or

the like that, if not correctly per-

formed or adhered to, could

result in damage to the product

or loss of important data. Do not

proceed beyond a CAUTION

notice until the indicated condi-

tions are fully understood and

met.

WARNING

A WARNING notice denotes a

hazard. It calls attention to an

operating procedure, practice,

or the like that, if not correctly

performed or adhered to, could

result in personal injury or

death. Do not proceed beyond a

WARNING notice until the indi-

cated conditions are fully under-

stood and met.

SD-1 Solvent Delivery - User Manual 3

In This Book

This manual contains information on:

•Agilent SD-1 Isocratic Solvent Delivery Module (G9302A)

•Agilent SD-1 Add-on Solvent Delivery Module (G9303A)

1Introduction

This chapter gives an instrument overview.

2 Site Requirements and Specifications

This chapter provides information on environmental requirements, physical

and performance specifications.

3Installation

This chapter gives information about the installation of your instrument.

4 Using the SD-1 Solvent Delivery Module

This chapter explains the operational parameters of the instrument.

5 Optimizing Performance

This chapter gives hints on how to optimize the performance or use additional

devices.

6 Troubleshooting and Diagnostics

This chapter gives an overview about the troubleshooting and diagnostic

features.

7 Error Information

This chapter describes the meaning of error messages, and provides

information on probable causes and suggested actions how to recover from

error conditions.

4 SD-1 Solvent Delivery - User Manual

In This Book

8 Maintenance and Repair

This chapter describes the maintenance of the instrument.

9Parts

This chapter provides information on parts for the instrument.

10 Cables

This chapter provides information on cables used with the instrument.

11 Appendix

This chapter provides addition information on safety, legal and web.

SD-1 Solvent Delivery - User Manual 5

Contents

1Introduction 7

Introduction to the System 8

Physical Layout 9

Check Valves 12

Control 14

2 Site Requirements and Specifications 23

Site Requirements 24

Physical Specifications 27

Performance Specifications 28

3Installation 31

Installation 32

4 Using the SD-1 Solvent Delivery Module 33

Hints for Successful Use of the Pump 34

Introduction 36

Power On 37

Initial Operation 38

Operation 42

5 Optimizing Performance 53

Maximum Pressure versus Flow 54

Scale-Up 55

System Requirements for High Performance Prep Chromatography 56

6 Troubleshooting and Diagnostics 61

Introduction to Troubleshooting and Diagnostics 62

Using the Pressure Display as Diagnostic Tool 63

Troubleshooting Guide 64

6 SD-1 Solvent Delivery - User Manual

Contents

7 Error Information 71

What are Error Messages 72

Pump Error Messages 73

8 Maintenance and Repair 77

Introduction to Maintenance 78

Warnings and Cautions 79

Maintenance Schedule 81

Service Logs 83

Clearing Air Bubbles from the Liquid Head 84

Replacing Seals 86

Replacing Piston 92

Cleaning Check Valves 95

Replacing Check Valves 97

Checking and/or Changing Power Fuses (F1) 99

9Parts 101

Modules 102

Pump Heads 103

Accessories 104

Pump Head Replacement Parts 105

10 Cables 109

Cable Overview 110

Cable Connections 111

11 Appendix 113

General Safety Information 114

Solvent Miscibility 120

The Waste Electrical and Electronic Equipment (WEEE) Directive

(2002-96-EC) 121

Batteries Information 122

Radio Interference 123

Electromagnetic Compatibility 124

Agilent Technologies on Internet 126

SD-1 Solvent Delivery - User Manual

Agilent Technologies

Introduction

Introduction to the System 8

Physical Layout 9

Check Valves 12

Control 14

This chapter gives an instrument overview.

8 SD-1 Solvent Delivery - User Manual

1Introduction

Introduction to the System

The Agilent SD-1 is an innovative HPLC solvent delivery system engineered

with preparative chromatographers in mind. Corrosion-resistant titanium

pump heads address the needs of biochemists for compatibility with

salt-containing buffers and freedom from unwanted metal ions. Each pump

head has a piston washing chamber to prevent deposition of abrasive salt

residues behind the high-pressure seal, thereby greatly extending seal life.

Major new technology includes dual independent linear piston drives. Rather

than operating both heads from cams attached to a single motor, as in

conventional dual piston pumps, the Agilent SD-1 uses two independent

stepper motors which connect to pistons via linear screw drives. The motors

reciprocate, rather than running only in one direction. Independent drive

frees the Agilent SD-1 from the operating constraints of mechanical cam

profiles and makes it the first dual piston pump to produce entirely pulse-free

flow under all operating conditions, without auxiliary hydromechanical pulse

dampers. Totally pulse-free flow favors improved column performance and

extended column life by saving expensive preparative columns from the

constant pressure-pulse pounding typical of other large piston and diaphragm

pumps.

In addition, the Agilent SD-1 meters flow at a constant rate independent of

solvent compressibility and without the slight refill-associated flow deficits

seen with conventional single-motor dual-piston models. In gradient

operation, this produces more precise composition profiles without the time

and volume delays introduced by large mixing chambers. Plus, flow rates

extend well into the analytical HPLC range, permitting method development

on smaller columns without interchanging heads.

Each Agilent SD-1 pump includes a standard serial interface for flow control.

A built-in two-channel analog-to-digital converter allows the computer to

collect data from HPLC detectors. Contact closure inputs and outputs are

provided for system automation. Firmware includes Good Laboratory

Practices (GLP) logging features.

SD-1 Solvent Delivery - User Manual 9

Introduction 1

Physical Layout

Figure 1 Agilent SD-1 Isocratic Solvent Delivery Module – front view

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10 SD-1 Solvent Delivery - User Manual

1Introduction

Physical Layout

Figure 2 Agilent SD-1 Isocratic Solvent Delivery Module – liquid end detail

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