Agilent Technologies 5973N Handbuch

Agilent Technologies

5973N and 5973 inert

Mass Selective Detector

Hardware Installation

2Hardware Installation

Notices

No part of this manual may be reproduced in

any form or by any means (including elec-

tronic storage and retrieval or translation

into a foreign language) without prior agree-

ment and written consent from Agilent

Technologies, Inc. as governed by United

States and international copyright laws.

Manual Part Number

G2589-90073

Edition

First edition, August 2003

Replaces part number G2589-90006

Printed in USA

Agilent Technologies, Inc.

2850 Centerville Road

Wilmington, DE 19808-1610 USA

Warranty

The material contained in this docu-

ment is provided “as is,” and is sub-

ject to being changed, without notice,

in future editions. Further, to the max-

imum extent permitted by applicable

law, Agilent disclaims all warranties,

either express or implied, with regard

to this manual and any information

contained herein, including but not

limited to the implied warranties of

merchantability and fitness for a par-

ticular purpose. Agilent shall not be

liable for errors or for incidental or

consequential damages in connec-

tion with the furnishing, use, or per-

formance of this document or of any

information contained herein. Should

Agilent and the user have a separate

written agreement with warranty

terms covering the material in this

document that conflict with these

terms, the warranty terms in the sep-

arate agreement shall control.

Safety Notices

CAUTION

A CAUTION notice denotes a haz-

ard. It calls attention to an operat-

ing procedure, practice, or the like

that, if not correctly performed or

adhered to, could result in damage

to the product or loss of important

data. Do not proceed beyond a

CAUTION notice until the indicated

conditions are fully understood and

met.

WARNING

A WARNING notice denotes a

hazard. It calls attention to an

operating procedure, practice, or

the like that, if not correctly per-

formed or adhered to, could result

in personal injury or death. Do not

proceed beyond a WARNING

notice until the indicated condi-

tions are fully understood and

met.

Acknowledgements

Microsoft® and Windows® are U.S. regis-

tered trademarks of Microsoft Corporation.

Swagelok® is a registered trademark of the

Swagelok Company.

Hardware Installation 3

Contents

1 General Information

Introduction 8

Important Safety Warnings 10

Many internal parts of the MSD carry dangerous voltages 10

Electrostatic discharge is a threat to MSD electronics 10

Many parts are dangerously hot 11

Hydrogen 11

Safety and Regulatory Certifications 13

Information 13

Symbols 14

Electromagnetic compatibility 15

Sound emission certification for Federal Republic of

Germany 15

Cleaning 16

Recycling the Product 16

Customer Responsibilities 17

Before You Start 18

Other Documentation 19

This section provides information on how to identify

specifically what type of MSD you are working with as well as

how to properly clean and dispose of the instrument. Also

included in this section are the “Important Safety Warnings”

which list critical safety precautions for all users.

8Hardware Installation

General Information

Introduction

This document provides installation instructions for the Agilent

Technologies 5973N and 5973 inert Mass Selective Detector

(MSD). Installation must be performed by an Agilent

Technologies service representative.

The Agilent Technologies 5973N Mass Selective Detector (MSD)

is a diffusion pump MSD while the 5973 inert Mass Selective

Detectors (MSDs) are turbo pump MSDs. This document will

refer to the 5973N MSD or 5973 inert MSD as 5973 Series MSD

unless otherwise noted.

The 5973 Series MSD system consists of:

•5973N or 5973 inert MSD

•Optional 59864B vacuum gauge controller (required for CI

operation)

•Gas Chromatograph

6890 Series GC, with options for MSD use

7683 Automatic Liquid Sampler (optional)

•PC and MSD ChemStation software

Refer to your MSD ChemStation documentation for

additional information

Table 1 lists possible configurations for the 5973 Series MSD.

Figure 1 identifies many of the common parts.

General Information

Hardware Installation 9

Table 1 Possible configurations

G2577A G2578A G2579A G2589A

High vac

pump

Diffusion

Pump

Standard turbo

pump

Performance

turbo pump

Performance

turbo pump

CI No No No PCI/NCI

59864B

gauge

controller

Recommended Recommended Recommended Required

DIP

compatible

(3rd party)

Yes Ye s Yes No

Figure 1 5973 Series MSD system

6890 Series

Gas Chromatograph

5973 Series

MSD

890 Series

LS tower

CI gas flow module

(EI/PCI/NCI MSDs only)

6890 Series

ALS tray

59864B high vacuum

Gauge Controller

5973 Series MSD LCP

10 Hardware Installation

General Information

Important Safety Warnings

Before moving on, there are several important safety notices

that you should always keep in mind when using the 5973 Series

MSD.

Many internal parts of the MSD carry dangerous voltages

If the MSD is connected to a power source, even if the power

switch is off, potentially dangerous voltages exist on the wiring

between the MSD power cord and the AC power supply, the AC

power supply itself, and the wiring from the AC power supply to

the power switch.

With the power switch on, potentially dangerous voltages also

exist on:

•All electronics boards in the instrument.

•The internal wires and cables connected to these boards.

•The wires for any heater (oven, detector, inlet, or valve box).

Electrostatic discharge is a threat to MSD electronics

The printed circuit (PC) boards in the MSD can be damaged by

electrostatic discharge. Do not touch any of the boards unless it

is absolutely necessary. If you must handle them, wear a

grounded wrist strap and take other antistatic precautions.

Wear a grounded wrist strap any time you must remove the MSD

right side cover.

WARNING All these parts are shielded by covers. With the covers in place, it

should be difficult to accidentally make contact with dangerous

voltages. Unless specifically instructed to, never remove a cover

unless the detector, inlet, or oven are turned off.

WARNING If the power cord insulation is frayed or worn, the cord must be

replaced. Contact your Agilent service representative.

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