Agilent Technologies InfinityLab LC Series Bedienungsanleitung

Diode Array Detectors

Agilent InfinityLab LC Series

User Manual

Agilent InfinityLab LC Series Diode Array Detectors User Manual

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Agilent InfinityLab LC Series Diode Array Detectors User Manual 3

In This Book

This manual covers the Agilent 1290 Infinity II Diode Array Detectors

•G7117A - 1290 Infinity II Diode Array Detector FS (with fixed slit)

•G7117B - 1290 Infinity II Diode Array Detector (with variable slit)

•G7117C - 1260 Infinity II Diode Array Detector HS (with fixed slit)

Find information on other Agilent Diode Array Detectors in separate manuals.

1 Introduction

This chapter gives an introduction to the detector and an instrument overview.

2 Site Requirements and Specifications

This chapter provides information on environmental requirements, physical and

performance specifications.

3 Using the Module

This chapter explains the essential operational parameters of the module.

4 Preparing the Module

This chapter provides information on how to set up the module for an analysis and

explains the basic settings.

5 Optimizing the Detector

This chapter provides information on how to optimize the detector.

6 Troubleshooting and Diagnostics

Overview about the troubleshooting and diagnostic features.

7 Error Information

This chapter describes the meaning of error messages, and provides information

on probable causes and suggested actions how to recover from error conditions.

Agilent InfinityLab LC Series Diode Array Detectors User Manual 4

8 Test Functions and Calibration

This chapter describes the tests for the module.

9 Maintenance

This chapter describes the maintenance of the module.

10 Parts and Materials for Maintenance

This chapter provides information on parts for maintenance.

11 Identifying Cables

This chapter provides information on cables used with the Agilent 1200 Infinity

Series modules.

12 Hardware Information

This chapter describes the detector in more detail on hardware and electronics.

13 LAN Configuration

This chapter provides information on connecting the module to the Agilent

ChemStation PC.

14 Appendix

This chapter provides addition information on safety, legal and web.

Agilent InfinityLab LC Series Diode Array Detectors User Manual 5

Contents

1 Introduction 9

Overview of the Module 10

Product Description 11

Optical System 14

Leak and Waste Handling 19

Operating Principle 24

2 Site Requirements and Specifications 25

Site Requirements 26

Physical Specifications 29

Performance Specifications 30

3 Using the Module 37

Magnets 38

Turn on/off 39

Status Indicators 41

Instrument Configuration 42

Set up the Detector with Agilent Open Lab ChemStation 44

The Detector User Interface 45

Detector Control Settings 47

Method Parameter Settings 48

4 Preparing the Module 52

Leak and Waste Handling 53

Setting up an Analysis 55

Solvent Information 62

Capillary Coding Guide 68

Installing Capillaries 71

Agilent InfinityLab LC Series Diode Array Detectors User Manual 6

5 Optimizing the Detector 75

Introduction 76

Optimization Overview 77

Optimizing for Sensitivity, Selectivity, Linearity and Dispersion 83

Optimizing Selectivity 94

Optimizing the Detector Regarding to the System 96

Warm up of the Detector 102

6 Troubleshooting and Diagnostics 104

Available Tests vs User Interfaces 105

Agilent Lab Advisor Software 107

7 Error Information 108

What Are Error Messages 109

General Error Messages 110

Detector Error Messages 116

8 Test Functions and Calibration 121

Introduction 122

Use of Max-Light Cartridge Test Cell 126

Conditions of Detector 127

Failing a Test 127

Self-Test 128

Intensity Test 130

Cell Test 132

Quick Noise Test 134

ASTM Drift and Noise Test 137

Slit Test 140

Wavelength Verification Test 143

Wavelength Calibration 145

D/A Converter (DAC) Test 148

Dark Current Test 150

Other Lab Advisor Functions 152

Agilent InfinityLab LC Series Diode Array Detectors User Manual 7

9 Maintenance 153

Introduction to Maintenance 154

Warnings and Cautions 154

Overview of Maintenance 156

Cleaning the Module 157

Remove and Install Doors 157

Replace the Deuterium Lamp 159

Replace the Max-Light Cartridge Cell 162

Clean the Max-Light Cartridge Cell 165

Storage of Max-Light Cartridge Cell 166

Correcting Leaks 167

Replace Leak Handling System Parts 168

Replace the Module Firmware 170

Information from Module’s Assemblies 171

10 Parts and Materials for Maintenance 172

Overview of Maintenance Parts 173

Accessory Kit 174

11 Identifying Cables 175

Cable Overview 176

Analog Cables 178

Remote Cables 180

CAN/LAN Cables 183

RS-232 Cables 184

USB Cables 184

12 Hardware Information 185

Firmware Description 186

Electrical Connections 189

Interfaces 192

Setting the 6-bit Configuration Switch 199

Instrument Layout 202

Early Maintenance Feedback 203

Agilent InfinityLab LC Series Diode Array Detectors User Manual 8

13 LAN Configuration 205

What You Have to Do First 206

TCP/IP parameter configuration 207

Configuration Switches 208

Initialization Mode Selection 209

Dynamic Host Configuration Protocol (DHCP) 211

Manual Configuration 214

14 Appendix 219

General Safety Information 220

Waste Electrical and Electronic Equipment (WEEE) Directive 226

Radio Interference 227

Sound Emission 227

Solvent Information 228

Agilent Technologies on Internet 229

Agilent InfinityLab LC Series Diode Array Detectors User Manual 9

1 Introduction

Overview of the Module 10

Product Description 11

Product Description G7117A 11

Product Description G7117B 12

Product Description G7117C 13

Optical System 14

Lamp 15

Max-Light Cartridge Flow Cell 15

Slit Assembly 16

Grating and Diode Array 18

Leak and Waste Handling 19

Waste Concept 23

Operating Principle 24

This chapter gives an introduction to the detector and an instrument overview.

Agilent InfinityLab LC Series Diode Array Detectors User Manual 10

1 Introduction

Overview of the Module

The detector is designed for highest optical performance, GLP compliance and

easy maintenance. It includes the following features:

•Maximum of 120 Hz (G7117A/G7117C) or 240 Hz (G7117B) data acquisition

rate.

•Higher sensitivity for conventional LC as well as ultra fast applications by

using next generation optical design.

•Increased sensitivity with 60 mm Max-Light cartridge flow cell.

•Optimized cell geometry for less peak dispersion for narrow bore applications.

•Max-Light cartridge flow cells for standard applications are available, see

“Max-Light Cartridge Flow Cell” on page 15.

•More reliable and robust peak integration process (automated) due to less

baseline noise/drift/refractive index and thermal effects especially under ultra

fast gradient conditions.

•RFID tracking technology is used for the UV-lamp and the Max-Light cartridge

flow cells.

•Multiple wavelength and full spectral detection at 120 Hz

(G7117A/G7117C)/240 Hz (G7117B) sampling rate, keeping up with the

analysis speed of ultra-fast LC.

•Programmable 1 – 8 nm slit (G7117B) or fixed 4 nm slit (G7117A/C) for rapid

optimization of sensitivity, linearity and spectral resolution provides optimum

incident light conditions.

•Improved Electronic temperature control (ETC) provides maximum baseline

stability and practical sensitivity under fluctuating ambient temperature and

humidity conditions.

•Additional diagnostic signals for temperature and lamp voltage monitoring.

•Easy exchange of flow cell by cartridge design.

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