ELTRA CS-2000 Bedienungsanleitung

Manual

Carbon and Sulfur Analyzer CS-2000

Translation

Eltra GmbH

Retsch-Allee 1-5

42781 Haan

Germany

 
 
 

 
Table of Contents 
1Contact information .............................................................................................................................. 6 
2Notes on the Manual ............................................................................................................................. 6 
1 Explanations of the Safety Instructions ............................................................................................. 7 
2 General Safety Instructions ............................................................................................................... 9 
3 Explanation of signs and symbols ................................................................................................... 10 
3Packaging, Transport and Installation .............................................................................................. 11 
1 Packaging........................................................................................................................................ 11 
2 Transport.......................................................................................................................................... 11 
3 Intended use.................................................................................................................................... 11 
4 Conditions for the Installation Site................................................................................................... 11 
5 Type Plate Description..................................................................................................................... 13 
4Installation............................................................................................................................................ 14 
1 Setting check up .............................................................................................................................. 14 
2 Front panel illustration ..................................................................................................................... 15 
3 Mains power connections................................................................................................................ 17 
4 Data Interface .................................................................................................................................. 18 
5 Gas connections.............................................................................................................................. 19 
6 Resistance furnace-Temperature adjustment ................................................................................. 20 
7 Gas purification furnance connecting (optional) .............................................................................. 21 
8 Autoloader (optional) ....................................................................................................................... 22 
5Analysis................................................................................................................................................ 23 
1 Working procedure .......................................................................................................................... 23 
1.1 Resistance furnace...................................................................................................................... 24 
1.2 Induction furnace ......................................................................................................................... 26 
2 Analysis example............................................................................................................................. 27 
2.1 Combustion peak......................................................................................................................... 27 
2.2 Combustion double peak............................................................................................................. 27 
3 Work breaks..................................................................................................................................... 28 
4 Crucibles preheating........................................................................................................................ 28 
4.1 Operating the pre-heating furnace (optional)............................................................................... 29 
5 TIC-determination (optional)............................................................................................................ 30 
5.1 TIC-module.................................................................................................................................. 30 
5.2 TIC analysis................................................................................................................................. 30 
5.3 TIC-module Operation procedure................................................................................................ 32 
6 Applications...................................................................................................................................... 33 
6.1 Induction furnace ......................................................................................................................... 33 
6.2 Resistance furnace...................................................................................................................... 37 
6.2.1 Coal analysis........................................................................................................................ 37 
6.2.2 Oil, plastics, asphalt and rubber analysis ............................................................................ 37 
6.2.3 Ash analysis......................................................................................................................... 38 
6.2.4 Graphite analysis................................................................................................................. 39 
6.2.5 Calcium carbonate analysis................................................................................................. 39 
6.2.6 Limestone analysis .............................................................................................................. 39 
6.2.7 Cement analysis .................................................................................................................. 39 
6.2.8 Gypsum and desulfurization products (from power plants) analysis................................... 39 
6.2.9 Low Carbon Analysis........................................................................................................... 39 
6Maintenance......................................................................................................................................... 43 
1 General information ......................................................................................................................... 43 
1.1 Resistance furnace operation...................................................................................................... 43 
1.2 Induction furnace operation ......................................................................................................... 43 
2 Reagent tubes –removing and installing ........................................................................................ 44 
3 Reagent tubes filling ........................................................................................................................ 47 

 
 
 

 
3.1 Chemicals.................................................................................................................................... 47 
3.2 Reagent tube filling-Induction furnace......................................................................................... 49 
3.3 Reagent tube filling-Resistance furnace...................................................................................... 52 
3.4 Oxygen purification furnace quartz tube filling (optional) ............................................................ 54 
3.5 Halogen trap filling (optional)....................................................................................................... 55 
4 Paper filter changing........................................................................................................................ 57 
5 Dust filter cartridge replacing........................................................................................................... 57 
6 O-rings replacement........................................................................................................................ 58 
6.1 Replacing the o-rings 11 and 12 for combustion tube:................................................................ 60 
6.2 Replacing the o-ring 13 for lower furnace lock ............................................................................ 60 
6.3 Replacing the o-rings for furnace seal......................................................................................... 61 
7 Furnace cleaning brush - replacing ................................................................................................. 64 
8 Dust trap cleaning............................................................................................................................ 65 
8.1 Dust trap cleaning-Induction furnace........................................................................................... 65 
8.2 Dust trap cleaning-Resistance furnace........................................................................................ 68 
9 Combustion tube replacement......................................................................................................... 69 
9.1 Induction furnace ......................................................................................................................... 70 
9.2 Resistance furnace...................................................................................................................... 72 
10 Generator tube replacing................................................................................................................. 74 
11 Combustion coil replacing................................................................................................................ 74 
12 Pedestal removing........................................................................................................................... 74 
13 Heating elements replacing............................................................................................................. 75 
14 Gas leaks checking.......................................................................................................................... 76 
14.1 Leaks in the furnace inlet system ............................................................................................ 77 
14.2 Leaks in the furnace ................................................................................................................ 77 
14.3 Leaks in the furnace outlet system.......................................................................................... 77 
7Function description........................................................................................................................... 78 
1 System overview.............................................................................................................................. 78 
2 Measuring principle.......................................................................................................................... 78 
3 Gas flow system .............................................................................................................................. 79 
4 Infrared cell...................................................................................................................................... 81 
5 Furnace............................................................................................................................................ 82 
5.1 Induction furnace ......................................................................................................................... 82 
5.2 Resistance furnace...................................................................................................................... 83 
8Miscellaneous...................................................................................................................................... 85 
1 Ordering numbers............................................................................................................................ 85 
1.1 Front side..................................................................................................................................... 85 
1.2 Left hand side .............................................................................................................................. 86 
1.3 Right side..................................................................................................................................... 87 
1.4 Pneumatics.................................................................................................................................. 88 
1.5 Oscillating circuit.......................................................................................................................... 89 
1.6 Furnace........................................................................................................................................ 91 
1.7 Furnace cleaning mechanism...................................................................................................... 93 
1.8 Gas purification furnace............................................................................................................... 94 
1.9 Front side and rear side............................................................................................................... 95 
1.10 Restistance furnace details...................................................................................................... 95 
1.11 Furnace tube cleaning ............................................................................................................. 97 
1.12 Tic-module............................................................................................................................... 98 
2 Packing.......................................................................................................................................... 100 
3 Pre-installation guide ..................................................................................................................... 103 
9Approved methodologies to which Eltra instruments conform................................................... 105 
1 Inorganic materials (Metals) .......................................................................................................... 105 
2 Organic materials (Oil, Coal, foodstuffs)........................................................................................ 106 
Disposal.............................................................................................................................................. 106 
Index ................................................................................................................................................... 108 

Contact information

1 Contact information

Please contact your local representative in the event of problems. You can find the complete

list of dealers at www.eltra.com.

Of course you can also contact ELTRA-Germany directly:

ELTRA GmbH

Retsch Allee 1-5

42781 Haan

Germany

Web: www.eltra.com

Email: service@eltra.com

2 Notes on the Manual

This Operating Manual provides technical instructions for the safe operation of the device and

contains all necessary information about the topics given in the table of contents. This technical

documentation is meant to be a tutorial and a reference. The individual chapters are self-

contained.

Knowledge of the relevant chapters (for the respective target groups defined according to

areas) is a prerequisite for the safe and correct use of the device.

This Operating Manual contains no repair instructions. In the event of any faults or necessary

repair work, please contact your supplier or Eltra GmbH directly.

Amendments

Subject to technical changes.

The forwarding or duplication of this documentation and the recycling and passing on of its

content are only permitted with the explicit consent of Eltra GmbH.

Any infringements of this constitute an obligation to pay damages.

Notes on the Manual

2.1 Explanations of the Safety Instructions

In this Operating Manual we give you the following safety warnings

Mortal injury may result from not following these safety warnings. We give you the following

warnings and corresponding content.

DANGER

Type of danger / personal injury

Source of danger

–Possible consequences if the dangers are not observed.

•Instructions on how the dangers are to be avoided.

We also use the following signal word box in the text or in the instructions on action to be taken:

DANGER

Serious injury may result from not following these safety warnings. We give you the following

warnings and corresponding content.

WARNING

Type of danger / personal injury

Source of danger

–Possible consequences if the dangers are not observed.

•Instructions on how the dangers are to be avoided.

We also use the following signal word box in the text or in the instructions on action to be taken:

WARNING

Moderate or mild injury may result from not following these safety warnings. We give you the

following warnings and corresponding content.

CAUTION

Type of danger / personal injury

Source of danger

–Possible consequences if the dangers are not observed.

•Instructions on how the dangers are to be avoided.

We also use the following signal word box in the text or in the instructions on action to be taken:

CAUTION

In the event of possible property damage we inform you with the word “Instructions” and the

corresponding content.

NOTICE

Nature of the property damage

Source of property damage

–Possible consequences if the instructions are not observed.

Notes on the Manual

•Instructions on how the dangers are to be avoided.

We also use the following signal word in the text or in the instructions on action to be taken:

NOTICE

Notes on the Manual

2.2 General Safety Instructions

CAUTION

C1.0002

Read the manual

Non-observance of the operating instructions

The non-observance of this manual can result in personal injuries.

•Read the manual before using the device.

•The adjacent symbol indicates the necessity of knowing the

contents of this manual.

Target group:

All activities required for correct use are described in this Operating Manual. Any activities that

go beyond this may only be performed by authorised electricians who have received in-depth

training for this analyzer.

As the operating company, you must ensure that the following applies to the persons working

on the analyzer;

•Operating personnel have been made aware of and have understood all safety

regulations;

•Operating personnel are familiar when starting work with all handling instructions and

regulations that apply to the relevant target group for them;

•Operating personnel have access at all times to the technical documentation of this

analyzer;

•New personnel are familiarised with the safe and intended use of the analyzer before

starting work on it by means of a verbal introduction by a competent person and using

this technical documentation.

Incorrect operation can result in injury and damage to property. You are responsible for your

own safety and for that of your employees.

Ensure that no unauthorised persons have access to the analyzer.

CAUTION

C2.0089

Changes to the machine

Changes to the machine may lead to personal injury.

•Do not make any change to the analyzer and use spare parts and

accessories that have been approved by Eltra exclusively.

NOTICE

N1.0074

Changes to the machine

Improper modifications

The conformity declared by EltraEltra GmbH with the European Directives

will lose its validity.

Any warranty claims will be terminated.

•Do not make any modification to the machine.

•Use spare parts and accessories that have been approved by EltraEltra

GmbH exclusively.

Notes on the Manual

2.3 Explanation of signs and symbols

Number

Symbol

Reference

Meaning

Danger, high voltage, electric shock

IEC 60417-5041

Caution, hot surface

ISO 7000-0434B

General hazards –see documentation

BGV A8 W27

Risk of crushing

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