Hach BioTector B3500 Kurzanleitung

DOC023.53.90740

BioTector B3500 Online TOC Analyzer

BASIC USER MANUAL

6/2018, Edition 1

Page 3

Table of Contents

SECTION 1 SAFETY PRECAUTIONS ......................................................................... 4

1.1 INFORMATION AND SAFETY SIGNS USED IN THE MANUAL.......................................................... 4

1.2 PRECAUTIONARY LABELS ATTACHED TO THE INSTRUMENT....................................................... 5

1.3 CERTIFICATION MARKS ATTACHED TO THE INSTRUMENT .......................................................... 6

1.4 POTENTIAL SYSTEM SAFETY HAZARDS..................................................................................... 7

1.4.1 Ozone and Toxicity..........................................................................................................................8

1.4.2 First Aid Treatment ..........................................................................................................................8

1.5 GENERAL SAFETY PRECAUTIONS ............................................................................................. 9

1.5 PRÉCAUTIONS GÉNÉRALES DE SÉCURITÉ.................................................................................. 9

1.5.1 Electrical and Burn Precautions ....................................................................................................10

1.5.1 Précautions relatives à l’électricité et aux brûlures.......................................................................10

1.5.2 Carrier Gas and Exhaust Gas Precautions...................................................................................11

1.5.2 Précautions relatives au gaz porteur et d'échappement ..............................................................11

1.5.3 Chemical Precautions ...................................................................................................................12

1.5.3 Précautions chimiques ..................................................................................................................12

1.5.4 Sample Stream Precautions .........................................................................................................13

1.5.4 Précautions relatives aux échantillons..........................................................................................14

SECTION 2 OPERATOR’S MANUAL ........................................................................ 15

2.1 SOFTWARE SCREENS AND SOFTWARE MENU DIAGRAM................................................................ 15

2.1.1 Startup State..................................................................................................................................17

2.1.2 System Status Messages..............................................................................................................17

2.1.3 Analysis Data Screen ....................................................................................................................18

2.1.4 Analysis Graph Screen..................................................................................................................19

2.1.5 Reagent Status Screen .................................................................................................................19

2.1.6 Select Level Menu .........................................................................................................................20

2.1.7 Enter Password Menu ...................................................................................................................20

2.2 OPERATION MENU .................................................................................................................. 21

2.2.1 Start Stop.......................................................................................................................................21

2.2.2 Reagents Setup.............................................................................................................................23

2.2.2.1 Install New Reagents ..........................................................................................................................23

2.2.2.2 Purge Reagents & Zero ......................................................................................................................24

2.2.3 System Range Data Screen..........................................................................................................24

2.2.4 Manual Program Menu..................................................................................................................25

2.2.5 Reaction Archive Screen...............................................................................................................26

2.2.6 Fault Archive Menu........................................................................................................................26

2.2.7 Time & Date Menu.........................................................................................................................27

2.2.8 Contact Information .......................................................................................................................27

2.2.9 LCD Adjust.....................................................................................................................................27

2.3 CALIBRATION MENU................................................................................................................ 28

2.3.1 Zero Calibration .............................................................................................................................28

2.3.2 Span Calibration ............................................................................................................................30

Page 4

Section 1 Safety Precautions

Please read this manual before unpacking, setting up, or operating the BioTector.

BioTector should only be used by qualified trained staff and for the purpose it is intended for. Do not use or

install this equipment in any way other than the methods specified in this manual. The procedures and

methods described in this manual are based on assuming the user have basic, fundamental background on

electronics, chemistry and analyzer equipment.

If the instructions in this manual are not followed, the operation and protection provided by the

equipment may be impaired.

1.1 Information and Safety Signs used in the Manual

When any supplementary information is required and if any hazards exist, the necessary information and

safety signs (Information, Caution, Warning and Danger) will be displayed for the corresponding section or

procedure in this manual.

Used to indic

ate supplementary information, to call attention to

recommendations, to simplify the operation and to guarantee the correct use

of the equipment.

Used when there is a danger of minor damage to the system if the user does

not follow precautions.

Used

when there is a danger of minor injury or serious damage to the

system if the user does do not follow the precautions.

Used when failure to observe a safety precaution may result in serious injury

or death.

Caution

WARNING

DANGER

Page 5

1.2 Precautionary Labels Attached to the Instrument

The labels and tags attached to the instrument are summarized below. Please read all labels and tags

attached to the instrument. If not observed, personal injury or damage to the instrument could occur.

This symbol, when displayed on the instrument, indicates that the user

must gather the necessary operation and/or safety information given in the

instruction manual.

This symbol, when attached on an enclosure, indicates an existing risk of

electrical shock and/or electrocution. Only qualified personnel should open

such enclosures and work with hazardous voltages.

This symbol, when displayed on a component, identifies that the

component surface can be hot. When it is necessary to work with this

component, it should be handled with care.

This symbol, when noted on a product, illustrates the risk of chemical harm

due to its corrosive, acidic, caustic or solvent nature. Only qualified and

trained staff should handle such chemicals.

This symbol, when noted on an analyzer, illustrates the risk of the presence

of toxic ozone gas produced in the analyzer. Only qualified and trained staff

should work with this analyzer.

This symbol, when displayed on the instrument, indicates the presence of

devices sensitive to Electro-Static Discharge (ESD). Prior to any work with

such components, the individual should be grounded via an earth strap to

prevent any possible damage.

This symbol, when displayed on the product, indicates that protective eye

wear must be used during the maintenance or service of the equipment.

This symbol, when used on the product, identifies the location of the

protective earth (ground) connection.

Page 6

Electrical equipment marked with this symbol may not be disposed of in

European domestic or public disposal systems. Return old or end-of-life

equipment to the manufacturer for disposal at no charge to the user.

1.3 Certification Marks Attached to the Instrument

The standard certification marks attached to the instrument and their meanings are summarized below.

Additional certification marks if required for specific markets are at the back of this manual.

This mark, which stands for European Conformity "Conformité

Européene", indicates that “The instrument complies with the

European product directives, health, safety and

environmental protection legislations”.

Conforms to

ANSI/UL Std. 61010-1

Certified to

CAN/CSA Std. 61010-1

If these marks are displayed on the instrument, they indicate

that “This product has been tested to Safety Requirements

of Electrical Equipment for Measurements

, Control and

Laboratory use; Part 1: General Requirements of ANSI/UL

61010-1 and CAN/CSA-C22.2 No 61010-1”. Intertek ETL listed

mark, which stands for Electrical Testing Laboratories, identifies

that the product has been tested by Intertek, found in

compliance with accepted national standards, and it meets the

minimal requirements required for sale or distribution.

Page 7

1.4 Potential System Safety Hazards

The potential safety hazards, which are associated with a running BioTector system, are as follows:

•Electrical hazards

•Potentially hazardous chemicals

•Oxygen gas and components generating Ozone gas

Please read the instructions in this manual carefully before installing or starting the BioTector.

The manufacturer cannot accept liability for damages due to non-observance of this manual. Use of spare

parts not supplied by the manufacturer will invalidate the warranty. If the equipment is used in a manner not

specified by the manufacturer, the protection provided by the equipment may be impaired. The manufacturer

shall not be liable for omissions or errors contained herein or for incidental or consequential damages in

connection with the furnishing, performance, or use of this material.

The information contained in this manual is subject to change without notice.

The information contained herein is protected by copyright. Reproduction, adaptation, or translation of any

part of this manual without prior written permission is prohibited, except as allowed under the copyright laws.

Product names mentioned herein are for identification purposes only and may be trademarks or registered

trademarks of their respective companies.

Where manuals are translated into several languages, the source language text is considered as the original.

Maintenance and operation should not be carried out unless personnel have been fully

trained in the operation of the BioTector.

Prior to working on the inside of the analyzer, the technician should be grounded via an

earth strap.

Caution

Page 8

1.4.1 Ozone and Toxicity

Ozone is found in gaseous form as a natural ingredient of the earth's atmosphere. Some of the chemical and

physical properties of ozone are as follows:

Terms

Properties of Ozone (O3)

Molecule Weight

47.9982 g/g-mol

Boiling Point

-119 ±0.3 °C

Melting Point

-192.7 ±0.2 °C

Exposure to even low concentrations of ozone can be damaging to delicate nasal, bronchial and pulmonary

membrane. Symptoms of acute ozone toxification appear at a concentration of about 1 ppm by volume. The

type and severity of symptoms depend on the concentration and duration of exposure. In mild cases and in

the early phases of severe cases, symptoms will include one or more of the following:

•Irritation or burning of the eyes, nose or throat

•Lassitude

•Frontal headache

•Sensation of sub-sternal pressure

•Constriction or oppression

•Acid taste in mouth

•Anorexia

In more severe cases, the symptoms may include dyspnoea, cough, choking sensation, tachycardia, vertigo,

lowering of blood pressure, severe cramping, chest pain, and generalized body pain. Pulmonary oedema may

develop with delayed onset, usually one or more hours after exposure.

Following severe acute ozone toxification, recovery is slow. In the few severe human cases reported, 10 -14

days of hospitalization were required. In these cases, minimal residual symptoms were present for as long as

9 months, but all cases eventually recovered completely.

The 1983 ACGIH has recommended a Threshold Limit Value (TLV) of 0.1 ppm (0.2 mg/m3) for ozone. The

safe level for short human exposure to concentrations of ozone in excess of 0.1 ppm (Threshold Limit Value)

is not known with certainty. The atmospheric concentration immediately hazardous to life is likewise not

known, but inhalation of 50 ppm for 30 minutes would probably be fatal. The odor threshold of ozone for a

normal person is 0.01 - 0.02 ppm by volume in air.

1.4.2 First Aid Treatment

Move the victim to an uncontaminated atmosphere. Control restlessness and pain by the administration of

sedatives and anodynes orally. Severe cases may require subcutaneous injections of small doses of

meperidine hydrochloride (Demerol) for relief of pain. Give oxygen inhalation by facemask when the acute

symptoms have subsided. Severe cases require hospitalization since deferred pulmonary oedema may

develop.

Page 9

1.5 General Safety Precautions

Please pay attention to all caution, warning and danger statements at all times. Non-observance of the safety

instructions can result in serious personal injury, death or damage to the equipment. Therefore observe the

following:

Only engineers trained by the manufacturer should carry out maintenance on the BioTector.

The power supplies contain capacitors that are charged to hazardous voltages. After disconnecting

the main power, allow a minimum of one minute for discharge before opening the control section.

Never wash or spray the system with water. Do not allow water to enter the interior.

Protect the system from one-sided heat radiation, direct sunlight and vibration. System must be

installed in a dry, dust-free room. Special precautions are required in environments with corrosive

gases, vapors or explosion risk.

Please do not place anything on top of the system.

1.5 Précautions générales de sécurité

Prière d’être toujours attentif à toutes les notices de prudence, d’avertissement ou de danger. Le non respect

des instructions de sécurité peut engendrer la blessure grave d’individus, leur décès ou la dégradation du

matériel. Pour ces raisons, prière d’observer les règles suivantes:

Seuls les ingénieurs formés par le fabricant doivent réaliser des travaux de maintenance sur le

BioTector.

L’alimentation électrique contient des condensateurs qui sont chargés à des tensions dangereuses.

Après avoir débranché l’alimentation électrique, attendre au moins une minute pour permettre la

décharge avant d'ouvrir le boîtier de commande.

Ne jamais laver ou arroser l’appareil avec de l’eau. Ne pas laisser de l’eau pénétrer à l’intérieur.

Protéger l’appareil des radiations de chaleur sur un seul côté, des rayons directs du soleil et des

vibrations. L’appareil doit être installé dans une pièce sèche et sans poussière. Il est nécessaire de

prendre des précautions particulières dans les environnements contenant des vapeurs ou gaz

corrosifs ou ceux à risque d’explosion.

Prière de ne rien poser sur le dessus de l'appareil.

Page 10

1.5.1 Electrical and Burn Precautions

During system installation, maintenance or servicing:

•Isolate the system power lines before starting any work in the electronic enclosure.

•All electrical work should be carried out by qualified electrical personnel only.

•Comply with all local and national regulations when working with electrical connections.

•Make sure the system is properly earthed (grounded) before switching on.

•It is required to connect the mains through an external isolator (2-pole disconnection switch), and if

possible connect the mains through an earth leakage circuit breaker.

•When working with hot surfaces, use protective gloves and handle the components with care.

1.5.1 Précautions relatives à l’électricité et aux brûlures

À l’installation de l’appareil, sa maintenance ou son entretien:

•Isoler les fils électriques de l’appareil avant de commencer tout travail dans le boîtier électronique.

•Seul le personnel électricien qualifié est habilité à effectuer tous travaux d’électricité.

•Se conformer aux règlementations locales et nationales pour tout travail sur un branchement

électrique.

•Avant de l’allumer, veiller à la bonne mise à la terre de l’appareil.

•Le branchement sur le courant secteur doit obligatoirement se faire par l'intermédiaire d'un

interrupteur sectionneur externe (interrupteur bipolaire), et prévoyez si possible un disjoncteur

différentiel.

•Utiliser des gants de protection pour les travaux sur les surfaces très chaudes et prendre soin en

manipulant les composants.

BioTector contains electrical components operating under high voltages.

Contact may result in electric shock and severe or fatal injury.

BioTector contient des composants électriques qui fonctionnent à des tensions

élevées. Un contact peut engendrer un choc électrique et des blessures graves

ou mortelles.

DANGER

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