HP DESKJET 1050 Produkthandbuch

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Find the Keysight / Agilent 79853C at our website: Click HERE

HP 1050 Series Variable Wavelength Detector

Installation and

Maintenance Guide

ABCDE

HP Part No. 79853-90009

Printed in FRG

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cÕCopyright Hewlett-

Packard Company 1992 Warranty Safety

Reproduction, adaption, or

translation without prior

written permission is pro-

hibited, except as allowed

under the copyright laws .

HP Part No. 79853-90009

Second edition, October 1992

Printed in FRG

For details of warranty , see

\Warranty Statement" in Chapter 5 For details of safety , see \Safety

Information " in Chapter 5

The apparatus is marked with this

symbol when the user should refer

to the instruction manual in order

to protect the apparatus against

damage .

Indicates dangerous voltages .

Indicates a protected ground

terminal.

Hewlett-P ackard GmbH

Hewlett-P ackard-Strasse 8

W-7517 Waldbronn 2

Federal Republic of Germany

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Using This

Handbook Use this handbook when you want to install ,

troubleshoot , or maintain your HP 1050 Series Variable

Wavelength Detector .

Chapter 1 describes how to install your detector and

prepare it for operation. Chapter 2 contains installation

instructions and information for accessories and

upgrades . Go to Chapter 3 when you get a not-ready

condition or error message, or other error symptom. Here

you will be directed to Chapter 4, when it is necessary

to replace a part. Chapter 5 gives supplementary

information about your detector .

What Other

Handbooks Are

Available?

Your detector comes complete with 2 further handbooks .

The User's Guide describes each of your detector's

functions .

Getting it all Together is intended for chromatographic

systems comprising only HP 1050 Series modules and

shows you how to connect diÀerent modules to make a

complete system.

iii

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Contents

1. Installing Your Detector

Choosing a Suitable Place . . . . . . . . . 1-1

Dimensions . . . . . . . . . . . . . . . 1-1

Weight . . . . . . . . . . . . . . . . . 1-1

Environment . . . . . . . . . . . . . . 1-1

Line Power . . . . . . . . . . . . . . . 1-1

Line Frequency . . . . . . . . . . . . . 1-2

Power Consumption . . . . . . . . . . . 1-2

Do I Need Anything Else? . . . . . . . . 1-2

Unpacking Your Detector . . . . . . . . . 1-2

Accessories . . . . . . . . . . . . . . . . 1-3

Setting Up Your Detector . . . . . . . . . 1-6

Removing the Locking Screws . . . . . . 1-7

Waste Drain . . . . . . . . . . . . . . 1-9

Solvent Inlet and Outlet . . . . . . . . . 1-11

Analog Output . . . . . . . . . . . . . 1-11

Remote Control . . . . . . . . . . . . . 1-12

Line Voltage . . . . . . . . . . . . . . 1-14

Fuses ................. 1-14

Power Cord . . . . . . . . . . . . . . . 1-16

Ground Connector . . . . . . . . . . . 1-17

Installing HP-IB Board . . . . . . . . . . 1-17

Checking Out Your Detector . . . . . . . . 1-19

Preparing the Detector . . . . . . . . . 1-20

Preparing the Pump . . . . . . . . . . . 1-20

Preparing the Recording Device . . . . . 1-20

Starting a Run . . . . . . . . . . . . . . 1-21

Contents-1

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2. Installing Accessories

3. Troubleshooting Your Detector

Troubleshooting During Start-Up . . . . . . 3-2

Detector Down . . . . . . . . . . . . . 3-2

ROMTEST FIM failed at U4 . . . . . . . 3-2

RAMTEST CMP failed at XXXXH . . . . . 3-2

Error Messages . . . . . . . . . . . . . . 3-3

Not Ready Conditions . . . . . . . . . . . 3-3

Troubleshooting During Operation . . . . . 3-3

Troubleshooting the Chromatogram . . . . 3-5

Retention Times Not Reproducible . . . . 3-5

Areas Not Reproducible . . . . . . . . . 3-6

Baseline Noise . . . . . . . . . . . . . 3-7

Baseline Wander . . . . . . . . . . . . 3-7

Baseline Drift . . . . . . . . . . . . . . 3-7

Baseline OÀset . . . . . . . . . . . . . 3-7

Tailing Peaks . . . . . . . . . . . . . . 3-8

Heading Peaks . . . . . . . . . . . . . 3-8

Double Peaks of One Substance . . . . . 3-8

Excessive Baseline Disturbance After

Injection . . . . . . . . . . . . . . 3-8

Air Bubbles in Flow Cell . . . . . . . . . 3-8

Removing Air Bubbles . . . . . . . . . . 3-9

4. Maintaining Your Detector

Changing Deuterium Lamp . . . . . . . . 4-2

Stage 1: Removing Lamp . . . . . . . . 4-2

Stage 2: Inserting New Lamp . . . . . . 4-4

Stage 3: Calibrating Zero-Order Light . . 4-4

Calibrating Wavelength Accuracy . . . . 4-5

Removing the Flow Cell . . . . . . . . . . 4-5

Cleaning Standard Flow Cell . . . . . . . . 4-6

Removing Standard Flow Cell . . . . . . 4-6

Disassembling Standard Flow Cell . . . . 4-6

Cleaning Parts of Standard Flow Cell . . . 4-7

Reassembling Standard Flow Cell . . . . 4-7

Cleaning Semi-Micro Flow Cell . . . . . . . 4-8

Removing Semi-Micro Flow Cell . . . . . 4-8

Disassembling Semi-Micro Flow Cell . . . 4-8

Cleaning Parts of Semi-Micro Flow Cell . . 4-9

Contents-2

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Reassembling Semi-Micro Flow Cell . . . 4-9

Cleaning Preparative Flow Cell . . . . . . 4-10

Removing Preparative Flow Cell . . . . . 4-10

Disassembling Preparative Flow Cell . . . 4-10

Cleaning Parts of Preparative Flow Cell . 4-11

Reassembling Preparative Flow Cell . . . 4-11

Cleaning High-Pressure Flow Cell . . . . . 4-12

Removing High-Pressure Flow Cell . . . . 4-12

Disassembling High-Pressure Flow Cell . . 4-12

Cleaning Parts of High-Pressure Flow Cell 4-13

Reassembling High-Pressure Flow Cell . . 4-13

5. Supplementary Information

Warranty Statement . . . . . . . . . . . . 5-1

All Analytical Products . . . . . . . . . 5-1

Limitation of Warranty . . . . . . . . . 5-2

Limitation of Remedies and Liability . . . 5-3

Responsibilities of the Customer . . . . . 5-3

Responsibilities of Hewlett-P ackard . . . 5-4

Safety Information . . . . . . . . . . . . 5-5

General . . . . . . . . . . . . . . . . 5-5

Operation . . . . . . . . . . . . . . . 5-5

Safety Symbols . . . . . . . . . . . . . 5-6

Solvent Information . . . . . . . . . . . . 5-9

Flow Cell . . . . . . . . . . . . . . . . 5-9

Solvents . . . . . . . . . . . . . . . . 5-9

Use of Solvents . . . . . . . . . . . . . . 5-10

Important . . . . . . . . . . . . . . . 5-11

Acids.................. 5-11

Bases . . . . . . . . . . . . . . . . . 5-11

Salts.................. 5-11

Organic Solvents . . . . . . . . . . . . 5-12

BuÀer Solutions . . . . . . . . . . . . 5-12

Degassing Solvents . . . . . . . . . . . 5-15

Radio Interference . . . . . . . . . . . . 5-16

Manufacturer's Declaration . . . . . . . 5-16

Hersteller- bescheinigung . . . . . . . . 5-16

Sound Emission . . . . . . . . . . . . . . 5-17

Manufacturer's Declaration . . . . . . . 5-17

Hersteller- bescheinigung . . . . . . . . 5-17

Declaration of Conformity . . . . . . . . . 5-18

Contents-3

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SpeciÃcations . . . . . . . . . . . . . . . 5-19

Detection Type . . . . . . . . . . . . . 5-19

Noise.................. 5-19

Drift .................. 5-19

Wavelength Range . . . . . . . . . . . 5-19

Wavelength Accuracy . . . . . . . . . . 5-19

Wavelength Reproducibility . . . . . . . 5-19

Bandwidth . . . . . . . . . . . . . . . 5-19

Linear Absorbance Range . . . . . . . . 5-19

Response Time . . . . . . . . . . . . . 5-19

Spectra................. 5-19

Light Source . . . . . . . . . . . . . . 5-20

Flow Cells . . . . . . . . . . . . . . . 5-20

Control ................. 5-20

Parameters . . . . . . . . . . . . . . . 5-20

Analog Output . . . . . . . . . . . . . 5-20

Communications . . . . . . . . . . . . 5-20

Safety Aids . . . . . . . . . . . . . . . 5-20

Environment . . . . . . . . . . . . . . 5-20

Dimensions . . . . . . . . . . . . . . . 5-20

Printing History . . . . . . . . . . . . . . 5-21

Your Comments Are Welcome . . . . . . . 5-23

Your Comments Are Welcome . . . . . . . 5-25

Index

Contents-4

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Figures

1-1. Position of Locking Screws and Spacers . 1-7

1-2. Holes on Rear Panel for Locking Screws

and Spacers . . . . . . . . . . . . . 1-8

1-3. Front of Detector . . . . . . . . . . . . 1-8

1-4. Rear of Detector . . . . . . . . . . . . 1-9

1-5. Position of Waste Drain and Lever . . . . 1-9

1-6. APG REMOTE Connector . . . . . . . . 1-13

3-1. Baseline Shapes . . . . . . . . . . . . . 3-9

4-1. Removing Detector Top Cover . . . . . . 4-3

4-2. Position of Flow Cell Cassette Screws . . 4-5

4-3. Standard Flow Cell . . . . . . . . . . . 4-6

4-4. Semi-Micro Flow Cell . . . . . . . . . . 4-8

4-5. Preparative Flow Cell . . . . . . . . . . 4-10

4-6. High-Pressure Flow Cell . . . . . . . . . 4-12

Tables

1-1. Packing List . . . . . . . . . . . . . . 1-2

1-2. Accessories . . . . . . . . . . . . . . . 1-3

1-3. Signal Cables . . . . . . . . . . . . . . 1-11

1-4. APG Remote Control Cables . . . . . . . 1-12

1-5. APG Remote Control Connector Functions 1-13

1-6. Fuses . . . . . . . . . . . . . . . . . 1-15

1-7. Integrator Scaling Factors . . . . . . . . 1-21

5-1. Warranty Services . . . . . . . . . . . . 5-4

Contents-5

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