Seres OL TOC Evolution VUV Bedienungsanleitung

TOC Evolution VUV
Operator’s Manual
TOC Evolution VUV
SOL-96.120.031 / 060223

© 2023, Seres OL SAS, France, all rights reserved.
The information contained in this document is subject to change without notice.
Customer Support
Seres OL and its representatives maintain a fully trained staff of technical specialists
around the world. For any technical question, contact your nearest Seres OL representa-
tive, or the manufacturer:
Seres OL SAS
ZA de la Sipière
219, Avenue de Provence
FR-13730 Saint-Victoret
France
Internet: www.seres-ol.com
E-mail: [email protected]
Document Status
Title: TOC Evolution VUV Operator’s Manual
ID: SOL-96.120.031
Revision Issue
00 February 2023 First edition

SOL-96.120.031 / 060223
TOC Evolution VUV
1
Table of Contents
1. Safety Instructions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3
1.1. Warning Notices . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4
1.2. General Safety Regulations . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6
1.3. Handling Precautions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7
1.4. International Symbols Used . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8
2. Product Description . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9
2.1. Instrument Specifications . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11
2.2. Instrument Overview . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 15
3. Installation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 17
3.1. Before Installation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 17
3.2. Mounting the Wall Cabinet . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 17
3.3. Hydraulic Connections . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 17
3.4. Electrical Connections. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 18
3.4.1 Connections on I/O Boards . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 19
3.4.2 Cable Thicknesses. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 23
3.4.3 Cable Cross-Section . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 23
3.4.4 AC Power. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 24
3.4.5 Jbus via RS485 (Option) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 25
3.4.6 Jbus via TCP/IP (Option) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 26
4. Startup . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 27
4.1. Installing the Reagent Bottles . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 27
4.2. Filling the Liquid Seal . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 28
4.3. Starting Sample Flow . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 29
4.4. Preliminary Start-Up . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 31
4.5. Run-in Period . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 33
4.6. Manual Measurement . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 33
4.7. Programming. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 33
4.8. Jbus Table. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 33
5. Operation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 34
5.1. Access Levels . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 34
5.2. User Interface . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 35
6. Maintenance. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 36
6.1. Maintenance Schedule . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 36
6.2. Stop of Operation for Maintenance . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 37
6.3. Replacing Reagents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 39
6.4. Replacing Peristaltic Pump Tubes . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 40
6.4.1 Reagent Pumps . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 40

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6.4.2 Sample Pump . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 42
6.5. Replacing Soda Lime and Activated Charcoal. . . . . . . . . . . . . . . . . . . . . . . . . . 43
6.6. Replacing Silica Gel . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 45
6.7. Replacing UV Lamp . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 46
6.8. Manual Measurement and Calibration . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 47
6.8.1 Manual Measurement . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 48
6.8.2 Zero Calibration . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 48
6.8.3 Standard Calibration . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 49
6.9. Longer Stop of Operation. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 50
7. Configuration of the Analyzer. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 51
8. Troubleshooting. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 55
8.1. What To Do If... . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 55
8.2. Saving Diagnostic Data to USB Stick. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 59
8.3. Replacing Parts . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 60
8.3.1 NDIR . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 60
8.3.2 Glassware. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 61
8.3.3 Reagent Pump . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 68
9. Fluidic Diagrams . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 70
10. Notes . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 76

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TOC Evolution VUV
Safety Instructions
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Operator’s Manual
This document describes the main steps for instrument setup,
operation and maintenance.
1. Safety Instructions
General The instructions included in this chapter explain the potential risks
associated with instrument operation and provide important safety
practices designed to minimize these risks.
If you carefully follow the information contained in this chapter, you
can protect yourself from hazards and create a safer work environ-
ment.
More safety instructions are given throughout this manual, at the
respective locations where observation is most important. Strictly
follow all safety instructions in this publication.
Target
audience
Operator: Qualified person who uses the equipment for its intended
purpose.
Instrument operation requires thorough knowledge of applications,
instrument functions and software as well as all applicable safety
rules and regulations.
OM location Keep the Operator’s Manual in proximity of the instrument.
Qualification,
training
To be qualified for instrument installation and operation, you must:
read and understand the instructions in this manual as well as
the Material Safety Data Sheets and
know the relevant safety rules and regulations.

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Safety Instructions
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1.1. Warning Notices
The signal words and symbols used for safety-related notices have
the following meaning:
DANGER
Your life or physical wellbeing are in serious danger if such
warnings are ignored.
Follow the prevention instructions carefully.
WARNING
Severe injuries or damage to the equipment can occur if such
warnings are ignored.
Follow the prevention instructions carefully.
CAUTION
Damage to the equipment, minor injury, malfunctions or incorrect
process values can be the consequence if such warnings are
ignored.
Follow the prevention instructions carefully.
Mandatory
signs
The mandatory signs in this manual have the following meaning:
Safety goggles
Safety gloves

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Safety Instructions
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Warning signs The warning signs in this manual have the following meaning:
Electrical shock hazard
Corrosive
Harmful to health
Flammable
Hot surface
UV radiation
General warning

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Safety Instructions
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1.2. General Safety Regulations
Spare parts
and
disposables
Use only official Seres OL spare parts and consumables. If other
parts are used during the normal warranty period, the manufacturer’s
warranty is voided.
Modifications Modifications and instrument upgrades shall only be carried out by
an authorized service technician. Seres OL will not accept responsi-
bility for any claim resulting from unauthorized modification or alter-
ation.
Local
regulations
All wiring and connections (electrical, hydraulic) may only be carried
out by qualified personnel and in accordance with the local regula-
tions of the respective country.
WARNING
Electrical shock hazard
If proper operation is no longer possible, the instrument must
be disconnected from all power lines, and measures must be
taken to prevent inadvertent operation.
To prevent from electrical shock, always make sure that the
protective earth wire is connected.
Service shall be performed by authorized personnel only.
Whenever electronic service is required, disconnect the
instrument from power.
WARNING
Chemical exposure hazard
When handling chemicals or performing maintenance work
on hydraulic parts of the analyzer, wear suitable protective
equipment.
Read the Material Safety Datasheets (MSDS) of the chemicals
carefully.

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Safety Instructions
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WARNING
Do not use this instrument in presence of flammable liquids or
vapors as this may pose a safety hazard.
WARNING
If it is necessary to carry out maintenance work with the UV lamp
switched on, wear UV protective goggles.
1.3. Handling Precautions
Position the box correctly (up/down). Carefully unpack the analyzer
and check it for visible damage. If the analyzer shows any visible
damage, do not connect it to power and contact customer service
immediately.

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Safety Instructions
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1.4. International Symbols Used
The symbols found on the instrument have the following meaning:
Electrical fuse
Ground
Equipotentiality
Alternating current
Hot surface
General attention
Electrical hazard
UV radiation
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