Thermo Scientific Orion Star Bedienungsanleitung

Thermo Scientiﬁc

Orion DUAL STAR™

pH/ISE Meter User Guide

ROSS and the COIL trade dress are trademarks of Thermo Fisher Scientific Inc. U.S. patent 6,793,787.

AQUAfast, Cahn, ionplus, KNIpHE, No Cal, ORION, perpHect, PerpHecT, PerpHecTion, pHISA, pHuture, Pure

Water, Sage, Sensing the Future, SensorLink, ROSS, ROSS Ultra, Sure-Flow, Titrator PLUS and TURBO2 are

registered trademarks of Thermo Fisher.

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DISPENSER, Auto-ID, AUTO-LOG, AUTO-READ, AUTO-STIR, Auto-Test, BOD AutoEZ, Cable-Free, CERTI-CAL,

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Easy/Extra Value, FAST QC, GAP, GLPcal, GLPcheck, GLPdoc, ISEasy, KAP, LabConnect, LogR, Low

Maintenance Triode, Minimum Stir Requirement, MSR, NISS, One-Touch, One-Touch Calibration, One-Touch

Measurement, Optimum Results, Orion Star, Pentrode, pHuture MMS, pHuture Pentrode, pHuture

Quatrode, pHuture Triode, Quatrode, QuiKcheK, rf link, ROSS Resolution, SAOB, SMART AVERAGING, Smart

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TRIUMpH, Unbreakable pH, Universal Access are trademarks of Thermo Fisher.

Guaranteed Success and The Technical Edge are service marks of Thermo Fisher.

PerpHecT meters are protected by U.S. patent 6,168,707.

PerpHecT ROSS electrodes are protected by U.S. patent 6,168,707.

ORION Series A meters and 900A printer are protected by U.S. patents 5,198,093, D334,208

and D346,753.

ionplus electrodes and Optimum Results solutions are protected by U.S. patent 5,830,338.

ROSS Ultra electrodes are protected by U.S. patent 6,793,787.

ORP standard is protected by U.S. patent 6,350,367.

No Cal electrodes are protected by U.S. patent 7,276,142.

Scientific Inc. and its subsidiaries.

The specifications, descriptions, drawings, ordering information and part numbers within this document

are subject to change without notice.

This publication supersedes all previous publications on this subject.

IThermo Scientiﬁc Orion DUAL STAR™pH/ISE Meter User Guide

Table of Contents

Chapter 1 Introduction..........................................1

GeneralInformation................................................1

MeterPackingList.................................................2

Chapter 2 MeterOverview.......................................3

MeterConnections.................................................4

Channel1andChannel2Inputs.....................................5

Connecting Electrodes and Cables to the Meter . . . . . . . . . . . . . . . . . . . . . . . . 6

MeterKeypad.....................................................7

ShortcutKeysontheMeterKeypad..................................8

AlphanumericKeypad.............................................9

MeterDisplay....................................................10

DualChannelDisplay............................................10

SingleChannelDisplay ..........................................12

PoweringtheMeterOnandOff......................................14

MeterMaintenance...............................................14

Chapter 3 MeterSetup.........................................15

EZ Startup™Menu ................................................15

SetupMenu.....................................................19

NavigatingtheSetupMenu.......................................19

Channel1andChannel2SetupMenus..............................20

Instrument Parameters Setup Menu . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 27

AutosamplerSetupMenu ........................................33

Incremental Techniques Setup Menu . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 34

GLPSetupMenu...............................................34

EZStartupSetupMenu..........................................34

Thermo Scientiﬁc Orion DUAL STAR™pH/ISE Meter User GuideII

Chapter 4 Calibration and Measurement . . . . . . . . . . . . . . . . . . . . . . . . . . 35

pHCalibrationandMeasurement.....................................35

pH Calibration Procedure (1 to 6 points). . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 36

pHMeasurementProcedure......................................38

ISECalibrationandMeasurement....................................39

ISE Calibration Procedure (2 to 6 points) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 40

ISEMeasurementProcedure......................................42

mV Measurement and RmV and ORP Calibration and Measurement . . . . . . . . . 43

mVMeasurementProcedure......................................43

RmVCalibrationProcedure........................................44

RmVMeasurementProcedure.....................................45

ORPCalibrationProcedure........................................47

ORPMeasurementProcedure.....................................48

Temperature Calibration and Measurement . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 49

Temperature Calibration Procedure . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 49

Temperature Measurement Procedure. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 50

Dissolved Oxygen Calibration and Measurement. . . . . . . . . . . . . . . . . . . . . . . . . 51

Dissolved Oxygen Calibration Procedure . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 51

Dissolved Oxygen Measurement Procedure . . . . . . . . . . . . . . . . . . . . . . . . . . 52

Chapter 5 Methods............................................53

Saving the Current Meter Settings as a New Method . . . . . . . . . . . . . . . . . . . . . 53

LoadinganExistingMethod.........................................54

EditingorPrintinganExistingMethod.................................54

CopinganExistingMethod .........................................55

DeletinganExistingMethod ........................................56

Chapter 6 IncrementalTechniques................................57

SingleKnownAddition.............................................59

DoubleKnownAddition............................................61

SingleKnownSubtraction ..........................................63

DoubleKnownSubtraction..........................................66

IIIThermo Scientiﬁc Orion DUAL STAR™pH/ISE Meter User Guide

Chapter 7 DataStorageandRetrieval.............................69

DataStorageSettings..............................................69

Viewing the Calibration Log and Data Log . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 71

InterfacingaPrinter ...............................................73

InterfacingaComputer.............................................73

MeterSoftwareUpgrade.........................................74

Chapter 8 AutosamplerOperation ...............................75

Interfacing the Meter and Autosampler . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 75

AutosamplerSetupMenu...........................................76

RunningtheAutosampler...........................................79

AutosamplerErrorMessages......................................80

Chapter 9 CustomerServices ...................................81

TroubleshootingGuide.............................................81

ElectrodeStabilityTest...........................................81

MeterSelfTestandCheckout......................................82

UserReset....................................................83

FactoryConﬁguration............................................84

AboutMeter...................................................84

ElectrodeConditionIcon .........................................85

Assistance ....................................................85

Warranty......................................................85

MeterErrorCodes................................................86

NoticeofCompliance..............................................89

WEEECompliance................................................89

DeclarationofConformity...........................................90

Real Time Clock Battery Maintenance . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 91

OrderingInformation ..............................................92

MeterSpeciﬁcations...............................................95

MeterFeatures...................................................96

Thermo Scientiﬁc Orion DUAL STAR™pH/ISE Meter User GuideIV

Appendix 1 AdvancedMeterFeatures............................97

Multipoint Calibration Curve Feature . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 97

AutomaticBlankCorrectionFeature...................................98

ErrorCodeE306...............................................100

IsopotentialPointFeature..........................................101

Determining an Isopotential Point . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 102

Automatic pH Buffer Recognition Feature . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 103

Testing a pH Electrode for Automatic Buffer Recognition . . . . . . . . . . . . . . . 104

Important Note

Please read this user guide thoroughly before using your meter.

Any use outside of these instructions may invalidate your

warranty and cause permanent damage to the meter.

Contact Information

For assistance with Thermo Scientific Orion products, contact Technical Support.

Within the United States call 1.800.225.1480 and outside the United States call

978.232.6000 or fax 978.232.6031. In Europe, the Middle East and Africa, contact

your local authorized dealer. For the most current contact information, visit

www.thermo.com/contactwater.

Applications and Technical Resources

For the latest application and technical resources for Thermo Scientific Orion

products, visit www.thermo.com/waterapps. Our application webpage includes

the Orion DUAL STAR Meter Quick Start Notes for Ammonia in Water and

Wastewater, Fluoride in Water and Wastewater, Nitrate in Water and Wastewater,

and pH of Water and Wastewater. These quick start notes provide step-by-step

illustrated instructions for performing common measurements on the Orion

DUAL STAR meter.

1Thermo Scientiﬁc Orion DUAL STAR™pH/ISE Meter User Guide

Chapter 1 Introduction

General Information

This user guide contains information on the preparation, operation and

maintenance of the Thermo Scientific Orion DUAL STAR pH/ISE benchtop meter.

The Orion DUAL STAR meter has two measuring channels and is capable of

measuring pH, concentration (ISE), raw millivolts (mV), relative millivolts (RmV),

oxidation-reduction potential (ORP) and temperature.

Display Features

The large, backlit LCD screen on the Orion DUAL STAR meter displays both

measuring channels simultaneously or each measuring channel separately. Step-

by-step instructions and prompts are displayed on the meter to assist operators

with the setup, calibration and autosampler menus. A calibration graph, which

includes the electrode slope between points and the average slope, can be

viewed in the calibration mode.

Data Features

The Orion DUAL STAR meter can save up to 10 calibrations per channel and 1000

data points in the meter data log. A graph of the calibration points with slope can

be viewed on the meter display and printed. Calibration and measurement data

can be exported from the meter to a printer or computer. The meter saves up to

10 methods per channel, so switching the meter to different testing methods is

fast and simple.

Automation Features

The Orion DUAL STAR meter can be interfaced with the AutoTration™-500

autosampler for automated laboratory analysis.The autosampler has a 28 beaker

rack or 48 beaker rack for comprehensive, interchangeable configurations. The

autosampler function for the Orion DUAL STAR meter will be available in 2009.

Troubleshooting Features

Troubleshooting procedures are available in the meter setup menu and include a

meter stability test, meter self-test and meter reset functions.

Thermo Scientiﬁc Orion DUAL STAR™pH/ISE Meter User Guide2

Meter Packing List

The Thermo Scientific Orion DUAL STAR pH/ISE benchtop meter includes:

One Orion DUAL STAR meter

Two BNC shorting caps, Cat. No. 090045

One universal power adapter, Cat. No. 1010003

One swing arm electrode stand, Cat. No. 090043

One RS232 interface cable, Cat. No. 1010053

One USB interface cable

One user guide

Refer to the Ordering Information section for a list of meter accessories,

pH electrodes, ion selective electrodes (ISE), ATC probes, buffers, solutions and

standards or visit www.thermo.com/water for a full offering of Thermo Scientific

Orion products.

Introduction

3Thermo Scientiﬁc Orion DUAL STAR™pH/ISE Meter User Guide

Chapter 2 Meter Overview

25.0°C

log/print setup

cal

25.0°C

1.00

Ch.2

F-stabilizing

ppm

ATC2

7.000 0.0mV

Ch.1

pH ready

ATC1

0.0mV

Dual Channel

Display

Keypad

Channel Number

Designations

BNC Inputs

Thermo Scientiﬁc Orion DUAL STAR™pH/ISE Meter User Guide4

Meter Connections

BNC – Input for pH, ion selective (ISE) or ORP/redox electrodes with BNC or

waterproof BNC connectors.

Ref. – Input for reference electrodes with standard 2.5 mm pin-tip connectors.

ATC – Input for ATC probes with 8 pin MiniDIN connectors.

Stirrer – Input for the stirrer probe, Cat. No. 096019. The stirrer probe must be

purchased separately from the meter.

USB – Input for the USB cable, used to connect the meter to a computer. USB

function for the Orion DUAL STAR meter will be available by December 2009.

RS232 – Input for the RS232 cable, used to connect the meter to a printer

or computer.

Ground – Input for a ground wire with a standard pin-tip connector.

Power – Input for the universal power adapter that is included with the meter.

Ref.

ATC

BNC

USB

BNC

Stirrer Ground Power

RS232

Meter Overview

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