Agilent Technologies InfinityLab LC Series Bedienungsanleitung

Agilent InfinityLab LC Series

Variable Wavelength Detectors

User Manual

Agilent InfinityLab LC Series VWD User Manual

Notices

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Document No: SD-29000240

Part No: G7114-90001 Rev. C

EDITION 10/2019

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Agilent InfinityLab LC Series VWD User Manual 3

In This Book

This manual covers:

•the Agilent 1290 Infinity II Variable Wavelength Detector (G7114B) and

•the Agilent 1260 Infinity II Variable Wavelength Detector (G7114A).

Find information on other Agilent Variable Wavelength Detectors in separate

manuals.

1 Introduction to the Variable Wavelength Detector

This chapter gives an introduction to the detector, instrument overview and

internal connectors.

2 Site Requirements and Specifications

This chapter gives information on environmental requirements, physical and

performance specifications.

3 Using the Module

This chapter explains the essential operational parameters of the module.

4 Preparing the Module

This chapter provides information on how to set up the detector for an analysis

and explains the basic settings.

5 Optimizing the Detector

This chapter provides information on how to optimize the detector.

6Troubleshootingand Diagnostics

Overview about the troubleshooting and diagnostic features.

Agilent InfinityLab LC Series VWD User Manual 4

7ErrorInformation

This chapter describes the meaning of detector error messages, and provides

information on probable causes and suggested actions how to recover from error

conditions.

8 Test Functions

This chapter describes the detector’s built in test functions.

9 Maintenance

This chapter provides general information on maintenance of the detector.

10 Parts and Materials for Maintenance

This chapter provides information on parts for maintenance.

11 Identifying Cables

This chapter provides information on cables used with the Agilent 1200 Infinity

Series modules.

12 Hardware Information

This chapter describes the detector in more detail on hardware and electronics.

13 LAN Configuration

This chapter provides information on connecting the module to the Agilent

ChemStation PC.

14 Appendix

This chapter provides addition information on safety, legal and web.

Agilent InfinityLab LC Series VWD User Manual 5

Contents

1 Introduction to the Variable Wavelength Detector 9

Introduction to the Detector 10

Product Description 11

Optical System Overview 13

Dual-Wavelength Mode 18

Leak and Waste Handling 19

Operating Principle 24

2 Site Requirements and Specifications 25

Site Requirements 26

Physical Specifications 29

Performance Specifications 30

3 Using the Module 35

Magnets 36

Turn on/off 37

Status Indicators 39

Instrument Configuration 40

Set up the Detector with Agilent Open Lab ChemStation 42

The Detector User Interface 43

Detector Control Settings 45

Method Parameter Settings 46

Scanning with the VWD 50

Agilent Local Control Modules 52

4 Preparing the Module 54

Leak and Waste Handling 55

Setting up an Analysis 57

Solvent Information 64

Agilent InfinityLab LC Series VWD User Manual 6

5 Optimizing the Detector 69

Introduction 70

Match the Flow Cell to the Column 71

Set the Detector Parameters 74

Warm up of the Detector 75

6 Troubleshooting and Diagnostics 77

Available Tests versus Interfaces 78

Agilent Lab Advisor Software 79

7ErrorInformation80

What Are Error Messages 81

General Error Messages 82

Detector Error Messages 89

8 Test Functions 99

Introduction 100

Intensity Test 105

Cell Test 108

Wavelength Verification-Calibration 110

ASTM Drift and Noise Test 112

Quick Noise Test 113

Dark Current Test 115

Holmium Oxide Test 117

D/A Converter (DAC) Test 120

Other Lab Advisor Functions 123

Agilent InfinityLab LC Series VWD User Manual 7

9 Maintenance 124

Introduction to Maintenance 125

Warnings and Cautions 126

Overview of Maintenance 128

Cleaning the Module 129

Remove and Install the Doors 130

Replace the Deuterium Lamp 132

Replace the Flow Cell / Cuvette Holder 135

Repair the Flow Cells 137

Using the Cuvette Holder 141

Correcting Leaks 143

Replace Leak Handling System Parts 145

Replace the Module Firmware 146

10 Parts and Materials for Maintenance 147

Overview of Maintenance Parts 148

Standard Flow Cell 10 mm / 14 µl 150

Micro Flow Cell 3 mm / 2 µl 152

Semi-micro Flow Cell (Parts) 154

High Pressure Flow Cell (Parts) 156

Cuvette Holder (Parts) 157

Accessory Kit 158

11 Identifying Cables 159

Cable Overview 160

Analog Cables 162

Remote Cables 164

CAN Cable 168

RS-232 Cables 169

USB Cables 170

Agilent InfinityLab LC Series VWD User Manual 8

12 Hardware Information 171

Firmware Description 172

Electrical Connections 175

Interfaces 178

Setting the 6-bit Configuration Switch 186

Instrument Layout 190

Early Maintenance Feedback (EMF) 191

13 LAN Configuration 193

What You Have to Do First 194

TCP/IP parameter configuration 195

Configuration Switch 196

Initialization Mode Selection 197

Dynamic Host Configuration Protocol (DHCP) 199

Manual Configuration 202

14 Appendix 206

General Safety Information 207

Waste Electrical and Electronic Equipment (WEEE) Directive 216

Radio Interference 217

Sound Emission 218

Solvent Information 219

Declaration of Conformity for HOX2 Filter 220

Agilent Technologies on Internet 221

Agilent InfinityLab LC Series VWD User Manual 9

1 Introduction to the Variable Wavelength

Detector

Introduction to the Detector 10

Product Description 11

Product Description G7114A 11

Product Description G7114B 12

Optical System Overview 13

Flow Cell 14

Lamp 15

Source Lens Assembly 15

Entrance Slit Assembly 15

Filter Assembly 16

Mirror Assemblies M1 and M2 17

Grating Assembly 17

Beam Splitter Assembly 17

Photo Diodes Assemblies 17

Photo Diode ADC (analog-to-digital converter) 17

Dual-Wavelength Mode 18

Leak and Waste Handling 19

Leak Sensor 23

Waste Concept 23

Operating Principle 24

This chapter gives an introduction to the detector, instrument overview and

internal connectors.

Agilent InfinityLab LC Series VWD User Manual 10

1 Introduction to the Variable Wavelength Detector

Introduction to the Detector

The Agilent variable wavelength detectors described in this manual are designed

for highest optical performance, GLP compliance and easy maintenance with:

•higher data rate up to 120 Hz (G7114A) or 240 Hz for ultra-fast-HPLC

(G7114B),

•deuterium lamp for highest intensity and lowest detection limit over a

wavelength range of 190 to 600 nm,

•optional flow-cell cartridges (standard 10 mm, 14 µL; high pressure 10 mm,

14µL;micro3mm,2µL;semi-micro6mm,5µL)andPrepCellsareavailable

and can be used depending on the application needs (other types may be

introduced later),

•Dual wavelength mode, see “Dual-Wavelength Mode” on page 18.

•easy front access to lamp and flow cell for fast replacement,

•electronic identification of flow cell and lamp with RFID (Radio Frequency

Identification) tag for unambiguous identification,

•lamp information: part number, serial number, production date, ignitions,

burn time

•cell information: part number, serial number, production date, nominal

path length, volume, maximum pressure

•built-in electronic temperature control (ETC) for improved baseline stability,

and

•built-in holmium oxide filter for fast wavelength accuracy verification.

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