Agilent Technologies 1260 Infinity Bedienungsanleitung

Agilent Technologies

Agilent 1260 Infinity

Diode Array and Multiple

Wavelength Detector

User Manual

Agilent 1260 Infinity DAD and MWD User Manual

Notices

No part of this manual may be reproduced

in any form or by any means (including elec-

tronic storage and retrieval or translation

into a foreign language) without prior agree-

ment and written consent from Agilent

Technologies, Inc. as governed by United

States and international copyright laws.

Manual Part Number

G1315-90013

Edition

06/10

Printed in Germany

Agilent Technologies

Hewlett-Packard-Strasse 8

76337 Waldbronn

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The material contained in this docu-

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ject to being changed, without notice,

in future editions. Further, to the max-

imum extent permitted by applicable

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either express or implied, with regard

to this manual and any information

contained herein, including but not

limited to the implied warranties of

merchantability and fitness for a par-

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consequential damages in connection

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Agilent and the user have a separate

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document that conflict with these

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arate agreement shall control.

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1987). U.S. Government users will receive

no greater than Limited Rights as defined in

FAR 52.227-14 (June 1987) or DFAR

252.227-7015 (b)(2) (November 1995), as

applicable in any technical data.

Safety Notices

CAUTION

A CAUTION notice denotes a

hazard. It calls attention to an

operating procedure, practice, or

the like that, if not correctly per-

formed or adhered to, could

result in damage to the product

or loss of important data. Do not

proceed beyond a CAUTION

notice until the indicated condi-

tions are fully understood and

met.

WARNING

A WARNING notice denotes a

hazard. It calls attention to an

operating procedure, practice,

or the like that, if not correctly

performed or adhered to, could

result in personal injury or

death. Do not proceed beyond a

WARNING notice until the indi-

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stood and met.

For Research Use Only

Agilent 1260 Infinity DAD and MWD User Manual 3

In This Guide…

This manual covers the Agilent 1260 Infinity Diode Array and Multiple

Wavelength Detector modules:

•G1315C - 1260 DAD VL+

•G1365C - 1260 MWD

•G1315D - 1260 DAD VL

•G1365D - 1260 MWD VL

1 Introduction

This chapter gives an introduction to the detector, instrument overview and

internal connectors.

2 Site Requirements and Specifications

This chapter provides information on environmental requirements, physical

and performance specifications.

3 Installing the Module

This chapter gives information about the preferred stack setup for your system

and the installation of your module.

4 LAN Configuration

This chapter provides information on connecting the detector to the Agilent

ChemStation PC.

5 Using the Detector

This chapter provides information on how to set up the detector for an

analysis and explains the basic settings.

6 How to optimize the Detector

This chapter provides information on how to optimize the detector.

4 Agilent 1260 Infinity DAD and MWD User Manual

In This Guide…

7 Troubleshooting and Diagnostics

This chapter gives an overview about the troubleshooting and diagnostic

features and the different user interfaces.

8 Error Information

This chapter describes the meaning of error messages, and provides

information on probable causes and suggested actions how to recover from

error conditions.

9TestFunctions

This chapter describes the detector’s built in test functions.

10 Maintenance

This chapter describes the maintenance of the detector.

11 Parts for Maintenance

This chapter provides information on parts for maintenance.

12 Identifying Cables

This chapter provides information on cables used with the 1200 series of

HPLC modules.

13 Appendix

This chapter provides addition information on safety, legal and web.

Agilent 1260 Infinity DAD and MWD User Manual 5

Contents

1 Introduction 9

Introduction to the Detector 10

Optical System 11

Early Maintenance Feedback (EMF) 14

Instrument Layout 15

Electrical Connections 16

Interfaces 18

Setting the 8-bit Configuration Switch 24

2 Site Requirements and Specifications 33

Site Requirements 34

Physical Specifications 37

Performance Specifications 38

3 Installing the Module 43

Unpacking the Detector 44

Optimizing the Stack Configuration 46

Installing the Detector 50

Flow Connections to the Detector 53

Setting up the LAN access 56

4 LAN Configuration 57

What you have to do first 58

TCP/IP parameter configuration 59

Configuration Switch 60

Initialization mode selection 61

Link configuration selection 65

Automatic Configuration with BootP 66

Storing the settings permanently with Bootp 76

Manual Configuration 77

6 Agilent 1260 Infinity DAD and MWD User Manual

Contents

5 Using the Detector 83

Setting up an Analysis 84

Special Settings of the Detector 100

Special Setups with Multiple DAD-MWDs 114

6 How to optimize the Detector 115

Introduction 116

Optimization Overview 117

Optimizing for Sensitivity, Selectivity, Linearity and Dispersion 119

Optimizing Selectivity 129

7 Troubleshooting and Diagnostics 133

Overview of the Module’s Indicators and Test Functions 134

Status Indicators 135

User Interfaces 137

Agilent Lab Advisor Software 138

8 Error Information 139

What Are Error Messages 141

General Error Messages 142

Detector Error Messages 150

9 Test Functions 161

Self-test 162

Filter Test 164

Slit Test 166

Dark-Current Test 167

Intensity Test 170

Holmium Oxide Test 174

Spectral flatness test 177

ASTM Noise Test 178

Cell Test 179

Using the Built-in Test Chromatogram 181

Wavelength Verification and Recalibration 183

Test Chromatogram 184

Diagnosis Information on Agilent ChemStation 186

D/A Converter (DAC) Test 188

Agilent 1260 Infinity DAD and MWD User Manual 7

Contents

10 Maintenance 191

Introduction to Maintenance 192

Cautions and Warnings 193

Overview of Maintenance 195

Cleaning the Module 196

Exchanging a Lamp 197

Exchanging a Flow Cell 200

Maintenance of Standard, Semi-Micro or Micro Flow Cell 203

Maintenance of High Pressure Flow Cell 207

Replacing Capillaries on a Standard Flow Cell 209

Replacing Capillaries on a Semi-Micro and Micro Flow Cell 214

Nano Flow Cell - Replacing or Cleaning 218

Cleaning or Exchanging the Holmium Oxide Filter 223

Correcting Leaks 226

Replacing Leak Handling System Parts 227

Replacing the CompactFlash Card (G1315C/G1365C only) 228

Replacing the Module’s Firmware 229

11 Parts for Maintenance 231

Overview of Maintenance Parts 232

Standard Flow Cell 234

Semi-Micro Flow Cell Parts 236

Micro Flow Cell 238

Prep Flow Cell - SST 240

Prep Flow Cell - Quartz 242

Nano Flow Cells 244

High Pressure Flow Cell 248

Accessory Kits 250

12 Identifying Cables 253

Cable Overview 254

Analog Cables 256

Remote Cables 258

BCD Cables 261

CAN/LAN Cables 263

Agilent 1200 module to PC 264

8 Agilent 1260 Infinity DAD and MWD User Manual

Contents

13 Appendix 265

General Safety Information 266

The Waste Electrical and Electronic Equipment (WEEE) Directive

(2002/96/EC) 269

Radio Interference 270

Sound Emission 271

UV-Radiation 272

Solvent Information 273

Declaration of Conformity for HOX2 Filter 275

Agilent Technologies on Internet 276

Agilent 1260 Infinity DAD and MWD User Manual

Agilent Technologies

Introduction

Introduction to the Detector 10

Optical System 11

Early Maintenance Feedback (EMF) 14

Instrument Layout 15

Electrical Connections 16

Serial Number Information (ALL) 17

Rear view of the module 17

Interfaces 18

Interfaces Overview 20

Setting the 8-bit Configuration Switch 24

Communication Settings for RS-232C 28

Special Settings 30

This chapter gives an introduction to the detector, instrument overview and

internal connectors.

10 Agilent 1260 Infinity DAD and MWD User Manual

1Introduction

Introduction to the Detector

The detector is designed for highest optical performance, GLP compliance and

easy maintenance. It includes the following features:

•80 Hz data acquisition rate for (ultra-) fast LC applications (requires

internal hard disk, G1315C and G1365C only),

•data recovery (DRC) feature provides data-never-lost insurance (requires

internal hard disk, G1315C and G1365C only),

•RFID tags for all flow cells and UV-lamps provides traceable information

about these assemblies,

•long-life deuterium with RFID tag and tungsten lamps for highest intensity

and lowest detection limit over a wavelength range of 190–950 nm,

•no loss in sensitivity for up to eight wavelengths simultaneous,

•programmable slit from 1–16 nm for complete optimization of sensitivity,

linearity and spectral resolution,

•optional flow-cell cartridges with RFID tag (standard 10 mm 13 µl,

semi-micro 6 mm 5 µl, micro 3 mm 2 µl, 80 nl, 500 nl, 10 mm, high pressure

10 mm 1.7 µl and prep-cells) are available and can be used depending on

the application needs,

•easy front access to lamps and flow cell for fast replacement, and

•built-in holmium oxide filter for fast wavelength accuracy verification,

•built-in temperature control for improved baseline stability,

•additional diagnostic signals for temperature and lamp voltage monitoring,

For specifications, see “Performance Specifications” on page 38.

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