Emerson Rosemount 3300HT Bedienungsanleitung

Rosemount™3300HT/3300HTVP/3400HT/

3400HTVP/3500P/3500VP

PERpH-X High Performance pH/ORP Sensors

Instruction Manual

LIQ-MA -PERpH-X

Rev. J

April 2017

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Emerson designs, manufactures and tests its products to meet many national and international stan-

dards. Because these sensors are sophisticated technical products, you MUST properly install, use,

and maintain them to ensure they continue to operate within their normal specifications. The

following instructions MUST be adhered to and integrated into your safety program when installing,

using, and maintaining Rosemount products. Failure to follow the proper instructions may cause

any one of the following situations to occur: loss of life; personal injury; property damage; damage

to this sensor; and warranty invalidation.

• Read all instructions prior to installing, operating, and servicing the product.

• If you do not understand any of the instructions, contact your Emerson representative for

clarification.

• Follow all warnings, cautions, and instructions marked on and supplied with the product.

• Inform and educate your personnel in the proper installation, operation, and maintenance

of the product.

• Install your equipment as specified in the Installation Instructions of the appropriate

Instruction Manual and per applicable local and national codes. Connect all products to

the proper electrical and pressure sources.

• To ensure proper performance, use qualified personnel to install, operate, update,

program, and maintain the product.

• When replacement parts are required, ensure that qualified people use replacement parts

specified by Emerson. Unauthorized parts and procedures can affect the product's

performance, place the safe operation of your process at risk, and VOID YOUR WARRA TY.

Third-party substitutions may result in fire, electrical hazards, or improper operation.

• Ensure that all equipment doors are closed and protective covers are in place, except when

maintenance is being performed by qualified persons, to prevent electrical shock and

personal injury.

The information contained in this document is subject to change without notice.

Essential Instructions

Read this page before proceeding!

Sensor/Process Application Compatibility

The wetted sensor materials may not be compatible with process composition and operating

conditions. Application compatibility is entirely the responsibility of the user.

WARNING

Before removing the sensor, be absolutely certain that the process pressure is reduced to 0 psig and

the process temperature is lowered to a safe level!

CAUTION

1. All pH/ORP sensors have a plastic enclosure which must only be cleaned with a damp cloth to avoid

the danger due to a build up of an electrostatic charge.

2. All pH/ORP sensor models are intended to be in contact with the process fluid and may not meet the

500V r.m.s. a.c. test to earth.

This must be taken into consideration at installation.

Special Conditions for Safe Use

CAUTION

This manual contains instructions for installation and operation of the Rosemount 3300HT/3300HTVP/

3400HT/3400HTVP/3500P/3500VP.

The following list provides concerning all revisions of this document.

Rev. Level Date Notes

J 04/2017 Updated information with new Emerson Style Guidelines, Updated

Ordering Information, Specifications, and Wiring Diagrams. Added

Accessories Information, EC Declaration of Conformity and

FM Installation Drawings.

About This Document

Contents

Section 1: Specifications

1.1 Specifications ......................................................................................................1

1.2 Product Certifications ..........................................................................................3

1.3 Ordering Information...........................................................................................4

Section 2: Installation

2.1 Storage................................................................................................................7

2.2 Installation...........................................................................................................7

2.3 Retraction with Kit P/ 23240-00 ......................................................................16

2.4 Electrical Installation..........................................................................................17

Section 3: Startup and Calibration

3.1 Electrode Preparation .......................................................................................21

3.2 pH Sensor Calibration ........................................................................................21

3.3 Recommended pH Sensor Standardization ........................................................21

Section 4: Maintenance

4.1 Electrode Cleaning.............................................................................................23

4.2 Reference Junction Replacement and Sensor Electrolyte Recharge .....................23

Section 5: Accessories

5.1 Accessories ........................................................................................................25

EC Declaration of Conformity.............................................................................27

Intrisicallly Safe Sensor Installation Drawing - FM ................................29

Instruction Manual Table of Contents

LIQ-MA -PERpH-X April 2017

Table of Contents i

Table of Contents Instruction Manual

April 2017 LIQ-MA -PERpH-X

ii Table of Contents

Section 1: Specifications

1.1 Specifications

Specifications 1

Instruction Manual Specifications

LIQ-MA -PERpH-X April 2017

Table 1-2: Rosemount 3300HT/3300HTVP sensor specifications

Measured Range

pH range 0 to 14 pH

ORP range -1500 mV to 1500 mV

Operating Temperature

Without Preamplifier 41 to 311 °F (5 to 155 °C)

With Preamplifier up to 212 °F (100 °C)

Storage Temperature

14 to 138 °F (-10 to 70 °C)

Maximum Process Pressure

400 psig (2859 kPa [abs])

CRN Rating: 200 psig at room temperature

Wetted Materials

Titanium, Ryton, Teflon, Glass, and User Specified O-ring Material (EPDM, Viton or Kalrez)

Reference Electrode

Double junction with replaceable process side electrolyte and Teflon junction

Temperature Sensor

Pt-100 RTD

Process Connections

Must use 1 in. compression process connector (P/N 23166-00 or 23166-01)

Weight/Shipping Weight

1 lb/2 lb (0.5 kg/0.9 kg)

Cable Length

15 ft. integral cable (Rosemount 3300HT) or VP8 Cable for Rosemount 3300HTVP (sold separately)

pH Range HT Series

0-2 pH 94%

2-12 pH 99%

12-13 pH 97%

13-14 pH 92%

Table 1-1: Percent linearity over pH

2 Specifications

Specifications Instruction Manual

April 2017 LIQ-MA -PERpH-X

Table 1-3: Rosemount 3400HT/3400HTVP sensor specifications

Measured Range

pH range 0 to 14 pH

ORP range -1500 mV to 1500 mV

Operating Temperature

Without Preamplifier 41 to 311 °F (5 to 155 °C)

With Preamplifier up to 293 °F (145 °C)

Storage Temperature

14 to 138 °F (-10 to 70 °C)

Maximum Process Pressure

400 psig (2859 kPa [abs])

CRN Rating: 200 psig at room temperature

Wetted Materials

Titanium, Ryton, Teflon, Glass, and User Specified O-ring Material (EPDM, Viton or Kalrez)

Reference Electrode

Double junction with replaceable process side electrolyte and Teflon junction

Temperature Sensor

Pt-100 RTD

Process Connections

Must use 1 in. compression process connector (P/N 23166-00 or 23166-01)

Can be inserted through a ball valve

Weight/Shipping Weight

21 inch Sensor 2 lbs/3 lbs (0.9 kg/1.4 kg)

36 inch Sensor 3 lbs/4 lbs (1.4 kg/1.8 kg)

Table 1-4: Rosemount 3500P/3500VP sensor specifications

Measured Range

pH range 0 to 14 pH

ORP range -1500 mV to 1500 mV

Operating Temperature

41 to 248 °F (5 to 120 °C)

Storage Temperature

14 to 122 °F (-10 to 50 °C)

Maximum Process Pressure

100 psig (790 kPa [abs])

CRN Rating: 40 psig at room temperature

Wetted Materials

Titanium, Ryton, Teflon, Glass, and User Specified O-ring Material (EPDM, Viton or Kalrez)

Reference Electrode

Double junction with replaceable process side electrolyte and Teflon junction

Temperature Sensor

Pt-100 RTD

Process Connections

1in. MNPT Front and Rear facing threads

Weight/Shipping Weight

21 inch Sensor 2 lbs/3 lbs (0.9 kg/1.4 kg)

Specifications 3

Instruction Manual Specifications

LIQ-MA -PERpH-X April 2017

1.2 Product Certifications

Please see online certificates for further details.

IECEx

Sensors without preamp – Ex ia C T4 Ga (-20 °C ≤ Ta ≤ +60°C)

Sensors with SMART preamp (pH only) – Ex ia C T4 Ga (-20°C ≤ Ta ≤ +60°C)

Sensors with standard preamp (ORP only) – Ex ia C T4 Ga (-20°C ≤ Ta ≤ +80°C) or

Ex ia C T5 Ga (-20°C ≤ Ta ≤ +40°C)

Per standards EC60079-0 : 2011, EC 60079-11 : 2011

ATEX

Sensors without preamp – 1 G Ex ia C T4 Ga (-20˚C ≤ Ta ≤ +60˚C)

Sensors with SMART preamp (pH only) – 1 G Ex ia C T4 Ga (-20˚C ≤ Ta ≤ +60˚C)

Sensors with standard preamp (ORP only) – 1 G Ex ia C T4 Ga (-20˚C ≤ Ta ≤ +80˚C) or

1 G Ex ia C T5 Ga (-20˚C ≤ Ta ≤ +40˚C)

Per standards EN 60079-0: 2012+A11:2013, EN 60079-11:2012

See online FM Certificate of Compliance for applicable sensor options:

ntrinsically Safe for use in Class , , and , Division 1, Groups A, B, C, D, E, F, and G; Temperature

Class T6 Ta = -20˚C to +60˚C

ntrinsically Safe for use in Class , Zone 0, AEx ia C T6 Ta = -20˚C to +60˚C

Nonincendive for use in Class , Division 2, Groups A, B, C, and D; Temperature Class T6 Ta = -20˚C

to +60˚C

Suitable for use in Class and , Division 2, Groups E, F, and G; Temperature Class T6 Ta = -20˚C

to +60˚C Hazardous (Classified) Locations

S/ , , /1/ABCDEFG/T6 Ta = 60°C - 1400332; Entity; /0/AEx ia C/T6 Ta = 60°C - 1400332; Entity;

N / /2/ABCD/T6 Ta = 60°C; S/ , /2/EFG/T6 Ta = 60°C

Per standards 3600:1998, 3610:2010, 3611:2004, 3810:2005

CSA

See online CSA Certificate of Compliance for applicable sensor options:

Sensors with preamp – ntrinsically Safe:

Class , Division 1, Groups ABCD; Class , Division 1, Groups EFG; Class ; Class , Division 2, Groups

ABCD; Ambient temperature rating -20˚C to +60˚C; Ex ia C; T6

Sensors without preamp – ntrinsically Safe and Non- ncendive:

Class , Division 1, Groups ABCD; Class , Division 1, Groups EFG; Class ; Class , Division 2, Groups

ABCD; Ex ia C; T6; Ambient temperature rating -20˚C to +60˚C: (Simple Apparatus)

Per standards C22.2 No. 0-10, C22.2 No. 0.4-M2004, C22.2 No. 94-M1991, C22.2 No. 142 – M1987,

C22.2 No 157 – M1992, CAN/CSA E60079-0:07, CAN/CSA E60079 - 11:02, UL50 11th Ed, UL508

17th Ed, UL913 7th Ed, UL 60079-0: 2005, UL 60079-11: 2002

4 Installation

Specifications Instruction Manual

April 2017 LIQ-MA -PERpH-X

1.3 Ordering Information

Table 1-5: Rosemount 3300HT sensor ordering information

Model Sensor type

3300HT pH/ORP Sensor

Measuring Electrode

10 pH - GPHT Glass

12 ORP

O-ring Material

30 EPDM

31 Viton

32 Kalrez

Typical Model Number: 3300HT-10-30

Table 1-6: Rosemount 3300HTVP sensor ordering information

Model Sensor type

3300HTVP pH/ORP Sensor

Measuring Electrode

10 pH - GPHT Glass

12 ORP

O-ring Material

30 EPDM

31 Viton

32 Kalrez

Preamplifier Option

_ o selection

70 SMART Preamplifier (1)

Typical Model Number: 3300HTVP-10-30-70

1. On y avai ab e if se ected with option 10.

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