Hach NV3300 Bedienungsanleitung

DOC023.97.90608
NV3300
10/2018, Edition 4
User Manual
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Manual del usuario
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Table of contents
Specifications on page 3 Maintenance on page 15
General information on page 4 Troubleshooting on page 16
Installation on page 8 Replacement parts and accessories on page 17
Operation on page 13
Legal information
Manufacturer: TriOS Mess- und Datentechnik GmbH
Distributor: Hach Lange GmbH
The translation of the manual is approved by the manufacturer.
Specifications
Specifications are subject to change without notice.
Specification Details
Measurement principle Attenuation, transmission
Detector type Light source: 2 LEDs; detector: Photo diodes
Parameter SAC436nm
Colouring: 410 nm (based on DIN EN ISO 7887)
Pt-Co color number: 390 or 455 nm (APHA/Hazen)
Accuracy 0.5 %
Turbidity compensation 740 nm
T100 response time 4 seconds
Measurement interval ≥ 2 seconds
Dimensions (Ø × L) 48 x 333 mm1
Enclosure Stainless steel 1.4571/1.4404; Titanium 3.7035
Weight Stainless steel: 2.5 kg; Titanium: 1.3 kg1
Environmental rating IP68
Interface Digital: Ethernet (TCP/IP), RS-232 or RS-485 (Modbus RTU, ASCII)
Analog: Ethernet (TCP/IP), 4-20 mA
Power requirements The controller supplies power to the probe
Maximum pressure With fixed cable: 3 bars
In flow cell: 1 bar; flow: 2 to 4 L/min
Sample temperature 2 to 40 °C (36 to 104 °F)
Operating temperature 2 to 40 °C (36 to 104 °F)
Storage temperature -20 °C to 80 °C (-4 °F to 176 °F)
Inflow velocity 0.1 to 10 m/s
Optical path length 50, 100, 150 and 250 mm (1.97, 3.94, 5.90 and 9.84 in)
1With 50 mm path
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Specification Details
Certifications CE
Warranty EU: 2 years, US: 1 year
Table 1 Specifications—Measurement ranges and detection limits
Parameter Unit Measurement range based on the optical path2 3
50 mm 100 mm 150 mm 250 mm
SAC 436 nm 1/m 0.1 to 30 0.05 to 15 0.03 to 10 0.02 to 6
True color 410 nm mg/L Pt 2 to 560 1 to 280 0.6 to 185 0.4 to 110
Hazen 390 nm mg/L Pt 0.8 to 220 0.4 to 110 0.3 to 75 0.2 to 45
Hazen 455 nm mg/L Pt 4 to 1100 2 to 550 1.5 to 360 0.8 to 220
General information
In no event will the manufacturer be liable for direct, indirect, special, incidental or consequential
damages resulting from any defect or omission in this manual. The manufacturer reserves the right to
make changes in this manual and the products it describes at any time, without notice or obligation.
Revised editions are found on the manufacturer’s website.
Safety information
N O T I C E
The manufacturer is not responsible for any damages due to misapplication or misuse of this product including,
without limitation, direct, incidental and consequential damages, and disclaims such damages to the full extent
permitted under applicable law. The user is solely responsible to identify critical application risks and install
appropriate mechanisms to protect processes during a possible equipment malfunction.
Please read this entire manual before unpacking, setting up or operating this equipment. Pay
attention to all danger and caution statements. Failure to do so could result in serious injury to the
operator or damage to the equipment.
Make sure that the protection provided by this equipment is not impaired. Do not use or install this
equipment in any manner other than that specified in this manual.
Use of hazard information
D A N G E R
Indicates a potentially or imminently hazardous situation which, if not avoided, will result in death or serious injury.
WARNING
Indicates a potentially or imminently hazardous situation which, if not avoided, could result in death or serious
injury.
CAUTION
Indicates a potentially hazardous situation that may result in minor or moderate injury.
N O T I C E
Indicates a situation which, if not avoided, may cause damage to the instrument. Information that requires special
emphasis.
2Transmission at 740 nm must always be higher than 33%, if not, the content of turbid material in
the medium is too high and the path must be lower.
3The detection limit specification refers to a standard reference solution with lab conditions.
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Precautionary labels
Read all labels and tags attached to the instrument. Personal injury or damage to the instrument
could occur if not observed. A symbol on the instrument is referenced in the manual with a
precautionary statement.
This is the safety alert symbol. Obey all safety messages that follow this symbol to avoid potential
injury. If on the instrument, refer to the instruction manual for operation or safety information.
This symbol indicates that a risk of electrical shock and/or electrocution exists.
This symbol identifies the presence of a strong corrosive or other hazardous substance and a risk of
chemical harm. Only individuals qualified and trained to work with chemicals should handle chemicals
or perform maintenance on chemical delivery systems associated with the equipment.
This symbol indicates the presence of devices sensitive to Electro-static Discharge (ESD) and
indicates that care must be taken to prevent damage with the equipment.
This symbol indicates the need for protective eye wear.
Electrical equipment marked with this symbol may not be disposed of in European domestic or public
disposal systems. Return old or end-of-life equipment to the manufacturer for disposal at no charge to
the user.
Electromagnetic waves
WARNING
Multiple hazards. Do not disassemble the instrument for maintenance. If the internal components must
be cleaned or repaired, contact the manufacturer.
WARNING
Electromagnetic radiation hazard. Do not use the instrument in dangerous environments.
N O T I C E
This instrument is sensitive to electromagnetic and electromechanical interference. These interferences can have
an effect on the analysis performance of this instrument. Do not put this instrument near equipment that can
cause interference.
Obey the safety information that follows to operate the instrument in accordance with local, regional
and national requirements.
• Do not operate the instrument in hospitals and equivalent establishments or near medical
equipment, such as pace makers or hearing aids.
• Do not operate the instrument near highly flammable substances, such as fuels, highly flammable
chemicals and explosives.
• Do not operate the instrument near combustible gases, vapors or dust.
• Keep the instrument away from strong vibration or shock.
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• The instrument can cause interference in immediate proximity to televisions, radios and
computers.
• The warranty does not cover improper use or wear.
Chemical and Biological Safety
D A N G E R
Chemical or biological hazards. If this instrument is used to monitor a treatment process and/or
chemical feed system for which there are regulatory limits and monitoring requirements related to
public health, public safety, food or beverage manufacture or processing, it is the responsibility of the
user of this instrument to know and abide by any applicable regulation and to have sufficient and
appropriate mechanisms in place for compliance with applicable regulations in the event of malfunction
of the instrument.
Normal operation of this device may require the use of chemicals or samples that are biologically
unsafe.
• Observe all cautionary information printed on the original solution containers and safety data
sheets prior to their use.
• Dispose of all consumed solutions in accordance with the local and national regulations and laws.
• Select the type of protective equipment suitable to the concentration and quantity of the dangerous
material being used.
Product overview
The NV3300 color probe is a photometric sensor used for Spectral Absorption Coefficient (SAC) or
transmission measurements in aqueous solutions in waste water, drinking water and environmental
applications. Refer to Figure 1.
There are 8 different models of the probe based on the application and the measured parameter.
Each model has different parameters based on the nominal wavelength of the LED. The probe is
available with 4 different optical path lengths: 50, 100, 150 and 250 mm. Refer to Specifications
on page 3.
The probe connects to a CD500 or a CD300 digital controller to monitor the measurement data,
calibration and configuration.
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Figure 1 Product overview
1 Optical path with optical windows 4 Hanging ring
2 Probe 5 Probe cable with connector
3 Chain holder mount 6 Compressed air connector
Product components
Make sure that all components have been received. Refer to Figure 2. If any items are missing or
damaged, contact the manufacturer or a sales representative immediately.
Figure 2 Product components
1 Probe 2 Compressed air connector
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Theory of operation
The sensor uses two LEDs for long-term stable measurements of SAC values or color numbers at a
different wavelengths. Table 2 shows the applicable parameters based on the sensor type.
The light intensity of the LEDs usually changes with the temperature. The sensor uses a correction
factor for each different wavelength to calculate the measurement value. The absorbance is
calculated with the formula that follows:
A = -log10 T
T = I / I0
where:
T = transmission in %
I = current light intensity
I0 = basic light intensity in ultra-pure water
A = absorption in AUs (absorbance units)
Based on the model, the sensor outputs the SAC (Spectral Absorption Coefficient) of the wavelength
of LED1. The wavelength and absorption of LED1 is labelled in the sub-index SACxxx and Axxx. The
wavelength of LED2 is 740 nm. The scattering of light on particles in a solution is seen as turbidity.
The sensor uses the absorbance of 740 nm (A740) for the turbidity correction of the absorption
measurement of the wavelength emitted by LED1. The SAC of each wavelength of LED1 is
calculated with the formula that follows:
SACXXX = (Axxx – A740) * 1000 / d
where:
d = length of the optical path of the sensor in mm
SAC = spectral absorption coefficient in 1/m
Table 2 SAC parameter
Parameters Unit Factor4LED 1 (nm) LED 2 (nm) In agreement with
SAC 436 1/m — 436 740 DIN EN ISO 7887:2011_method B
Installation
CAUTION
Multiple hazards. Only qualified personnel must conduct the tasks described in this section of the
document.
Installation guidelines
Note: Make sure that the enclosure of the probe is titanium before use in sea water.
• Do not use stainless steel probes in sea water or other corrosion-causing media (e.g., acids,
alkalis, chlorine-based compounds). Clean the probe immediately.
• Do not use titanium probes in bromine, hydrofluoric acid and hot acids. Clean the probe
immediately if the probe touches hydrofluoric acid or hot acids.
• The seals of the probe are made of NBR (nitrile butadiene rubber). Make sure that the measuring
medium does not cause damage to the probe components.
• Do not replace the cable. If the cable has damage, contact the manufacturer.
• Make sure that the cable is not routed near hot surfaces. Make sure not to put heavy objects on
the cable.
• Make sure that there are no unwanted materials in the optical path.
4In some applications it is necessary to enter a factor to scale the SAC at a specified
wavelength.
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• Immediately set the instrument to OFF if the probe sends out smoke, noxious fumes or gets hot.
Contact the manufacturer.
Installation overview
Figure 3 shows an example of the probe installation with a chain holder option. Figure 4 shows an
example of the probe installation with a flow cell option. Refer to the installation documentation to
install the probe.
Put the probe into the sample. Make sure that the optical path is always fully immersed into the
sample. Install the probe transversally to the flow direction of the sample so the particle on the
windows are at a minimum and the nano-layer function gives the optimum support. Refer to Figure 5.
Note: Make sure that the probe does not touch the ground.
Figure 3 Chain holder installation
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Figure 4 Sensor with flow cell
1 Outflow, 6mm OD 3 Flow cell
2 Connector for cleaning fluid 4 Inflow, 8 mm OD
Figure 5 Flow direction
Connect the probe to the controller
N O T I C E
Never connect the sensor to the controller when the controller is energized or damage to the sensor can
occur.
The probe has a 10 m fixed cable with an M12 industrial plug that connects to a digital controller for
signal transmission and power. Refer to Figure 6 and Figure 7.
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