IKA C 200 Bedienungsanleitung

Andere Handbücher für C 200

2

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IKA®

Operating instructions EN

35 488 01

Calorimeter system C 200

C200 Vers. 01 Reg.-No. 4343-01

IKA®-WERKE C 200 Ver. 02/2.06

Table of contents

Chapter Page

1 Safety precautions 6

2 User information 9

2.1 Information regarding operating instructions 9

2.2 Warranty and liability 9

3 Transport, storage, place of installation 10

3.1 Conditions of transport and storage 10

3.2 Place of installation 10

3.3 Unpacking 10

3.4 Contents C 200 11

4 Installation and starting up 12

4.1 Calorimeter C 200 12

4.2 Installation 12

4.3 Switching on the system 14

4.4 Display and operating elements 14

4.5 Configuring the system 16

4.6 System settings 17

4.7 Filling the calorimeter for the first time 19

4.8 Switching off the system 20

4.9 Coding decomposition vessels 20

4.10 Oxygen station C 248 21

5 Calorimetric measurements 22

5.1 Determining the calorific value 22

5.2 Corrections 23

5.3 Information about the sample 24

5.4 Calibration 25

6Preparing and performing measurements 26

6.1 Decomposition vessel C 5010 26

6.2 Preparing the decomposition vessel 27

6.3 Preparing the measurement 29

6.4 Performing the measurement 30

6.5 Cleaning the decomposition vessel 32

6.6 Errors in the measuring procedure 33

7 Service menu 36

7.1 Operation 36

7.2 Description of service menu options 37

4IKA®-WERKE C 200 Ver. 02/2.06

Table of contents

Chapter Page

8 Cleaning and maintenance 38

8.1 Inner vessel filter 38

8.2 Filler 38

8.2a Micro filter 38

8.3 Maintaining the water circulation 39

8.4 Decomposition vessels 40

8.5 Cleaning information 40

9IKA®accessories and consumablesl 41

9.1 Accessories 41

9.2 Consumables 41

10 Technical data 42

IKA®-WERKE C 200 Ver. 02/2.06

CE – KONFORMITÄTSERKLÄRUNG

Wir erklären in alleiniger Verantwortung, dass dieses Produkt den Bestimmungen

der Richtlinien 89 / 336 EWG; 89 / 392 EWG und 73 / 23 EWG entspricht und mit

folgenden Normen und normativen Dokumenten übereinstimmt:

EN 61 010; EN 50 082; EN 55 014; EN 60 555.

CE – DECLARATION OF CONFIRMITY

We declare under our sole responsibility that this product corresponds to the

regulations 89 / 336 EEC; 89 / 392 EEC and 73 / 23 EEC and conforms with the

standards or standardized documents:

EN 61 010; EN 50 082; EN 55 014; EN 60 555.

DÉCLARATION DE CONFORMITÉ CE

Nous déclarons sous notre responsabilité que se prodiut est conforme aux

réglementations 89 / 336 CEE; 89 / 392 CEE et 73 / 23 CEE et en conformité avec

les normes ou documents normalisés suivant:

EN 61 010; EN 50 082; EN 55 014; EN 60 555.

DECLARACION DE CONFORMIDAD DE CE

Declaramos por nuestra responsabilidad propia que este produkto corresponde

alas directrices 89 / 336 CEE; 89 / 392 CEE y 73 / 23 CEE y que cumple las normas

odocumentos normativos siguientes:

EN 61 010; EN 50 082; EN 55 014; EN 60 555.

CE – DICHIARAZIONE DI CONFORMITÀ

Dichiariamo, assumendone la piena responsabilità, che il prodotto è conforme alle

seguenti direttive CCE 89 / 336 ; CCE 89 / 392 e CCE 73 / 23, in accordo ai seguenti

regolamenti e documenti:

EN 61 010; EN 50 082; EN 55 014; EN 60 555.

IKA®-LABORTECHNIK Janke & Kunkel GmbH & Co. KG

Staufen, November 2005

DE

EN

FR

ES

IT

6IKA®-WERKE C 200 Ver. 02/2.06

Safety precautions1

Calorimeter system C 200 may only be used to determine the calorific value of solid and

fluid materials. Only the appropriate original IKA®decomposition vessels may be used

for this purpose. For detailed information, please see the operating instructions for the

decomposition vessels.

The maximum extra energy added to the decomposition vessel must not exceed 40,000 J

(select the test mass accordingly). The permitted operating pressure of 230 bar must not

be exceeded. The maximum permitted operating temperature must not exceed 50°C.

Do not overfill the decomposition vessel with sample. Only fill the decomposition vessel

with oxygen to a maximum pressure of 40 bar. Check the set pressure on the pressure

reducer. Perform a leakage test before each combustion process (follow operating

instructions for decomposition vessel!).

Some materials tend to explode when combusted (e.g. due to formation of peroxide),

which could cause the decomposition vessel to crack.

Standarddecomposition vessels may not be used for testing explosive samples.

If the burning behaviour of a material is unknown, it must be tested before combustion

in the decomposition vessel (risk of explosion). If you are burning unknown samples,

leave the room or keep your distance from the calorimeter.

Benzoic acid may only be combusted in its pressed form! Flammable dust and powder

must be first pressed. Oven-dry dust and powder such as splints, hay, straw etc. explode

when combusted! Always wet these materials first! Highly flammable liquids with a low

vapour pressure(e.g. tetramethyl dihydrogen disiloxane) must not directly touch the

cotton thread!

Furthermore, toxic combustion residue in the form of gases, ashes or condensation, for

example, is possible in the inner wall of the decomposition vessel.

Please observe the accident prevention regulations applicable for the activity and the

workstation. Wear your personal protective equipment.

When handling combustion samples, combustion residue and auxiliary materials, please

observe the relevant safety regulations.

The following materials, for example, could pose a risk:

– corrosive

– highly flammable

– explosive

– bacteriologically contaminated

– toxic

7

Please observe the relevant regulations when handling oxygen.

Warning: oxygen as a compressed gas is oxidising; intensively aids combustion; can

react violently with flammable materials.

Do not use oil or grease!

Caution - magnetism! Beware of effects from the magnetic field (pacemakers, data media

etc.).

When using stainless steel crucibles thoroughly check their condition after each experi-

ment. If the material gets thinner, the crucible may catch fire and damage the decomposi-

tion vessel. Crucibles must not be used for more than 25 combustions for safety reasons.

The decomposition vessel is manufactured in accordance with the directive for pressure

equipment 97/23/EC. This is indicated by the CE symbol with the ID number of the noti-

fied body. The decomposition vessel is a category III pressure device. The decomposition

vessel has undergone an EC prototype test. The CE declaration of conformity confirms

that this decomposition vessel corresponds to the pressure device described in the EC

prototype test certificate. The decomposition vessel has undergone a pressure test with

the test pressure of 330 bar and a leakage test with oxygen at 30 bar.

Decomposition vessels areexperiment autoclaves and must be tested by a technical

expert after each use.

Individual use is understood here to include a series of experiments performed under

roughly the same conditions in terms of pressure and temperature. Experiment autocla-

ves must be operated in special chambers (C 2000, C 5000, C 7000, C 200).

The decomposition vessels must undergo repeated tests (internal tests and pressure

tests) performed by the technical expert.The frequency of these tests is to be determi-

ned by the operator on the basis of experience, type of operation and the material used

in the decomposition vessel

The declaration of conformity becomes invalid if mechanical modifications are carried

out to the experiment autoclaves or if tightness can no longer be guaranteed as a result

of major corrosion (e.g. pitting by halogens).

The threads on the body of the decomposition vessel and the union nut are subject to

considerable stress in particular and must therefore be checked regularly for wear.

The condition and function of the seals must be checked and ensured by way of a leaka-

ge test (see operating instructions for decomposition vessel!).

Only technical experts may perform pressure tests and service work on the decomposi-

tion vessel

We recommend that you send the decomposition vessel to our factory for inspection,

and if necessary, repair after 1000 tests or after one year or sooner depending on use.

IKA®-WERKE C 200 Ver. 02/2.06

8IKA®-WERKE C 200 Ver. 02/2.06

For the purposes of these operating instructions a technical expert is someone

1. who guarantees to conduct the tests properly on the basis of his training, knowledge

and experience gained through practical work,

2. who is sufficiently reliable,

3. who is not subject to any instructions in terms of the test activity

4. who has suitable test equipment if necessary

5. who can provide appropriate proof of the requirements listed in 1

National directives and laws must be observed for operating pressure vessels!

Anyone operating a pressure vessel must keep it in a proper condition, operate it proper-

ly, supervise it, carry out the necessary maintenance and repair work immediately and

implement the safety measures required in the circumstances.

Pressure vessels must not be used if they have defects which could pose a risk to staff or

third parties. The pressure equipment directive can be obtained from Carl Heymanns or

Beuth publishers.

9

User information2

This symbol indicates information which is essential for the safety of your

health.Failure to observe this information can cause damage to health and

injuries.

This symbol indicates information which is important for ensuring that the

appliance functions without any technical problems.Failure to observe

this information could damage the calorimeter system.

This symbol indicates information which is important for ensuring that

calorimetric measurements are performed efficiently and for using the

calorimeter system. Failure to observe this information can result in inac-

curate measurements.

This symbol indicates references to the optimization of operatinal sequen-

ces are characterized.

Numbers ➀,➁,➂etc. indicate guidelines in the following sections which must always

be carried out in order.

You have purchased an original IKA®product, manufactured to the latest, highest quality

standards. According to IKA®'s conditions of warranty, this product is guaranteed for

12 months. Toensure the long-term precision and function of the calorimeter system,

we recommend that you conclude a maintenance agreement (annual maintenance) with

IKA®or an authorised IKA®workshop. If the first maintenance is carried out within

12 months of purchase, the warranty will be extended to 24 months.

In the case of a warranty claim, please contact the responsible representative or the sup-

plier. You can also returnthe appliance directly to IKA®-WERKE.

Please enclose the sales invoice and the reason for the claim and state the name of the

contact person at your company. Freight charges are to be paid by the sender.

Please read these operating instructions carefully.

IKA®-WERKE only consider themselves to be responsible for the safety, reliability and

performance of the appliance when

•the appliance has been operated in accordance with the operating instructions,

•only persons authorised by the manufacturer interferewith the appliance,

•only original parts and original accessories areused for repairs

IKA®-WERKE do not accept liability for damage or costs resulting from accidents, misuse

of the appliance or unauthorised changes, repairs or upgrades.

2.1 Information regarding operating instructions

2.2 Warranty and liability

IKA®-WERKE C 200 Ver. 02/2.06

TIPP

10

Transport, storage, place of installation3

The system must be protected against mechanical impact, vibrations, dust deposits and

corrosive ambient air during transportation and storage.

It is also important to ensure that the relative humidity does not exceed 80%.

Only the original packing may be used for transportation.

The appliance must be completely emptied before storing and transportation.

Please observe the respective country-specific regulations for operating pressure equip-

ment when installing the appliance.

Aconstant ambient temperature is an important requirement for ensuring the high mea-

suring accuracy of the system. The following conditions must therefore be fulfilled at the

place of installation:

•No direct solar radiation

•No draughts (e.g. beside windows, doors, air conditioning)

•Sufficient distance to radiators and other heat sources

•The (constant) room temperature should be around 20 °C ... 25 °C.

•The system must be installed on a level surface.

•An adequate power supply corresponding to the nameplates on the system compo-

nents.

•Oxygen supply (99.95 % pure oxygen, quality 3.5; pressure 30 bar) with pressure

display and shut-off device. (C29 reducing valve, accessories)

Please unpack the system components carefully and check for any damage. When you

unpack the equipment, check for any damages which may have occurred during trans-

portation. Make a note of any damage and reportit immediately (post, railway, shipping

company).

3.1 Conditions of transport and storage

3.2 Place of installation

3.3 Unpacking

IKA®-WERKE C 200 Ver. 02/2.06

11

1xbasic device C 200

1xdecomposition vessel C 5010

1xignition adaptor

1xattachment set

1xtable power supply

1xplug

1xoperating instructions

1xwater emptying hose (length: 1 m)

1xoxygen station C 248

1xmeasuring cup (2 l)

3.4 Contents C 200

IKA®-WERKE C 200 Ver. 02/2.06