Peak Scientific Precision 500 Bedienungsanleitung

Precision 500 230v

Hydrogen Generator

User Manual

2012 © Peak Scientific – Rev 2 – 07/11/12

Precision 500 User Manual

Page 2 2012 © Peak Scientific – Rev 2 – 07/11/12

Contents

Change History 3

How to use this Manual 3

Introduction 4

Warranties and Liabilities 5

Safety Notices 6

Symbols 6

Safety Notice to Users 6

Declaration of Conformity 8

Environmental Declaration 9

Technical Specification 10

Environment 10

Generator Outlets 10

Electrical Requirements 10

General 10

Principle of Operation 11

General Safety 12

Generator Safety Features 13

Unpacking & Contents 14

Unpacking Instructions 14

Installation 15

Unpacking 16

General Dimensions 17

Unit Controls 18

Rear Connections 18

Tubing 19

H2 Ventilation 19

Fittings Kit 19

Automatic Filling 20

Electrical Connection 21

Start-up Sequence 22

Liquid Leak Detectors 22

H2Detector Option 23

Gas Traps 24

Expanding Capacity 25

Rear Connections 25

Supply Line Tubing 26

Switching the unit off 27

Cleaning 27

Replacement of Deioniser Resin Column 28

Refilling the Deioniser Resin Column 29

Health and Safety Data- Deioniser Resin 30

IMPORTANT DOCUMENT

Service Requirements 33

Trouble Shooting 34

Precision 500 User Manual

Page 3 2012 © Peak Scientific – Rev 2 – 07/11/12

Change History

Rev.

Comment

Name

Date

Altered D.O.C.

Liam Couttie

17/09/12

Fittings Kit Additions

Liam Couttie

07/11/12

How to use this Manual

This manual is intended for end users and has been written so that it can either

be read as a step by step guide to installation and usage or as a reference

document where you can skip to the relevant information.

Users of a hard copy version can refer to the contents page to find the relevant

information. Users of the soft copy version can use the hyperlinks from the

contents page as well as the hyperlinks between sections.

Please review each of the following sections carefully.

Thank you for selecting Peak Scientific to meet your Gas Generation needs, and

should you require any further assistance or support please do not hesitate to

contact Peak Scientific or Peak Partner from which you purchased your

Generator.

Precision 500 User Manual

Page 4 2012 © Peak Scientific – Rev 2 – 07/11/12

Introduction

The Precision 500 has been developed to cater for the requirements of GCMS

instruments.

This model provides a source of High Purity Hydrogen gas.

Other features include:

•Touch screen interface

•>99.9999% purity

•Robust dryer technology

•Expandable; Inter-connectable generators for increased capacity.

With the Precision 500 based on proven technology, it produces Hydrogen by

electrolysis using a Proton exchange membrane (PEM) cell. Moisture removal is

achieved by a pressure swing adsorption process, using molecular sieve.

To ensure this Generator model meets our high expectations with regards to

reliability and performance, we have tested this model extensively at our

manufacturing plant to ensure reliability and longevity of the system.

Precision 500 User Manual

Page 5 2012 © Peak Scientific – Rev 2 – 07/11/12

Warranties and Liabilities

1. The Company warrants that it has title to the Goods.

2. Subject to the provisions of this clause the Company warrants that the

Goods shall comply in all material respects with any specification

referred to in the Order Confirmation (as the same may be amended)

and shall, subject thereto, be free from defects in material and

workmanship for the lesser of a period of twelve months from the date

of delivery or thirteen months from the date of dispatch from the

factory.

3. Save as provided in this clause and except where the Goods are sold to

a person dealing as a consumer (within the meaning of the Unfair

Contract Terms Act 1977) all warranties, conditions or other terms

implied by statute or common law are hereby expressly excluded save

to the extent they may not be lawfully excluded. When the Goods are

sold to a consumer within the meaning of the Unfair Contract Terms Act

1977 their statutory rights are not affected by the provisions of this

clause.

4. In the event of the Customer making a claim in respect of any defect in

terms of clause 2 hereof the Customer must.

1. Reasonably satisfy the Company that the Goods have been

properly installed, commissioned, stored, serviced and used and

without prejudice to the generality of the foregoing that any

defect is not the direct or indirect result of lack of repair and/or

servicing, incorrect repair and/or servicing, use of wrong

materials and/or incorrect spare parts

2. Allow the company to inspect the Goods and/or any installation

and any relevant packaging as and when reasonably required by

the Company.

5. Subject to the Company being notified of any defect as is referred to in

sub-clause 2 hereof within a reasonable time of it becoming apparent

and subject always to the terms of sub-clause 4 hereof, the Company

shall, in its option, replace or repair the defective Goods or refund a

proportionate part of the Price. The Company shall have no further

liability to the Customer (save as mentioned in sub-clause 6 hereof).

6. The Company shall be liable to indemnify the Customer in respect of

any claim for death or personal injury to any person in so far as such is

attributable to the negligence or breach of duty of the Company or any

failure by the Company to comply with the provisions of sub-clause 2

hereof.

7. Save as provided in sub-clause 2 hereof the Company shall not be liable

in respect of any claim by the Customer for costs, damages, loss or

expenses (whether direct, indirect, consequential or otherwise) or

indemnity in any respect howsoever arising including, but not by way of

limitation, liability arising in negligence (other than pursuant to clause 6

above) that may be suffered by the Customer or any third party.

Precision 500 User Manual

Page 6 2012 © Peak Scientific – Rev 2 – 07/11/12

Safety Notices

Symbols

This manual uses the following symbols to highlight specific areas important to

the safe and proper use of the Generator

Safety Notice to Users

These instructions must be read thoroughly and understood

before installation and operation of your Peak Precision 500

Hydrogen Generator. Use of the Generator in a manner not

specified by Peak Scientific MAY impair the SAFETY provided

by the equipment.

When handling, operating or carrying out any maintenance,

personnel must employ safe engineering practices and

observe all relevant local health and safety requirements and

regulations. The attention of UK users is drawn to the Health

and Safety at Work Act 1974, and the Institute of Electrical

Engineers regulations.

If the equipment is used in a manner not specified by the

manufacturer, the protection provided by the equipment

maybe impaired.

WARNING

notice denotes a hazard. It calls attention to an operating procedure,

process or similar, which if not correctly performed or adhered to, could cause

personal injury or in the worst case death. Do not proceed beyond a WARNING notice

until the indicated conditions are fully understood or met.

A CAUTION notice denotes a hazard. It calls attention to an operating procedure,

process or similar, which if not correctly performed or adhered to, could cause damage

to the Generator or the Application. Do not proceed beyond a CAUTION notice until

the indicated conditions are fully understood or met.

Caution, risk of electric shock. Ensure power to the Generator has been removed

before proceeding.

Precision 500 User Manual

Page 7 2012 © Peak Scientific – Rev 2 – 07/11/12

ATTENTION - IMPORTANT NOTICE TO ALL USERS

These instructions must be read thoroughly, section by section and understood

before installation and operation of your Peak Scientific Hydrogen Generator.

Please follow the appropriate safety standards for handling hydrogen gas and

other gases as determined by the laws and regulations of your country.

Please save the product packaging for storage or future shipment of the

generator.

1. For your own personal safety and to prevent accidental damage to your

generator please ensure that you read and understand our Directions

for Use Manual.

2. Do not store away the generator when not in operation. The generator

should be powered up at least twice a month and a small flow taken for

1 hour. It is recommended that you replace the water monthly to

prevent biological growth developing in the tank and tubing. Failure to

do this will greatly reduce the life of the generator and render the

warranty void.

3. Do not place the external water bottle above the height of the

generator. The bottle may be placed at the same level or below the

generator.

4. Use only high grade de-ionised water (1µS/cm or better). Do not

attempt to connect pressurised water to the generator.

5. It is recommended that you operate the generator at the lowest

pressure permissible for your particular application. Do not

automatically set the pressure to maximum if not required.

6. Failure to maintain the Deioniser Column as recommended will reduce

the operational life of your generator and render its warranty void.

7. Do not attach any additional tanks or gas cylinders to your generator

without first consulting Peak Scientific.

8. Ensure your entire installation, both pipe work and analysers, are

completely gas tight. Even minor leaks will affect the operation of your

generator and generally reduce its operational life.

9. Has your generator been correctly sized for your application? If in

doubt, consult your dealer or Peak Scientific.

10. Ensure the ambient temperature inside your laboratory does not rise

above 25°C/77°F. Extremes of operating temperature will reduce cell

life.

Precision 500 User Manual

Page 8 2012 © Peak Scientific – Rev 2 – 07/11/12

Declaration of Conformity

We Peak Scientific Instruments Ltd.

of Fountain Crescent, Inchinnan. Renfrewshire PA4 9RE

declare that:

Equipment Hydrogen Gas Generator

Model Precision 500

To which this declaration relates, is in conformity with the applicable EC Directives,

harmonized standards, and other normative requirements.

•Low Voltage Directive 2006/95/EC

EN 61010-1: 2010

Safety Requirements for Electrical Equipment for Measurement, Control and

Laboratory Use.

Part 1: General requirements.

•Electromagnetic Compatibility Directive 2004/108/EC

EN 61326-1: 2006

Electrical Equipment for Measurement, Control and Laboratory Use – EMC

Requirements.

Part 1: General requirements.

All evaluation, testing and certification issued by:

York EMC Services (2007) Ltd

Donibristle Industrial Park

Dunfermline

Fife

KY11 9HZ

Signed By:

Name: Chris Pugh

Position: Engineering Director

Done at: Peak Scientific Instruments Ltd, Inchinnan, Scotland.

Date: 2nd August 2012

Precision 500 User Manual

Page 9 2012 © Peak Scientific – Rev 2 – 07/11/12

Environmental Declaration

We Peak Scientific Instruments Ltd.

of Fountain Crescent, Inchinnan. Renfrewshire PA4 9RE

declare that:

Equipment Hydrogen Gas Generator

Model Precision 500

Is fully compliant with the following Directives:

2002/96/EC WEEE (Waste of Electrical and Electronic Equipment)

2002/95/EC RoHS (Restriction of Hazardous Substances)

Peak Scientific Instruments Ltd fully complies with its obligations towards the

European WEEE (Waste of Electrical and Electronic Equipment) Directive

2002/96/EC. These obligations are being met within the B2B compliance

group.

Peak Scientific Instruments Ltd has developed all reasonable ‘due diligence’

controls to ensure that our products comply with the principles and

requirements of the European RoHS (Restriction of Hazardous Substances)

Directive 2002/95/EC. Similar directives in the United States and China, for

example, have also been captured within this program.

Where a specific certificate of compliance is required, this can be requested, on

a product serial number basis, directly from Peak Scientific Instruments Ltd, by

contacting us through our website on www.peakscientific.com

Signed By:

Name: Chris Pugh

Position: Engineering Director

Done at: Peak Scientific Instruments Ltd, Inchinnan, Scotland.

Date: 2nd August 2012

Precision 500 User Manual

Page 10 2012 © Peak Scientific – Rev 2 – 07/11/12

Technical Specification

Environment

Minimum operating ambient temperature

10°C (50°F)

Maximum operating ambient temperature 25°C (77°F)

Maximum relative humidity 90% Non-Condensing

Minimum storage temperature*

10oC (50oF)

Maximum storage temperature* 25

C (77

*NOTE – When taken out of storage the Generator should be allowed to acclimatize at

room temperature for a minimum of 3 hours before operation.

Generator Outlets

Max Flow Rate 500 cc/min

Purity 99.9999%

Gas outlet

1 x 1/8” Swagelok compression fitting

Delivery pressure

0-100 psi (0-6.9 bar)

Electrical Requirements

Voltage 230V

Frequency

50/60 Hz

Fuse T10AH250V

Current

10 Amps

Input connection C14 Connection

Power cord (Supplied) C13 socket to local connection (10A minimum)

Pollution degree

Insulation category II

General

Generator dimensions in cm W x D x H 38 x 55.3 x 48.4 (14.9” x 21.7” x 19.1”)

Generator weight

55 kg (121 lb)

Shipping crate dimensions in cm W x D x H 55 x 80 x 68 (21.6” x 31.4” x 26.7”)

Shipping weight

66 kg (145 lb)

Water purity requirement <1.0µ Siemens/cm OR >1 Mohm-cm

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