PerkinElmer STA 8000 Montageanleitung
STA 8000
Installation and Hardware
Guide
THERMAL ANALYSIS
Release History
Part Number Release Publication Date
09931395 B March 2018
Any comments about the documentation for this product should be addressed to:
User Assistance
PerkinElmer, Inc.
710 Bridgeport Avenue
Shelton, Connecticut 06484-4794
U.S.A.
Or email http://www.perkinelmer.com/contactus/
Notices
The information contained in this Help file is subject to change without notice.
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warranty of any kind with regard to this Help file, including, but not limited to, the implied
warranties of merchantability and fitness for a particular purpose.
PerkinElmer shall not be liable for errors contained herein for incidental consequential damages in
connection with furnishing, performance or use of this material.
Copyright Information
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Copyright © 2018 PerkinElmer, Inc.
Trademarks
Registered names, trademarks, etc. used in this Help file, even when not specifically marked as such,
are protected by law.
PerkinElmer is a registered trademark of PerkinElmer, Inc.
Pyris is a trademark of PerkinElmer, Inc.
Microsoft and Windows are registered trademarks of Microsoft Corporation in the United States and
other countries.
Contents
Introduction...............................................................................................7
Pyris Installation ............................................................................................... 8
Safety and Regulatory Information...........................................................9
Symbols Used in this Help.................................................................................10
Notes, Cautions and Warnings....................................................................10
Symbols Used on the Instruments.....................................................................13
Electrical Warnings...........................................................................................14
Electromagnetic Compatibility (EMC) .................................................................16
Europe......................................................................................................16
South Korea..............................................................................................16
United States (FCC)...................................................................................16
Electrical Safety ...............................................................................................17
WEEE Instructions for PerkinElmer Products ......................................................18
Prepare the Laboratory............................................................................21
Prepare the Laboratory.....................................................................................22
Electrical Requirements..............................................................................22
Environmental Requirements......................................................................22
Purge Gas and Pneumatic Supply ...............................................................23
Space Requirements..................................................................................23
Install Multiple Analyzers ........................................................................25
Install Multiple Analyzers ..................................................................................26
Install an STA 8000..................................................................................29
Safety Precautions for the STA 8000 .................................................................30
Important Specifications ............................................................................32
Decontamination and Cleaning..........................................................................33
Decontamination .......................................................................................33
Cleaning the Instrument ............................................................................33
General Laboratory Safety..........................................................................33
STA 8000 Warning Labels.................................................................................34
Warning Labels on the Upper Ring Around the Furnace................................34
Warning Labels on the Back of the STA 8000 ..............................................35
Installing an STA 8000 .....................................................................................37
Unpacking the STA 8000 ..................................................................................38
Set Up the STA 8000 System Components.........................................................40
Connect the Purge Gas Supply to the STA 8000...........................................40
Connect the Purge Gas and System Purge Gas Lines to the STA 8000...........41
Removal of the Shipping/Alignment Tool.....................................................42
Install the Sensor ......................................................................................42
Connect the Cooling Device to the STA 8000...............................................44
Connect the STA 8000 Components ..................................................................48
Configure the STA 8000....................................................................................49
Calibration of the STA 8000 ..............................................................................51
Weight Calibration.....................................................................................51
Weight Verification ....................................................................................51
DTA Baseline Optimization .........................................................................52
TG Drift Optimization.................................................................................52
Temperature and Heat Flow Verification......................................................52
STA 8000 Hardware .................................................................................55
STA 8000 Hardware Overview...........................................................................56
Sample Handling..............................................................................................57
Sample Preparation ...................................................................................57
Sample Pans .............................................................................................58
Sample Atmosphere...................................................................................58
Loading Samples into the STA 8000............................................................59
Heating ...........................................................................................................60
STA 8000 Maintenance.....................................................................................61
Cleaning the Furnace and Sensor...............................................................61
Cleaning the Cover....................................................................................61
STA 8000 Part Numbers...................................................................................62
Introduction
8 . STA 8000 Installation and Hardware Guide
Pyris Installation
NOTE: If you are going to install multiple analyzers, or just want to install a universal serial
bus, see
Install Multiple Analyzers
before you begin to install an analyzer.
This user’s guide gives information on the installation of your PerkinElmer Thermal Analysis
System, and details about the operation and maintenance of the hardware. This information
can also be found in the Pyris Installation and Hardware Help provided with your Pyris
software.
Information on the operation of the Pyris software can be found in the software Help.
In general, the installation procedure consists of the following steps:
•Prepare the laboratory
•Unpack the thermal analysis system
•Set up the required system components (for example, purge gases, cooling supply, and
analyzer-specific items)
•Connect the system components
•Configure the analyzer
•Calibrate the analyzer
Safety and Regulatory
Information
10 . STA 8000 Installation and Hardware Guide
Symbols Used in this Help
Bold text refers to text that is displayed on the screen.
UPPERCASE text, for example ENTER or ALT, refers to keys on the computer keyboard. '+' is
used to show that you have to press two keys at the same time, for example, ALT+F.
All eight-digit numbers are PerkinElmer part numbers unless stated otherwise.
Notes, Cautions and Warnings
Three terms, in the following standard formats, are also used to highlight special
circumstances and warnings.
NOTE: Anote indicates additional, significant information that is provided with some
procedures.
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