PerkinElmer Lambda 25 Bedienungsanleitung
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SM
View
Instra
Lambda 25, 35, 45
User’s Guide
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Release History
Part Number Release Publication Date
09934422 A August 2000
B September 2000
User Assistance
PerkinElmer Ltd
Post Office Lane
Beaconsfield
Buckinghamshire
HP9 1QA
Printed in the United Kingdom.
Notices
The information contained in this document is subject to change without notice.
PerkinElmer makes no warranty of any kind with regard to the material, including, but not
limited to, the implied warranties of merchantability and fitness for a particular purpose.
PerkinElmer shall not be liable for errors contained herein for incidental consequential
damages in connection with furnishing, performance or use of this material.
Copyright Information
This document contains proprietary information that is protected by copyright.
All rights are reserved. No part of this publication may be reproduced in any form
whatsoever or translated into any language without the prior, written permission of
PerkinElmer, Inc.
Copyright © 2000 PerkinElmer, Inc.
Trademarks
Registered names, trademarks, etc. used in this document, even when not specifically marked
as such, are protected by law.
UV WinLab is a trademark of PerkinElmer, Inc.
PerkinElmer is a registered trademark of PerkinElmer, Inc.
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Contents
3
Contents
Contents.......................................................................................................... 3
Warnings and Safety Information .............................................................. 7
Safety Information.......................................................................................... 9
Safety Information in the Handbook ....................................................... 9
IEC 61010 Compliance ........................................................................... 9
CSA Compliance..................................................................................... 9
Electrical Protection ................................................................................ 9
Electrical Safety..................................................................................... 10
EMC Compliance ......................................................................................... 13
EC Directive .......................................................................................... 13
FCC rules and regulations ..................................................................... 13
Environment ................................................................................................. 14
Lifting the Lambda 25, 35, 45 ...................................................................... 17
Labels............................................................................................................ 18
Introduction ................................................................................................ 21
About this Manual ........................................................................................ 23
Conventions Used in this Manual................................................................. 24
Definitions ............................................................................................. 24
Notes, cautions and warnings ................................................................ 24
Other Warnings used in this Manual ..................................................... 27
System Description ..................................................................................... 35
Introduction .................................................................................................. 37
Features ................................................................................................. 37
Optical System of the Lambda 25, 35, 45..................................................... 38
Lambda 25 Specification .............................................................................. 41
General .................................................................................................. 41
Optics..................................................................................................... 42
Abscissa................................................................................................. 42
Ordinate ................................................................................................. 43
Data Output ........................................................................................... 44
Lambda 35 Specification .............................................................................. 45
General .................................................................................................. 45
Optics..................................................................................................... 46
Abscissa................................................................................................. 46
Ordinate ................................................................................................. 47
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Lambda 25, 35, 45 User’s Guide
4
Lambda 45 Specification .............................................................................. 49
General .................................................................................................. 49
Optics..................................................................................................... 50
Abscissa................................................................................................. 50
Ordinate ................................................................................................. 51
Data Output ........................................................................................... 52
Installation................................................................................................... 53
Preparing the Working Area......................................................................... 55
Equipment Provided ..................................................................................... 57
Spectrometer.......................................................................................... 57
Components........................................................................................... 57
Unpacking your Instrument .......................................................................... 58
Unpacking and Inspection ..................................................................... 58
Connecting to the Electrical Supply ............................................................. 59
Setting up the PC .......................................................................................... 60
Connecting the PC to the spectrometer ................................................. 60
Installing UV WinLab ........................................................................... 60
Startup and Shutdown................................................................................... 61
Startup ................................................................................................... 61
Shutdown............................................................................................... 62
Installing the Single Cell Holder .................................................................. 63
Description ............................................................................................ 63
Accessories................................................................................................... 71
Accessory Installation................................................................................... 73
Accessory Connector Panel ................................................................... 74
Accessory Connections Overview......................................................... 76
Sample Compartment Cover ................................................................. 76
Sample Compartment Front Cover........................................................ 77
Sample Compartment Window ............................................................. 77
Linear Transporter ........................................................................................ 78
Installation Overview ............................................................................ 78
Temperature Sensor...................................................................................... 79
Installation Overview ............................................................................ 79
Multisippers .................................................................................................. 80
Installation Overview ............................................................................ 80
Autosampler .......................................................................................... 81
Operating with Accessories .......................................................................... 82
General .................................................................................................. 82
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Contents
5
Accessories............................................................................................ 82
Requirements for Operation with Accessories ...................................... 83
Maintenance ................................................................................................ 85
Maintenance.................................................................................................. 87
Obtaining Service .................................................................................. 87
Daily Care.............................................................................................. 87
Cleaning the Sample Compartment....................................................... 88
Use and Care of Cells ................................................................................... 90
Cell Handling......................................................................................... 90
Pressure Buildup in Cells ...................................................................... 91
Replacing a Lamp......................................................................................... 92
Halogen Lamp Replacement ................................................................. 93
Deuterium Lamp Replacement.............................................................. 96
Lamp Energy Attenuator ....................................................................... 99
Lamp Alignment Procedure................................................................. 101
Changing Fuses........................................................................................... 102
Replacement Parts ...................................................................................... 104
Analytical Notes ........................................................................................ 105
Unusual Samples ........................................................................................ 107
Volatile Samples.................................................................................. 107
Samples not Governed by the Beer-Lambert Law .............................. 107
Chemically Reactive Samples ............................................................. 108
Photoactive Samples............................................................................ 108
Other Sample Properties...................................................................... 108
Solvent Properties....................................................................................... 109
Index .......................................................................................................... 111
Index ........................................................................................................... 113
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Lambda 25, 35, 45 User’s Guide
6
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Warnings and
Safety Information 1
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Artisan Technology Group - Quality Instrumentation ... Guaranteed | (888) 88-SOURCE | www.artisantg.com
Warnings and Safety Information
9
Safety Information
Safety Information in the Handbook
This handbook contains information and warnings that must be followed by the user
to ensure safe operation and to maintain the instrument in a safe condition.
Possible hazards that could harm the user or result in damage to the instrument are
clearly stated at appropriate places throughout this handbook.
Before using the instrument it is essential to read the manual carefully and to pay
particular attention to any advice concerning potential hazards that may arise from
the use of the instrument. The advice is intended to supplement, not supercede the
normal safety code of behavior prevailing in the user’s country.
IEC 61010 Compliance
This instrument has been designed and tested in accordance with IEC 1010-1: Safety
requirements for electrical equipment for measurement, control, and laboratory use,
and Amendment 1 to this standard.
CSA Compliance
This instrument meets the Canadian Standards Association (CSA) Standard
CAN/CSA-C22.2-1010.1: Safety Requirements for Electrical Equipment for
Measurement, Control, and Laboratory Use – General Requirements.
Electrical Protection
Insulation: Class I as defined in IEC 61010-1.
Installation Category: The instruments are able to withstand transient overvoltage
according to Installation Category II as defined in IEC 61010-1 and IEC 664.
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Dieses Handbuch passt für folgende Modelle
2
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