PerkinElmer Lambda 465 Bedienungsanleitung

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PerkinElmer, 710 Bridgeport Avenue,

Shelton, CT 06484-4794, U.S.A

Produced in the USA.

Lambda 465 Fiber Optic Probe Installation Instructions

This instruction sheet describes the installation of this accessory which is used with the Lambda 465

Spectrophotometer.

NOTE:

Read these instructions before you install this accessory.

Contacting PerkinElmer

Supplies, replacement parts, and accessories can be ordered directly from PerkinElmer, using the part

numbers.

See our website:

http://perkinelmer.com

PerkinElmer's catalog service offers a full selection of high-quality supplies.

To place an order for supplies and many replacement parts, request a free catalog, or ask for information:

If you are located within the U.S., call toll free 1-800-762-4002, 8 a.m. to 8 p.m. EST. Your order will be

shipped promptly, usually within 24 hours.

If you are located outside of the U.S., call your local PerkinElmer sales or service office.

Introduction

The probes provide a convenient way of performing absorption or transmission measurements by dipping

or inserting the probe end into the medium or environment. This accessory is especially useful for

embedding into process streams for real-time, on-line sample monitoring.

Features

•Easy to install

•Dip Probe for measuring liquid samples without using a cell

Figure 1 Lambda 465 Fiber Optic Probe [P/N: N4104012]

with Fiber Optic Probe [Part No: N4101048]

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Dimensions and Specifications

Physical Characteristic Specification

Fiber Optic Probe

A: Fiber Type Fused Silica

B: Fiber Size 600 µm

C: Connector SMA 905

D: PVC Jacket ∅0.19’’ OD

E: Path Length 10 mm

Spectral Range 200 nm ~ 1100 nm

Overall Length (OAL) 100 ~ 120 cm

Breakout Length (BOL) 18 ~ 23cm

Probe Length (PL) 15.2 cm

Fiber Coupling Mount Dimension (mm) 150(W) X 100(H) X 84(L)

Weight (Kg) 0.75

Description

Configuration of the Fiber Optic Probe

Figure 2 Lambda 465 Fiber Optic Probe include Fiber Coupling mount

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Installation

1. Disassemble the existing cell holder.

Figure 3 Location of the two knob bolts

2. Install the fiber optic probe by fastening the knob bolts.

Figure 4 Installing the fiber Optic probe

3. Connect the communication cable and the power cord, and then turn on the power of the Lambda

465.

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4. Place the probe into the liquid sample.

Figure 5 Placing the probe in the liquid

Measurement

NOTE:

Start the sample measurement after warming up at least 20 minutes.

1. Launch the UV Lab software.

2. Choose the Fiber Module in the Accessory Type.

3. After dipping the probe into the blank solution, select the intensity mode, and then click Blank. By

changing the Integration no. up to 30000, adjust the D2 peak intensity not to be saturated in the

spectrum as shown in the picture below.

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4. Select the Absorbance mode and measure blank and sample.

Before measurement, make sure that bubble does not exist at the mirror side of the probe.

5. Clean the probe with D.I water after the measurement.

Troubleshooting

When the Intensity value is low

1. Make sure that bubble does not exist at the mirror side of the probe.

If bubbles existed, the intensity of the light is low due to scattering of bubbles. You should remove

the bubbles completely and perform measuring.

2. Increase the Integration Number in the UV Lab Software

You should increase the Integration Number since the intensity of the light which passes through the

fiber is somewhat weak.

3. Check the condition of the fiber optic probe

Check if the lens placed inside the fiber optic probe is contaminated.

Remove the contaminant with alcohol.

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