TABLE OF CONTENT
1Technical Specifications of the Titrator TitroLine® 5000................................... 81
1.1 Summary................................................................................................................................. 81
1.2 Specifications Titrator TitroLine®5000.................................................................................... 82
1.3 Warning and safety information .............................................................................................. 84
2Unpacking and First Operation ............................................................................ 85
2.1 Unpacking and First Operation of the titrator.......................................................................... 85
2.2 Connection and installing of Piston Burette and magnetic stirrer TM 50................................ 85
2.3 Connecting the Titrator - Combination with Accessories and Additional Devices .................. 86
2.3.1 Back panel of the titrator TitroLine® 5000 .............................................................................. 86
2.3.2 Connection ports of the TitroLine® 5000 . Connection of Electrodes..................................... 86
2.3.3Connecting a printer................................................................................................................ 86
2.3.4 Connecting a USB device (manual controller, keyboard, memory device, hub) .................... 86
2.3.5 Connection of analytical balances........................................................................................... 86
2.4 Setting the Language of the Country ...................................................................................... 87
2.5 Dosing unit and Accessories................................................................................................... 89
2.6 Initial Filling and Rinsing ......................................................................................................... 90
3Working with the Titrator TitroLine®5000 ........................................................... 92
3.1 Front Keyboard........................................................................................................................ 92
3.2 Display..................................................................................................................................... 92
3.3 Manual controller “mouse“ ...................................................................................................... 93
3.4 External PC Keyboard............................................................................................................. 93
3.5 Menu Structure........................................................................................................................ 94
3.6 Main Menu............................................................................................................................... 96
3.6.1 Automatic Titration .................................................................................................................. 96
3.6.2 Calibration (CAL menu)........................................................................................................... 98
3.6.3 Manual Titration..................................................................................................................... 101
3.6.4 Dosage.................................................................................................................................. 103
4Method Parameters ............................................................................................. 105
4.1 Method editing and new method........................................................................................... 105
4.2 Default methods .................................................................................................................... 106
4.3 Copy Methods....................................................................................................................... 106
4.4 Delete Methods ..................................................................................................................... 107
4.5 Print method.......................................................................................................................... 107
4.6 Change Method Parameters................................................................................................. 107
4.6.1 Method type........................................................................................................................... 108
4.6.2 Titration mode ....................................................................................................................... 108
4.6.3 Result .................................................................................................................................... 110
4.6.4 Titration parameters.............................................................................................................. 119
4.6.5 ‘End-point titration’ Titration parameters ............................................................................... 127
4.6.6 Dosing parameter.................................................................................................................. 128
4.6.7 Sample identification............................................................................................................. 129
4.6.8 Documentation ...................................................................................................................... 130
5System settings................................................................................................... 131
5.1Calibration settings................................................................................................................ 131
5.2 Reagents –Dosing unit......................................................................................................... 133
5.2.1 Replacing the dosing unit...................................................................................................... 133
5.2.2 Replacing the titration solution.............................................................................................. 138
5.3 Globale Memory.................................................................................................................... 138
5.4 RS232 Settings ..................................................................................................................... 139
5.5 Connection of Printers........................................................................................................... 141
5.6 Stirrer..................................................................................................................................... 142
5.7 Date and Time....................................................................................................................... 142
5.8 RESET .................................................................................................................................. 143
5.9 Device Information ................................................................................................................ 143
5.10 System Tone......................................................................................................................... 144
5.11 Data exchange...................................................................................................................... 144
5.12 Software Update.................................................................................................................... 146
