Agilent Technologies 1260 Infinity Bedienungsanleitung

Agilent Technologies

Agilent 1260 Infinity

Standard Autosampler

User Manual

Agilent 1260 Infinity Standard Autosampler User Manual

Notices

2010

No part of this manual may be reproduced

in any form or by any means (including elec-

tronic storage and retrieval or translation

into a foreign language) without prior agree-

ment and written consent from Agilent

Technologies, Inc. as governed by United

States and international copyright laws.

Manual Part Number

G1329-90013

Edition

06/10

Printed in Germany

Agilent Technologies

Hewlett-Packard-Strasse 8

76337 Waldbronn

This product may be used as a com-

ponent of an in vitro diagnostic sys-

tem if the system is registered with

the appropriate authorities and com-

plies with the relevant regulations.

Otherwise, it is intended only for gen-

eral laboratory use.

Warranty

The material contained in this docu-

ment is provided “as is,” and is sub-

ject to being changed, without notice,

in future editions. Further, to the max-

imum extent permitted by applicable

law, Agilent disclaims all warranties,

either express or implied, with regard

to this manual and any information

contained herein, including but not

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applicable in any technical data.

Safety Notices

CAUTION

A CAUTION notice denotes a

hazard. It calls attention to an

operating procedure, practice, or

the like that, if not correctly per-

formed or adhered to, could

result in damage to the product

or loss of important data. Do not

proceed beyond a CAUTION

notice until the indicated condi-

tions are fully understood and

met.

WARNING

A WARNING notice denotes a

hazard. It calls attention to an

operating procedure, practice,

or the like that, if not correctly

performed or adhered to, could

result in personal injury or

death. Do not proceed beyond a

WARNING notice until the indi-

cated conditions are fully under-

stood and met.

Agilent 1260 Infinity Standard Autosampler User Manual 3

In This Book

This manual covers the Agilent 1260 Infinity Standard Autosampler (G1329B).

1 Introduction to the Autosampler

This chapter gives an introduction to the autosampler, instrument overview

and internal connectors.

2 Site Requirements and Specifications

This chapter provides information on environmental requirements, physical

and performance specifications.

3 Installing the Autosampler

This chapter provides information on unpacking, checking on completeness,

stack considerations and installation of the module.

4 Using the Autosampler

This chapter provides information on how to set up the module for an analysis

and explains the basic settings.

5 Optimizing Performance

This chapter provides information on how to optimize the module.

6 Troubleshooting and Diagnostics

Overview about the troubleshooting and diagnostic features.

7 Error Information

This chapter describes the meaning of error messages, and provides

information on probable causes and suggested actions how to recover from

error conditions.

4 Agilent 1260 Infinity Standard Autosampler User Manual

In This Book

8 Maintenance

This chapter describes the maintenance of the module.

9 Parts and Materials for Maintenance

This chapter provides information on parts for maintenance.

10 Identifying Cables

This chapter provides information on cables used with the module.

11 Appendix

This chapter provides addition information on safety, legal and web.

Agilent 1260 Infinity Standard Autosampler User Manual 5

Contents

1 Introduction to the Autosampler 9

Introduction to the Autosampler 10

Early Maintenance Feedback (EMF) 20

Instrument Layout 21

Electrical Connections 22

Interfaces 24

Setting the 8-bit Configuration Switch (On-Board LAN) 30

2 Site Requirements and Specifications 39

Site Requirements 40

Physical Specifications 44

Performance Specifications Standard Autosampler 45

3 Installing the Autosampler 47

Unpacking the Autosampler 48

Optimizing the Stack Configuration 49

Installing the Autosampler 53

Installing the Thermostatted Autosampler 56

Flow Connections 60

Installing the Sample Tray 62

Transporting the Autosampler 63

4 Using the Autosampler 65

Sample Trays 66

List of Compatible Vials and Caps 68

5 Optimizing Performance 71

Optimization for Lowest Carry-over 72

Fast Injection Cycle and Low Delay Volume 75

Precise Injection Volume 77

Choice of Rotor Seal 79

6 Agilent 1260 Infinity Standard Autosampler User Manual

Contents

6 Troubleshooting and Diagnostics 81

Overview of the Sampler’s Indicators and Test Functions 82

Status Indicators 83

Maintenance Functions 85

Standard Autosampler Step Commands 92

Troubleshooting 94

Troubleshooting Guide for the Sample Transport Assembly 96

Agilent Lab Advisor Software 103

7 Error Information 105

What are Error Messages 107

General Error Messages 108

Autosampler Error Messages 115

8 Maintenance 125

Introduction into Maintenance and Repair 126

Maintenance Functions 129

Simple Repairs 130

9 Parts and Materials for Maintenance 147

Main Assemblies 148

Analytical-Head Assembly 150

Vial Trays 152

Standard Autosampler Accessory Kit G1329-68755 153

Maintenance Kit G1313-68719 153

Multi-Draw Kit 154

External Tray G1313-60004 154

Agilent 1260 Infinity Standard Autosampler User Manual 7

Contents

10 Identifying Cables 155

Cable Overview 156

Analog Cables 158

Remote Cables 160

BCD Cables 163

External Contact Cable 165

CAN/LAN Cables 166

Auxiliary Cable 167

RS-232 Cables 168

11 Appendix 169

General Safety Information 170

The Waste Electrical and Electronic Equipment (WEEE) Directive

(2002/96/EC) 173

Lithium Batteries Information 174

Radio Interference 175

Solvent Information 176

Sound Emission 178

Agilent Technologies on Internet 179

8 Agilent 1260 Infinity Standard Autosampler User Manual

Contents

Agilent 1260 Infinity Standard Autosampler User Manual

Agilent Technologies

Introduction to the Autosampler

Introduction to the Autosampler 10

Sampling Sequence 12

Sampling Unit 15

Transport Assembly 18

Early Maintenance Feedback (EMF) 20

Instrument Layout 21

Electrical Connections 22

Serial Number Information (ALL) 23

Electrical Connections 22

Interfaces 24

Overview Interfaces 26

Setting the 8-bit Configuration Switch (On-Board LAN) 30

Communication Settings for RS-232C 34

Special Settings 36

This chapter gives an introduction to the autosampler, instrument overview and

internal connectors.

10 Agilent 1260 Infinity Standard Autosampler User Manual

1Introduction to the Autosampler

Introduction to the Autosampler

Figure 1 Overview of the Autosampler

The Agilent 1260 Infinity autosamplers are designed for use with other

modules of the Agilent 1200 Infinity Series, 1200 Series and 1100 Series LC

system, or with other LC systems if adequate remote control inputs and

outputs are available. The autosamplerss are controlled by the Agilent control

module (G4208A Instant Pilot) or by Agilent control software (ChemStation

for LC, EZChrom Elite etc.).

Three sample-rack sizes are available for the autosamplers. The standard

full-size rack holds 100 × 1.8 mL vials, while the two half-size racks provide

space for 40 × 1.8 mL vials and 15 × 6 mL vials respectively. Any two half-size

rack trays can be installed in the autosamplers simultaneously. A specially

designed sample-rack holding 100 × 1.8 mL vials is available for use with

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