Agilent Technologies 1290 infinity Bedienungsanleitung

Agilent Technologies

Agilent 1290 Infinity

Thermostatted Column

Compartment

User Manual

1290 Infinity TCC User Manual

Notices

No part of this manual may be reproduced

in any form or by any means (including elec-

tronic storage and retrieval or translation

into a foreign language) without prior agree-

ment and written consent from Agilent

Technologies, Inc. as governed by United

States and international copyright laws.

Manual Part Number

G1316-90030

Edition

07/10

Printed in Germany

Agilent Technologies

Hewlett-Packard-Strasse 8

76337 Waldbronn

This product may be used as a com-

ponent of an in vitro diagnostic sys-

tem if the system is registered with

the appropriate authorities and com-

plies with the relevant regulations.

Otherwise, it is intended only for gen-

eral laboratory use.

Warranty

The material contained in this docu-

ment is provided “as is,” and is sub-

ject to being changed, without notice,

in future editions. Further, to the max-

imum extent permitted by applicable

law, Agilent disclaims all warranties,

either express or implied, with regard

to this manual and any information

contained herein, including but not

limited to the implied warranties of

merchantability and fitness for a par-

ticular purpose. Agilent shall not be

liable for errors or for incidental or

consequential damages in connection

with the furnishing, use, or perfor-

mance of this document or of any

information contained herein. Should

Agilent and the user have a separate

written agreement with warranty

terms covering the material in this

document that conflict with these

terms, the warranty terms in the sep-

arate agreement shall control.

Technology Licenses

The hardware and/or software described in

this document are furnished under a license

and may be used or copied only in accor-

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Restricted Rights Legend

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U.S. Government prime contract or subcon-

tract, Software is delivered and licensed as

“Commercial computer software” as

defined in DFAR 252.227-7014 (June 1995),

or as a “commercial item” as defined in FAR

2.101(a) or as “Restricted computer soft-

ware” as defined in FAR 52.227-19 (June

1987) or any equivalent agency regulation

or contract clause. Use, duplication or dis-

closure of Software is subject to Agilent

Technologies’ standard commercial license

terms, and non-DOD Departments and

Agencies of the U.S. Government will

receive no greater than Restricted Rights as

defined in FAR 52.227-19(c)(1-2) (June

1987). U.S. Government users will receive

no greater than Limited Rights as defined in

FAR 52.227-14 (June 1987) or DFAR

252.227-7015 (b)(2) (November 1995), as

applicable in any technical data.

Safety Notices

CAUTION

A CAUTION notice denotes a

hazard. It calls attention to an

operating procedure, practice, or

the like that, if not correctly per-

formed or adhered to, could

result in damage to the product

or loss of important data. Do not

proceed beyond a CAUTION

notice until the indicated condi-

tions are fully understood and

met.

WARNING

A WARNING notice denotes a

hazard. It calls attention to an

operating procedure, practice,

or the like that, if not correctly

performed or adhered to, could

result in personal injury or

death. Do not proceed beyond a

WARNING notice until the indi-

cated conditions are fully under-

stood and met.

1290 Infinity TCC User Manual 3

In This Guide...

This manual covers the Agilent 1290 Infinity Thermostatted Column

Compartment (TCC) (G1316C).

1 Introduction to the Column Compartment

This chapter gives an introduction to the TCC, instrument overview and

internal connectors.

2 Site Requirements and Specifications

This chapter provides information on environmental requirements, physical

and performance specifications.

3 Installing the Module

This chapter provides information on unpacking, checking on completeness,

stack considerations and installation of the module.

4 How to optimize the Column Compartment

This chapter provides information on how to optimize the Thermostatted

Column Compartment.

5 Troubleshooting and Diagnostics

Overview about the troubleshooting and diagnostic features.

6 Error Information

This chapter describes the meaning of error messages, and provides

information on probable causes and suggested actions how to recover from

error conditions.

7 Test Functions and Calibrations

This chapter describes the TCC’s built in test functions.

4 1290 Infinity TCC User Manual

In This Guide...

8 Maintenance

This chapter describes the maintenance tasks for the TCC. If the instrument

needs repair please contact your Agilent service representative.

9 Parts and Materials for Maintenance

This chapter provides information on parts for maintenance.

10 Identifying Cables

This chapter summarizes information on all cables.

11 Appendix

This chapter provides addition information on safety, legal and web.

1290 Infinity TCC User Manual 5

Contents

1 Introduction to the Column Compartment 9

Overview of the Module 10

System Overview 11

Column-Identification System 13

Column Switching Valve (Optional) 15

Early Maintenance Feedback 24

Instrument Layout 25

Electrical Connections 26

Interfaces 29

Setting the 8-bit Configuration Switch 34

2 Site Requirements and Specifications 41

Site Requirements 42

Physical Specifications 45

Performance Specifications 46

Extended Specifications on G1316C 47

3 Installing the Module 49

Unpacking the module 50

Optimizing the Stack Configuration 51

Installing the Column Compartment 56

Installing Valve Heads 61

Installation of Heater Devices 64

Flow Connections of the Column Compartment 66

Placing Columns 74

4 How to optimize the Column Compartment 77

Optimizing the Column Compartment 78

Using Additional Heater Devices 79

Delay Volume and Extra-Column Volume 80

How to Configure the Optimum Delay Volume 82

How to Achieve Higher Injection Volumes 83

How to Achieve High Throughput 84

6 1290 Infinity TCC User Manual

Contents

5 Troubleshooting and Diagnostics 87

Overview of the Module’s Indicators and Test Functions 88

Status indicators 89

Available Tests vs User Interfaces 91

Agilent Lab Advisor Software 92

6 Error Information 93

What Are Error Messages 94

General Error Messages 95

TCC Error Messages 100

7 Test Functions and Calibrations 111

Thermostat Function Test 112

Pressure Test 114

Temperature Calibration 115

8 Maintenance 119

Introduction to Maintenance and Repair 120

Cautions and Warnings 121

Overview of Maintenance 123

Cleaning the Column Compartment 124

Changing Column Identification Tags 125

Adding Heater Devices 127

Installing the capillaries 131

Correcting Leaks 141

Replacing Valve Heads 142

Preparing the Thermostatted Column Compartment for Transportation 145

Replacing the Module Firmware 147

9 Parts and Materials for Maintenance 149

Valve Options Overview 150

Heater and Cooling Devices 152

Column Switching Valve 8 Position-9 Port 155

2 pos/6 Port Ultra High Pressure Valve Head 156

2Pos/10Port Ultra High Pressure Valve Head 157

8Pos/9Port Ultra High Pressure Valve Head 158

1290 Infinity TCC User Manual 7

Contents

2pos/6 port valve head 600 bar 159

2pos/10 port valve head 600 bar 160

8pos/9 port valve head 600 bar 161

Accessory Kits 162

10 Identifying Cables 167

Cable Overview 168

Analog cables 170

Remote Cables 172

BCD Cables 175

CAN Cable 177

RS-232 Cable Kit 178

Agilent Module to Printer 179

11 Appendix 181

General Safety Information 182

The Waste Electrical and Electronic Equipment (WEEE) Directive

(2002-96-EC) 185

Lithium Batteries Information 186

Radio Interference 187

Sound Emission 188

Solvent Information 189

Agilent Technologies on Internet 190

8 1290 Infinity TCC User Manual

Contents

1290 Infinity TCC User Manual

Agilent Technologies

Introduction to the Column

Compartment

Overview of the Module 10

System Overview 11

Column-Identification System 13

Column Switching Valve (Optional) 15

Typical Applications 18

Early Maintenance Feedback 24

Instrument Layout 25

Electrical Connections 26

Serial Number Information 27

Rear view of the module 28

Interfaces 29

Overview Interfaces 30

Setting the 8-bit Configuration Switch 34

Communication Settings for RS-232C 37

Special Settings 39

This chapter gives an introduction to the TCC, instrument overview and internal

connectors.

10 1290 Infinity TCC User Manual

1Introduction to the Column Compartment

Overview of the Module

The Agilent 1290 Infinity thermostatted column compartments is a stackable

temperature-controlled column compartment for LC. It is available as

standalone module or as a component of an Agilent 1290 Infinity system. It is

used for heating and cooling to meet extreme requirements of retention time

reproducibility.

The main features of the 1290 Infinity thermostatted column compartment

are:

•Peltier heating and cooling from 10 degrees below ambient up to 100 °C

with high heating and cooling speeds for maximum application flexibility

and stability,

•holds up to three 30 cm columns and optimized design gives minimum dead

volumes and maximum efficiency,

•two independently programmable heat exchangers contribute volumes of

only 3 and 6 µl,

•additional heating devices for low flow rates, which reduce the risk of

additional dispersion,

•it can be supplemented by a kit to install a small heat-exchanger with 1.6 µl

delay volume to reduce the delay volume.

•electronic column-identification module as standard for GLP

documentation of column type, and major column parameters,

•optional high-quality Rheodyne®column switching valves with ceramic

stator-face assemblies for prolonged lifetime.

For specifications, see “Performance Specifications” on page 46.

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