Agilent Technologies 1260 Infinity Bedienungsanleitung

Agilent Technologies

Agilent 1260 Infinity

Standard Autosampler

User Manual

Agilent 1260 Infinity Standard Autosampler User Manual

Notices

2013

No part of this manual may be reproduced

in any form or by any means (including elec-

tronic storage and retrieval or translation

into a foreign language) without prior agree-

ment and written consent from Agilent

Technologies, Inc. as governed by United

States and international copyright laws.

Manual Part Number

G1329-90015 Rev. B

Edition

04/2013

Printed in Germany

Agilent Technologies

Hewlett-Packard-Strasse 8

76337 Waldbronn

This product may be used as a com-

ponent of an in vitro diagnostic sys-

tem if the system is registered with

the appropriate authorities and com-

plies with the relevant regulations.

Otherwise, it is intended only for gen-

eral laboratory use.

Warranty

The material contained in this docu-

ment is provided “as is,” and is sub-

ject to being changed, without notice,

in future editions. Further, to the max-

imum extent permitted by applicable

law, Agilent disclaims all warranties,

either express or implied, with regard

to this manual and any information

contained herein, including but not

limited to the implied warranties of

merchantability and fitness for a par-

ticular purpose. Agilent shall not be

liable for errors or for incidental or

consequential damages in connection

with the furnishing, use, or perfor-

mance of this document or of any

information contained herein. Should

Agilent and the user have a separate

written agreement with warranty

terms covering the material in this

document that conflict with these

terms, the warranty terms in the sep-

arate agreement shall control.

Technology Licenses

The hardware and/or software described in

this document are furnished under a license

and may be used or copied only in accor-

dance with the terms of such license.

Restricted Rights Legend

If software is for use in the performance of a

U.S. Government prime contract or subcon-

tract, Software is delivered and licensed as

“Commercial computer software” as

defined in DFAR 252.227-7014 (June 1995),

or as a “commercial item” as defined in FAR

2.101(a) or as “Restricted computer soft-

ware” as defined in FAR 52.227-19 (June

1987) or any equivalent agency regulation

or contract clause. Use, duplication or dis-

closure of Software is subject to Agilent

Technologies’ standard commercial license

terms, and non-DOD Departments and

Agencies of the U.S. Government will

receive no greater than Restricted Rights as

defined in FAR 52.227-19(c)(1-2) (June

1987). U.S. Government users will receive

no greater than Limited Rights as defined in

FAR 52.227-14 (June 1987) or DFAR

252.227-7015 (b)(2) (November 1995), as

applicable in any technical data.

Safety Notices

CAUTION

A CAUTION notice denotes a

hazard. It calls attention to an

operating procedure, practice, or

the like that, if not correctly per-

formed or adhered to, could

result in damage to the product

or loss of important data. Do not

proceed beyond a CAUTION

notice until the indicated condi-

tions are fully understood and

met.

WARNING

A WARNING notice denotes a

hazard. It calls attention to an

operating procedure, practice,

or the like that, if not correctly

performed or adhered to, could

result in personal injury or

death. Do not proceed beyond a

WARNING notice until the indi-

cated conditions are fully under-

stood and met.

Agilent 1260 Infinity Standard Autosampler User Manual 3

In This Book

This manual covers the Agilent 1260 Infinity Standard Autosampler (G1329B).

1 Introduction to the Autosampler (ALS)

This chapter gives an introduction to the autosampler and instrument

overview.

2 Site Requirements and Specifications

This chapter provides information on environmental requirements, physical

and performance specifications.

3 Installing the Autosampler

This chapter provides information on unpacking, checking on completeness,

stack considerations and installation of the module.

4 Using the Autosampler

This chapter provides information on how to set up the module for an analysis

and explains the basic settings.

5 Optimizing Performance

This chapter provides information on how to optimize the module.

6 Troubleshooting and Diagnostics

Overview about the troubleshooting and diagnostic features.

7 Error Information

This chapter describes the meaning of error messages, and provides

information on probable causes and suggested actions how to recover from

error conditions.

4 Agilent 1260 Infinity Standard Autosampler User Manual

In This Book

8 Maintenance

This chapter describes the maintenance of the module.

9 Parts and Materials for Maintenance

This chapter provides information on parts for maintenance.

10 Identifying Cables

This chapter provides information on cables used with the module.

11 Hardware Information

This chapter describes the detector in more detail on hardware and

electronics.

12 Appendix

This chapter provides addition information on safety, legal and web.

Agilent 1260 Infinity Standard Autosampler User Manual 5

Contents

1 Introduction to the Autosampler (ALS) 9

Introduction to the Autosampler (ALS) 10

2 Site Requirements and Specifications 21

Site Requirements 22

Physical Specifications 25

Performance Specifications Standard Autosampler 26

3 Installing the Autosampler 27

Unpacking the Autosampler 28

Optimizing the Stack Configuration 29

Installing the Autosampler 32

Flow Connections 35

Installing the Sample Tray 37

Transporting the Autosampler 38

4 Using the Autosampler 39

Sample Trays 40

Choice of Vials and Caps 42

5 Optimizing Performance 45

Optimization for Lowest Carry-over 46

Fast Injection Cycle and Low Delay Volume 49

Precise Injection Volume 51

Choice of Rotor Seal 53

6 Troubleshooting and Diagnostics 55

Overview of the Module’s Indicators and Test Functions 56

Status Indicators 57

Maintenance Functions 59

ALS Step Commands 66

6 Agilent 1260 Infinity Standard Autosampler User Manual

Contents

Troubleshooting 68

Troubleshooting Guide for the Sample Transport Assembly 70

Agilent Lab Advisor Software 77

7 Error Information 79

What are Error Messages 81

General Error Messages 82

Autosampler Error Messages 88

8 Maintenance 101

Introduction to Maintenance 102

Cautions and Warnings 103

Updating the Firmware 105

Cleaning the Module 106

Safety Flap, Flex Board 107

Transport Assembly Parts 108

Maintenance Functions 109

Simple Repairs 110

Exchanging the Needle Assembly 111

Exchanging the Needle-Seat Assembly 114

Exchanging the Rotor Seal 116

Exchanging the Metering Seal and Piston 120

Exchanging the Gripper Arm 124

Exchanging the Interface Board 126

Replacing the Module’s Firmware 127

9 Parts and Materials for Maintenance 129

Main Assemblies 130

Analytical-Head Assembly 132

Vial Trays 134

Standard Autosampler Accessory Kit 136

Maintenance Kit 137

Injection Upgrade Kit 138

Multi-Draw Kit 139

External Tray 140

Agilent 1260 Infinity Standard Autosampler User Manual 7

Contents

10 Identifying Cables 141

Cable Overview 142

Analog Cables 144

Remote Cables 146

BCD Cables 149

External Contact Cable 151

CAN/LAN Cables 152

Auxiliary Cable 153

RS-232 Cables 154

11 Hardware Information 155

Firmware Description 156

Interfaces 159

Setting the 8-bit Configuration Switch 166

Electrical Connections 170

Early Maintenance Feedback (EMF) 172

Instrument Layout 173

12 Appendix 175

General Safety Information 176

The Waste Electrical and Electronic Equipment (WEEE) Directive

(2002/96/EC) 179

Lithium Batteries Information 180

Radio Interference 181

Solvent Information 182

Sound Emission 184

Agilent Technologies on Internet 185

8 Agilent 1260 Infinity Standard Autosampler User Manual

Contents

Agilent 1260 Infinity Standard Autosampler User Manual

Agilent Technologies

Introduction to the Autosampler (ALS)

Introduction to the Autosampler (ALS) 10

Sampling Sequence 12

Sampling Unit 15

Transport Assembly 18

This chapter gives an introduction to the autosampler and instrument overview.

10 Agilent 1260 Infinity Standard Autosampler User Manual

1Introduction to the Autosampler (ALS)

Introduction to the Autosampler (ALS)

Figure 1 Overview of the Autosampler

The Agilent 1260 Infinity autosampler is designed for use with other modules

of the Agilent 1200 Infinity Series, 1200 Series and 1100 Series LC, or with

other LC systems if adequate remote control inputs and outputs are available.

The autosamplers are controlled by the Agilent Instant Pilot (G4208A) or by

Agilent control software (OpenLAB CDS, ChemStation for LC, EZChrom Elite

etc.).

Three sample-rack sizes are available for the autosampler. The standard

full-size rack holds 100 × 1.8 mL vials, while the two half-size racks provide

space for 40 × 1.8 mL vials and 15 × 6 mL vials respectively. Any two half-size

rack trays can be installed in the autosampler simultaneously. A specially

designed sample-rack holding 100 × 1.8 mL vials is available for use with

thermostatted autosamplers. The half-size racks trays are not designed for an

optimal heat transfer when they are used with a thermostatted autosampler.

6cVani^XVa]ZVY

<g^eeZgVgb

CZZYaZhZVi

K^VaigVn

Hl^iX]^c\kVakZ

Andere Handbücher für 1260 Infinity

Inhaltsverzeichnis

Andere Agilent Technologies Laborausrüstung Handbücher

Agilent Technologies

Agilent Technologies G3183B Betriebsanleitung

Agilent Technologies

Agilent Technologies 7890B Bedienungsanleitung

Agilent Technologies

Agilent Technologies 1100 Series Bedienungsanleitung

Agilent Technologies

Agilent Technologies 5890 Bedienungsanleitung

Agilent Technologies

Agilent Technologies PSG Series Bedienungsanleitung

Agilent Technologies

Agilent Technologies Intuvo 9000 Merkblatt

Agilent Technologies

Agilent Technologies 5975T LTM GC/MSD Betriebsanleitung

Agilent Technologies

Agilent Technologies 6820 Bedienungsanleitung

Agilent Technologies

Agilent Technologies 8453 Bedienungsanleitung

Agilent Technologies

Agilent Technologies 7100 Bedienungsanleitung

Agilent Technologies

Agilent Technologies 7890A Handbuch

Agilent Technologies

Agilent Technologies BenchCel Microplate Handler Bedienungsanleitung

Agilent Technologies

Agilent Technologies 7694 Bedienungsanleitung

Agilent Technologies

Agilent Technologies 979 Bedienungs- und Sicherheitshinweise

Agilent Technologies

Agilent Technologies 6100 Series LC/MS Bedienungsanleitung

Agilent Technologies

Agilent Technologies 33120A Bedienungsanleitung

Agilent Technologies

Agilent Technologies 2200 TapeStation Bedienungsanleitung

Agilent Technologies

Agilent Technologies G2747A Bedienungsanleitung

Agilent Technologies

Agilent Technologies TS-5400 Bedienungsanleitung

Agilent Technologies

Agilent Technologies G1701EA Bedienungsanleitung

Agilent Technologies

Agilent Technologies 7200 Bedienungsanleitung

Agilent Technologies

Agilent Technologies 1147A Bedienungsanleitung

Agilent Technologies

Agilent Technologies InfinityLab LC Series Bedienungsanleitung

Agilent Technologies

Agilent Technologies 240 Series AA Bedienungsanleitung

Beliebte Laborausrüstung Handbücher anderer Marken

Qiagen

Qiagen DML 3000 Bedienungsanleitung

Queensgate

Queensgate NANOSCAN OP400 Programmierhandbuch

Conviron

Conviron GEN1000-GE Bedienungsanleitung

Parr Instrument

Parr Instrument 4560 Bedienungsanleitung

IKA

IKA IC control Bedienungsanleitung

Integra

Integra DOSE IT Bedienungsanleitung

Endress+Hauser

Endress+Hauser Cleanfit CPA875 Bedienungsanleitung

NI PXI-5422 Handbuch

Collomix

Collomix Aqix Bedienungsanleitung

SPEX SamplePrep

SPEX SamplePrep 6875 Freezer/Mill Series Bedienungsanleitung

Ocean Insight

Ocean Insight FLAME-NIR+ Bedienungsanleitung

Parker

Parker ALIGN-MG-NA Bedienungsanleitung

BD 644787 Bedienungsanleitung

DENTAURUM

DENTAURUM Compact Megaplus Bedienungsanleitung

Biuged Laboratory Instruments

Biuged Laboratory Instruments BGD 626 Bedienungsanleitung

VWR

VWR SAS Super IAQ Bedienungsanleitung

illumina

illumina MiSeqDx Bedienungsanleitung

Yamato

Yamato BM510 Bedienungsanleitung