Agilent Technologies 1260 Infinity Bedienungsanleitung

Agilent Technologies

Agilent 1260 Infinity

Standard Autosampler

User Manual

Agilent 1260 Infinity Standard Autosampler User Manual

Notices

2013

No part of this manual may be reproduced

in any form or by any means (including elec-

tronic storage and retrieval or translation

into a foreign language) without prior agree-

ment and written consent from Agilent

Technologies, Inc. as governed by United

States and international copyright laws.

Manual Part Number

G1329-90015 Rev. B

Edition

04/2013

Printed in Germany

Agilent Technologies

Hewlett-Packard-Strasse 8

76337 Waldbronn

This product may be used as a com-

ponent of an in vitro diagnostic sys-

tem if the system is registered with

the appropriate authorities and com-

plies with the relevant regulations.

Otherwise, it is intended only for gen-

eral laboratory use.

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The material contained in this docu-

ment is provided “as is,” and is sub-

ject to being changed, without notice,

in future editions. Further, to the max-

imum extent permitted by applicable

law, Agilent disclaims all warranties,

either express or implied, with regard

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contained herein, including but not

limited to the implied warranties of

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Safety Notices

CAUTION

A CAUTION notice denotes a

hazard. It calls attention to an

operating procedure, practice, or

the like that, if not correctly per-

formed or adhered to, could

result in damage to the product

or loss of important data. Do not

proceed beyond a CAUTION

notice until the indicated condi-

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met.

WARNING

A WARNING notice denotes a

hazard. It calls attention to an

operating procedure, practice,

or the like that, if not correctly

performed or adhered to, could

result in personal injury or

death. Do not proceed beyond a

WARNING notice until the indi-

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stood and met.

Agilent 1260 Infinity Standard Autosampler User Manual 3

In This Book

This manual covers the Agilent 1260 Infinity Standard Autosampler (G1329B).

1 Introduction to the Autosampler (ALS)

This chapter gives an introduction to the autosampler and instrument

overview.

2 Site Requirements and Specifications

This chapter provides information on environmental requirements, physical

and performance specifications.

3 Installing the Autosampler

This chapter provides information on unpacking, checking on completeness,

stack considerations and installation of the module.

4 Using the Autosampler

This chapter provides information on how to set up the module for an analysis

and explains the basic settings.

5 Optimizing Performance

This chapter provides information on how to optimize the module.

6 Troubleshooting and Diagnostics

Overview about the troubleshooting and diagnostic features.

7 Error Information

This chapter describes the meaning of error messages, and provides

information on probable causes and suggested actions how to recover from

error conditions.

4 Agilent 1260 Infinity Standard Autosampler User Manual

In This Book

8 Maintenance

This chapter describes the maintenance of the module.

9 Parts and Materials for Maintenance

This chapter provides information on parts for maintenance.

10 Identifying Cables

This chapter provides information on cables used with the module.

11 Hardware Information

This chapter describes the detector in more detail on hardware and

electronics.

12 Appendix

This chapter provides addition information on safety, legal and web.

Agilent 1260 Infinity Standard Autosampler User Manual 5

Contents

1 Introduction to the Autosampler (ALS) 9

Introduction to the Autosampler (ALS) 10

2 Site Requirements and Specifications 21

Site Requirements 22

Physical Specifications 25

Performance Specifications Standard Autosampler 26

3 Installing the Autosampler 27

Unpacking the Autosampler 28

Optimizing the Stack Configuration 29

Installing the Autosampler 32

Flow Connections 35

Installing the Sample Tray 37

Transporting the Autosampler 38

4 Using the Autosampler 39

Sample Trays 40

Choice of Vials and Caps 42

5 Optimizing Performance 45

Optimization for Lowest Carry-over 46

Fast Injection Cycle and Low Delay Volume 49

Precise Injection Volume 51

Choice of Rotor Seal 53

6 Troubleshooting and Diagnostics 55

Overview of the Module’s Indicators and Test Functions 56

Status Indicators 57

Maintenance Functions 59

ALS Step Commands 66

6 Agilent 1260 Infinity Standard Autosampler User Manual

Contents

Troubleshooting 68

Troubleshooting Guide for the Sample Transport Assembly 70

Agilent Lab Advisor Software 77

7 Error Information 79

What are Error Messages 81

General Error Messages 82

Autosampler Error Messages 88

8 Maintenance 101

Introduction to Maintenance 102

Cautions and Warnings 103

Updating the Firmware 105

Cleaning the Module 106

Safety Flap, Flex Board 107

Transport Assembly Parts 108

Maintenance Functions 109

Simple Repairs 110

Exchanging the Needle Assembly 111

Exchanging the Needle-Seat Assembly 114

Exchanging the Rotor Seal 116

Exchanging the Metering Seal and Piston 120

Exchanging the Gripper Arm 124

Exchanging the Interface Board 126

Replacing the Module’s Firmware 127

9 Parts and Materials for Maintenance 129

Main Assemblies 130

Analytical-Head Assembly 132

Vial Trays 134

Standard Autosampler Accessory Kit 136

Maintenance Kit 137

Injection Upgrade Kit 138

Multi-Draw Kit 139

External Tray 140

Agilent 1260 Infinity Standard Autosampler User Manual 7

Contents

10 Identifying Cables 141

Cable Overview 142

Analog Cables 144

Remote Cables 146

BCD Cables 149

External Contact Cable 151

CAN/LAN Cables 152

Auxiliary Cable 153

RS-232 Cables 154

11 Hardware Information 155

Firmware Description 156

Interfaces 159

Setting the 8-bit Configuration Switch 166

Electrical Connections 170

Early Maintenance Feedback (EMF) 172

Instrument Layout 173

12 Appendix 175

General Safety Information 176

The Waste Electrical and Electronic Equipment (WEEE) Directive

(2002/96/EC) 179

Lithium Batteries Information 180

Radio Interference 181

Solvent Information 182

Sound Emission 184

Agilent Technologies on Internet 185

8 Agilent 1260 Infinity Standard Autosampler User Manual

Contents

Agilent 1260 Infinity Standard Autosampler User Manual

Agilent Technologies

Introduction to the Autosampler (ALS)

Introduction to the Autosampler (ALS) 10

Sampling Sequence 12

Sampling Unit 15

Transport Assembly 18

This chapter gives an introduction to the autosampler and instrument overview.

10 Agilent 1260 Infinity Standard Autosampler User Manual

1Introduction to the Autosampler (ALS)

Introduction to the Autosampler (ALS)

Figure 1 Overview of the Autosampler

The Agilent 1260 Infinity autosampler is designed for use with other modules

of the Agilent 1200 Infinity Series, 1200 Series and 1100 Series LC, or with

other LC systems if adequate remote control inputs and outputs are available.

The autosamplers are controlled by the Agilent Instant Pilot (G4208A) or by

Agilent control software (OpenLAB CDS, ChemStation for LC, EZChrom Elite

etc.).

Three sample-rack sizes are available for the autosampler. The standard

full-size rack holds 100 × 1.8 mL vials, while the two half-size racks provide

space for 40 × 1.8 mL vials and 15 × 6 mL vials respectively. Any two half-size

rack trays can be installed in the autosampler simultaneously. A specially

designed sample-rack holding 100 × 1.8 mL vials is available for use with

thermostatted autosamplers. The half-size racks trays are not designed for an

optimal heat transfer when they are used with a thermostatted autosampler.

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