Agilent Technologies SPS 4 Bedienungsanleitung

Agilent Technologies

Agilent SPS 4

Autosampler

User’s Guide

Notices

No part of this manual may be reproduced in

any form or by any means (including elec-

tronic storage and retrieval or translation

into a foreign language) without prior agree-

ment and written consent from Agilent

Technologies, Inc. as governed by United

States and international copyright laws.

Manual Part Number

G8410-90000

Edition

Revision A, May 2015

Agilent Technologies

9-1 Takakura-cho, Hachioji-shi,

Tokyo 192-8510 Japan

Printed in Malaysia

Warranty

The material contained in this docu-

ment is provided "as is," and is sub-

ject to being changed, without notice,

in future editions. Further, to the max-

imum extent permitted by applicable

law, Agilent disclaims all warranties,

either express or implied, with regard

to this manual and any information

contained herein, including but not

limited to the implied warranties of

merchantability and fitness for a par-

ticular purpose. Agilent shall not be

liable for errors or for incidental or

consequential damages in connec-

tion with the furnishing, use, or per-

formance of this document or of any

information contained herein. Should

Agilent and the user have a separate

written agreement with warranty

terms covering the material in this

document that conflict with these

terms, the warranty terms in the sep-

arate agreement shall control.

Technology Licenses

The hardware and/or software described in

this document are furnished under a license

and may be used or copied only in accor-

dance with the terms of such license.

Restricted Rights Legend

If software is for use in the performance of a

U.S. Government prime contract or subcon-

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or as a "commercial item" as defined in FAR

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ware" as defined in FAR 52.227-19 (June

1987) or any equivalent agency regulation or

contract clause. Use, duplication or disclo-

sure of Software is subject to Agilent Tech-

nologies' standard commercial license

terms, and non-DOD Departments and

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receive no greater than Restricted Rights as

defined in FAR 52.227-19(c)(1-2) (June

1987). U.S. Government users will receive

no greater than Limited Rights as defined in

FAR 52.227-14 (June 1987) or DFAR

252.227-7015 (b)(2) (November 1995), as

applicable in any technical data.

Safety Notices

WARNING

A WARNING notice denotes a

hazard. It calls attention to an

operating procedure, practice, or

the like that, if not correctly per-

formed or adhered to, could result

in personal injury or death. Do not

proceed beyond a WARNING

notice until the indicated condi-

tions are fully understood and

met.

CAUTION

A CAUTION notice denotes a haz-

ard. It calls attention to an operat-

ing procedure, practice, or the like

that, if not correctly performed or

adhered to, could result in damage

to the product or loss of important

data. Do not proceed beyond a

CAUTION notice until the indicated

conditions are fully understood and

met.

NOTE

A NOTE contains helpful informa-

tion on the usage - it does not

denote a hazard.

Agilent products must only be used in the

manner described in the Agilent product

user guides. Any other use may result in

damage to the product or personal injury.

Agilent is not responsible for any damages

caused, in whole or in part, by improper use

of the products, unauthorized alterations,

adjustments or modifications to the prod-

ucts, failure to comply with procedures in

Agilent product user guides, or use of the

products in violation of applicable laws,

rules or regulations.

Agilent shall not be liable for errors or dam-

ages on products or performance due to

using non-Agilent genuine parts.

Contents

Agilent SPS 4 Autosampler User’s Guide 3

Contents

1 Safety Practices and Hazards

Electrical Hazards 8

Flammable Liquids 9

Other Precautions 9

Safety Symbols 10

Warning Symbols 11

CE Compliance 12

Environmental Conditions 12

Electromagnetic Compatibility 13

2 Introduction

Overview 16

Front and Rear Views 17

Front View 17

Rear View 19

Intended Use 21

Specifications 22

Environmental 22

Power 22

Weights and Dimensions 23

Key Specifications 23

Options and Accessories 25

3 Installation

Installation Procedure 30

Orientation 30

Bench Requirements 32

4 Agilent SPS 4 Autosampler User’s Guide

Contents

Inspection and Unpacking 32

Unpacking and Lifting 32

Installing the Cover Kit 34

Fitting the Spill Tray 34

Installing the Rack Location Mat 36

Installing the Wash Reservoir 37

Installing the Standards Rack 39

Installing the Sample Racks 40

Fitting the Sample Probe 42

Fitting the Wash Pump Tubing 44

Two Drain Arrangements 46

Loading Wash Pump Tubing 47

Pressure Plate Adjustment 48

Connecting the Power and the Communications Cable 48

Confirming the Operation 50

Setting up the Instrument Controlling Software for SPS 4 50

Notes on Lifting the Autosampler 51

4Operation

Starting up the Autosampler 54

Shutting Down the Autosampler 55

Flushing the Wash Reservoir and Flow Path 55

Software Control 56

5 Maintenance

Routine Maintenance 58

Cleaning 58

Contents

Agilent SPS 4 Autosampler User’s Guide 5

Replacing the Wash Pump Tubing 59

Lubrication 60

Service 60

Spare Parts 60

6 Troubleshooting

Troubleshooting Guide 64

Power Supply Problems 65

Operating State Problems 65

Error Indicator Codes 66

Initialization Problems 68

Probing Problems 69

Probe Arm Jam 69

When the Sample Probe Hits an Object 69

Communication Problems 70

7 Running the Calibration Wizard

Before User Calibration 72

Calibration Wizard Overview 72

Performing User Calibration 74

Error List 79

AAppendices

Installing the Cover Kit 82

Introduction 82

Tools Required 83

Unpacking your Autosampler Cover 83

Installing your Autosampler Cover 84

Door Operation 91

6 Agilent SPS 4 Autosampler User’s Guide

Contents

Connections 92

Care and Maintenance 92

Preventing Earthquake Damage 94

Default Rinse Materials 95

Agilent Technologies

Agilent SPS 4 Autosampler

User’s Guide

Safety Practices and Hazards

Electrical Hazards 8

Flammable Liquids 9

Other Precautions 9

Safety Symbols 10

Your Agilent SPS 4 autosampler has been carefully designed

so that when used properly you have an accurate, fast,

flexible and safe analytical system.

If the equipment is used in a manner not specified by

Agilent, the protection provided by the equipment may be

impaired.

Information about safety practices appears throughout the

documentation provided with your equipment. Before using

the equipment, ensure you read these safety practices

carefully.

Observe all relevant safety practices at all times.

8 Agilent SPS 4 Autosampler User’s Guide

1 Safety Practices and Hazards

Electrical Hazards

The Agilent SPS 4 contains electrical circuits, devices, and components

operating at dangerous voltages. Contact with these circuits, devices and

components can cause death, serious injury, or painful electrical shock.

To reduce the risks of electrical shock, this equipment employs a

three- wire electrical cord and plug to ground the equipment. To use this

safety feature:

•Ensure the matching wall outlet receptacle is properly wired and

grounded correctly.

•Never use a three- wire to two- wire plug adapter.

•Never use a two wire extension cord or a non- grounded multiple outlet

receptacle strip.

•Do not use any power cord other than that supplied with this

equipment.

•The power cord set that is shipped with this equipment cannot be used

with other products.

•Position the autosampler so that it is easy to access the mains power

on the wall outlet or to remove the power cord from the autosampler or

wall outlet.

•Only Agilent- trained, Agilent- qualified, or Agilent- approved customer

support representatives may open panels or covers that are secured by

screws. Removal of such panels or covers can expose parts that involve

the risk of electric shock or personal injury.

Application of the wrong supply voltage can create a fire hazard and a

potentially serious shock hazard, and can seriously damage the

autosampler.

Do not connect the autosampler to the mains power supply until all

checks and settings have been completed.

Replace or repair faulty or frayed insulation on power cords.

NOTE This equipment is rated Equipment Class I.

Safety Practices and Hazards 1

Agilent SPS 4 Autosampler User’s Guide 9

Flammable Liquids

Observe the following precautions when using your autosampler in

conjunction with flammable liquids.

To reduce the risk of fire:

•Ensure the following autosampler parts do not contact the surface of

the fluid or have parts near the surface of the fluid:

•parts that consume power

•parts that produce heat

•parts that conduct heat from other areas in any form

•Ensure no parts in or near the fluid surface are capable of igniting a

flammable liquid.

•Operators must adhere to standard laboratory practices for the safe

handling of flammable liquids.

Other Precautions

Use of the autosampler in any manner other than that specified by Agilent

may impair the protection provided by the equipment.

Use of the autosampler may involve materials, solvents and solutions that

are flammable, corrosive, toxic or otherwise hazardous.

Careless, improper, or unskilled use of materials, solvents and solutions

can create explosions, fire, toxicity and other hazards that can result in

death, serious personal injury and damage to equipment and property.

WARNING The autosampler must always be connected to protective earth through the power

cord. Position the autosampler so that it is easy to access the mains power switch

on the wall outlet or to remove the power cord from the autosampler or wall outlet.

10 Agilent SPS 4 Autosampler User’s Guide

1 Safety Practices and Hazards

Always ensure that laboratory safety practices governing the use, handling

and disposal of such materials are strictly observed. These safety practices

should include the wearing of appropriate safety clothing and safety

glasses.

Components of the autosampler move automatically and at speed.

Safety Symbols

The general definitions of safety symbols used on equipment or in

manuals are listed below.

Direct current.

On supply.

Off supply.

Hazardous voltage and potential for electrical shock. Do not touch

terminals that have this symbol when the equipment is on.

Caution, refer to accompanying documentation. Equipment marked with

this symbol indicates that it is necessary for the user to refer to the

instruction manual.

The CE mark shows that the product complies with all applicable

European Directives.

The CSA mark is a registered trademark of the Canadian Standards

Association.

WARNING Keep clear of the probe arm assembly during operation to prevent injury.

NOTE A protective cover is available to prevent accidental contact with the probe arm assembly.

Contact your local Agilent representative for further information.

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