Agilent Technologies Cary 50 Bedienungsanleitung

Cary 50

Spectrophotometer

Hardware Manual

2Cary 50 Spectrophotometer Hardware Manual

Notices

1999, 2002, 2004, 2006, 2010 and 2011

No part of this manual may be

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and retrieval or translation into a

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Agilent Technologies, Inc. as governed

by United States and international

Manual Part Number

8510159600

Edition

Ninth edition, March 2011

Printed in Australia

Agilent Technologies, Inc.

Warranty

The material contained in this

document is provided “as is,” and is

subject to being changed, without

notice, in future editions. Further, to

the maximum extent permitted by

applicable law, Agilent disclaims all

warranties, either express or implied,

with regard to this manual and any

information contained herein,

including but not limited to the

implied warranties of merchantability

and fitness for a particular purpose.

Agilent shall not be liable for errors

or for incidental or consequential

damages in connection with the

furnishing, use, or performance of

this document or of any information

contained herein. Should Agilent and

the user have a separate written

agreement with warranty terms

covering the material in this

document that conflict with these

terms, the warranty terms in the

separate agreement shall control.

Technology Licenses

The hardware and/or software

described in this document are

furnished under a license and may be

used or copied only in accordance

with the terms of such license.

Restricted Rights Legend

If software is for use in the

performance of a U.S. Government

prime contract or subcontract,

Software is delivered and licensed as

“Commercial computer software” as

defined in DFAR 252.227-7014 (June

1995), or as a “commercial item” as

defined in FAR 2.101(a) or as

“Restricted computer software” as

defined in FAR 52.227-19 (June 1987)

or any equivalent agency regulation or

contract clause. Use, duplication or

disclosure of Software is subject to

Agilent Technologies‟ standard

commercial license terms, and non-

DOD Departments and Agencies of the

U.S. Government will receive no

greater than Restricted Rights as

defined in FAR 52.227-19(c)(1-2) (June

1987). U.S. Government users will

receive no greater than Limited Rights

as defined in FAR 52.227-14 (June

1987) or DFAR 252.227-7015 (b)(2)

(November 1995), as applicable in any

technical data.

Safety Notices

A CAUTION notice denotes a hazard.

It calls attention to an operating

procedure, practice, or the like that, if

not correctly performed or adhered to,

could result in damage to the product

or loss of important data. Do not

proceed beyond a CAUTION notice

until the indicated conditions are fully

understood and met.

A WARNING notice denotes a

hazard. It calls attention to an

operating procedure, practice, or the

like that, if not correctly performed or

adhered to, could result in personal

injury or death. Do not proceed

beyond a WARNING notice until the

indicated conditions are fully

understood and met.

WARNING

CAUTION

Contents

Cary 50 Spectrophotometer Hardware Manual 3

Contents

1. Safety Practices and Hazards 5

Lamp module 6

Electrical hazards 6

Modules, covers and panels 6

Other precautions 7

Warning and caution messages 7

Information symbols 8

Color coding 9

CE compliance 10

2. Introduction 11

Installation requirements11

Documentation 11

Conventions 12

Specifications 12

Environmental 13

Weights and dimensions13

Computer power supply 13

Connections 14

3. Installation 15

Cell holder 16

Alignment 18

Other sample holders 18

Contents

4Cary 50 Spectrophotometer Hardware Manual

Uninstalling the Cary WinUV software 19

Uninstalling the Cary 50 driver 19

4. Maintenance 21

Cleaning 22

Lamp module 22

Replacing 22

Aligning the source mirror 25

5. Troubleshooting 27

Windows XP service or driver failure 27

Access denied during installation28

FCary service failed to start 29

No green light indicating that the Cary 50 is powered 30

Start button replaced with Connect button 30

Hard disk power supply connection 32

Absorbance is 10 and fluctuates wildly during a scan 32

Instrument performance testing 33

Wavelength calibration 35

6. Spare Parts 37

Safety Practices and Hazards

Cary 50 Spectrophotometer Hardware Manual 5

1. Safety Practices and Hazards

Lamp module 6

Electrical hazards 6

Modules, covers and panels 6

Other precautions 7

Warning and caution messages 7

Information symbols 8

Color coding 9

CE compliance 10

Your Agilent Cary 50 instrument and accessories have been carefully

designed so that when used properly, you have an accurate, fast,

flexible and safe analytical system.

If the equipment is used in a manner not specified by the

manufacturer, the protection provided by the equipment may be

impaired.

Information about safety practices appears throughout the

documentation (both hard copy and online) provided with your

instrument and accessories to help you safely operate the instrument

and accessories. Before using the instrument or accessories, you

must thoroughly read these safety practices. ALWAYS operate the

instrument and accessories in accordance with these safety practices.

Safety Practices and Hazards

6Cary 50 Spectrophotometer Hardware Manual

Lamp module

The lamp is enclosed in a self-contained module. This module

contains components operating at high voltages. To avoid electric

shock, NEVER disassemble the module.

When operating, the lamp module emits high-intensity light, which

can cause serious damage to eyes. To avoid eye damage, never

operate the lamp outside the instrument.

Electrical hazards

The Cary 50 spectrophotometer is powered by the computer

controlling the instrument. Safe operation of the instrument depends

on the integrity of the switching power supply of the computer. Your

computer must comply with IEC 60950.

Modules, covers and panels

The ONLY modules of the Cary 50 spectrophotometer that operators

and other unauthorized personnel are permitted to access are the

lamp module (on the underside of the instrument) and the sample

compartment. White circles indicate the screws you need to undo to

remove the lamp module. ALWAYS switch off the computer before

changing a lamp.

The only panel you are permitted to remove is the snap-out panel

covering the lamp mirror adjustment screws on the front of the

instrument.

Any other panels or covers that are retained by screws on the

spectrophotometer and accessories may be opened ONLY by Agilent-

trained, Agilent-qualified, or Agilent-approved customer support

representatives. Consult the manuals or product labels supplied with

your computer, monitor and printer to determine which parts are

operator-accessible.

NOTE

The safety classification is given as Safety Class III (EN 61010-1).

Safety Practices and Hazards

Cary 50 Spectrophotometer Hardware Manual 7

Other precautions

Do not block any ventilation grilles present on the computer. Consult

the manuals supplied with your computer, monitor and printer for

their specific ventilation requirements.

Use of the Cary 50 system and accessories may involve materials,

solvents and solutions that are flammable, corrosive, toxic or

otherwise hazardous.

Careless, improper, or unskilled use of such materials, solvents and

solutions can create explosion hazards, fire hazards, toxicity and

other hazards which can result in death, serious personal injury, and

damage to equipment and property.

ALWAYS ensure that laboratory safety practices governing the use,

handling and disposal of such materials are strictly observed. These

safety practices should include the wearing of appropriate safety

clothing and safety glasses.

Warning and caution messages

Carefully read all warnings and cautions and observe them at all

times.

A Warning message is used in the text when failure to observe

instructions or precautions could result in death or injury. Warnings

have the following format:

WARNING

Hazard Type

Nature of the hazard, information on how to avoid the hazard, and possible

consequences if you don’t.

The triangular symbols that appear in conjunction with warnings are

outlined in the next section.

Safety Practices and Hazards

8Cary 50 Spectrophotometer Hardware Manual

A Caution message is used when failure to observe instructions could

result in damage to equipment (Agilent-supplied and/or other

associated equipment). Cautions have the following format:

CAUTION

Caution information appears here.

Information symbols

The following triangular symbols appear in conjunction with

warnings on the spectrometer and associated documentation. The

hazard they depict is shown below each symbol:

Broken glass

Corrosive liquid

Electrical shock

Eye hazard

Fire hazard

Heavy weight

(danger to feet)

Heavy weight

(danger to hands)

Hot surface

Noxious gas

The following symbol may be used on warning labels attached to the

instrument. When you see this symbol, refer to the relevant operation

or service manual for the correct procedure referred to by that

warning label.

Safety Practices and Hazards

Cary 50 Spectrophotometer Hardware Manual 9

The following symbols also appear on the instrument or in the

documentation:

Indicates that a high voltage xenon flash lamp is present.

Indicates viewing hole to check the operation of the Xenon flash

lamp.

When attached to the rear of the instrument, indicates that the

product complies with the requirements of one or more EU

directives.

When attached to the rear of the product, indicates that the product

has been certified (evaluated) to CSA 1010.1 and UL 3101-1.

Color coding

The various indicator lights appearing on Agilent instruments and

associated accessories are color-coded to represent the status of the

instrument or accessory.

The green indicator lamp on the front of the Cary 50 indicates the

instrument is powered up (that is, the computer is switched on) and

is in normal/standby condition. When the indicator lamp is flashing,

this indicates the instrument is busy.

Safety Practices and Hazards

10 Cary 50 Spectrophotometer Hardware Manual

CE compliance

Agilent Cary 50 instruments have been designed to comply with the

requirements of the Electromagnetic Compatibility (EMC) Directive

and the Low Voltage (electrical safety) Directive (commonly referred

to as the LVD) of the European Union. Agilent has confirmed that

each product complies with the relevant directives by testing a

prototype against the prescribed EN (European Norm) standards.

Proof that a product complies with the directives is indicated by:

The CE marking appearing on the rear of the product.

The documentation package that accompanies the product,

containing a copy of the Declaration of Conformity. This

declaration is the legal declaration by Agilent that the product

complies with the directives and also shows the EN standards to

which the product was tested to demonstrate compliance.

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