Agilent Technologies 8355 Sulfur Bedienungsanleitung
Agilent Technologies
Agilent 8355 Sulfur and
8255 Nitrogen
Chemiluminescence
Detectors
User Manual
Notices
© Agilent Technologies, Inc. 2017
No part of this manual may be reproduced
in any form or by any means (including
electronic storage and retrieval or
translation into a foreign language)
without prior agreement and written
consent from Agilent Technologies, Inc. as
governed by United States and
international copyright laws.
Manual Part Number
G3488-90010
Edition
Fifth edition, March 2017
Fourth edition, February 2016
Third edition, December 2015
Second edition, October 2015
First edition, September 2015
Printed in USA or China
Agilent Technologies, Inc.
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Wilmington, DE 19808-1610 USA
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is provided “as is,” and is subject to
being changed, without notice, in future
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Safety Notices
CAUTION
A CAUTION notice denotes a hazard.
It calls attention to an operating
procedure, practice, or the like that, if
not correctly performed or adhered to,
could result in damage to the product
or loss of important data. Do not
proceed beyond a CAUTION notice
until the indicated conditions are fully
understood and met.
WARNING
A WARNING notice denotes a hazard.
It calls attention to an operating
procedure, practice, or the like that, if
not correctly performed or adhered
to, could result in personal injury or
death. Do not proceed beyond a
WARNING notice until the indicated
conditions are fully understood and
met.
8355 SCD and 8255 NCD User Manual 3
Contents
1 Getting Started
Manuals, Information, Tools and Where to Find Them 8
Safety Information 8
Online help 8
Education Opportunities 9
Overview of the 8355 SCD and 8255 NCD 10
Overview of Installation and First Startup 14
2SystemDescription
Specifications 16
8355 SCD 16
8255 NCD 16
MDL calculations 17
Theory of Operation 18
SCD 18
NCD 18
Description of Major Components 20
Burner assembly 20
Ozone generator 22
Reaction cell and photomultiplier tube (PMT) 23
EPC modules 23
Vacuum pump 23
Ozone destruction trap 23
Oil coalescing filter 23
FID adapter (optional) 24
NCD chiller 24
3Operation
Introduction 26
Integrated version 26
Setting Parameters 27
Parameters and ranges 27
Software control 28
GC keyboard control 30
Identifying the detector 30
Detector Stability and Response 31
48355 SCD and 8255 NCD User Manual
Typical Operating Conditions 32
Adjusting the Operating Conditions 33
Start-up 34
Resource Conservation 36
Shutdown 37
Configure Auto Flow Zero on the GC 37
Automatic Configuration of the Detector 39
4 Maintenance
Maintenance Log and Early Maintenance Feedback (EMF) 42
Maintenance Schedule 43
Tracking Detector Sensitivity 44
Consumables and Replacement Parts 45
Exploded Parts View of the SCD 47
Exploded Parts View of the NCD 48
Detector Maintenance Method 49
Attach a Column to the Detector 50
Replace the Inner Ceramic Tube (SCD) 53
Replace the Quartz Tube (NCD) 56
Check the Vacuum Pump Oil 60
Add Vacuum Pump Oil 61
Replace the Vacuum Pump Oil 63
Replace the Ozone Trap 65
Change the Oil Mist Filter 66
Clean the Detector Exterior 67
Calibrate the Flow and Pressure Sensors 68
Updating Firmware 69
5 Troubleshooting
Solving Detector Problems 72
Troubleshooting Table 73
Status Indicator LED 76
Detector Messages 77
8355 SCD and 8255 NCD User Manual 5
Leaks 78
Ozone leaks 78
Hydrogen leaks 78
Oxidizer leaks 78
Checking for hydrogen and oxidizer leaks 79
Power Problems 80
No power 80
Ozone Generation Problems 81
Coking 82
Hydrogen Poisoning 83
Contaminated Gases 84
6 Performance Verification
About Chromatographic Checkout 86
Prepare for Chromatographic Checkout 87
Prepare sample vials 88
Check SCD Performance 89
Check NCD Performance 95
68355 SCD and 8255 NCD User Manual
7
Agilent 8355 SCD and 8255 NCD
User Manual
Agilent Technologies
1
Getting Started
Manuals, Information, Tools and Where to Find Them 8
Overview of the 8355 SCD and 8255 NCD 10
Overview of Installation and First Startup 14
This chapter introduces the Agilent 8355 Sulfur
Chemiluminescence Detector (SCD) and the Agilent 8255
Nitrogen Chemiluminescence Detector (NCD), and provides
details about where to find helpful information and tools, such
as GC manuals, flow calculators, and so forth.
88355 SCD and 8255 NCD User Manual
1Getting Started
Manuals, Information, Tools and Where to Find Them
This manual describes how to operate the 8355 SCD and the
8255 NCD as installed on an Agilent 7890B Gas Chromatograph
(GC). This manual also provides operating recommendations,
maintenance procedures, and troubleshooting. For installation
instructions, see “Overview of Installation and First Startup” on
page 14. To prepare the installation site for a new SCD or NCD,
see the Agilent Site Preparation Guide.
In addition, Agilent provides other manuals, familiarization
information, and help systems for self-paced learning about the
7890B GC. You will need to reference this general GC
information for installation and operation of the detector. The
sections below describe this information and where to find it.
Safety Information
Before proceeding, read the important safety and regulatory
information found in the Agilent Safety and Regulatory
Information manual for the 8355, 8355 S and 8255, 8255 S
Chemiluminescence Detectors.
Online help
In addition to hardware manuals, your GC data system also
includes an extensive online help system with detailed
information, common tasks, and video tutorials on using the
software.
Getting Started 1
8355 SCD and 8255 NCD User Manual 9
Education Opportunities
Agilent has designed customer courses to help you learn how to
use your GC to maximize your productivity while learning about
all of the great features of your new system:
For course details and education opportunities, visit
http://www.agilent.com/chem/education, or call your local Agilent
sales representative.
10 8355 SCD and 8255 NCD User Manual
1Getting Started
Overview of the 8355 SCD and 8255 NCD
Figure 1 through Figure 5 show the controls, parts, and
components of the 8355 SCD and 8255 NCD used or accessed
during installation, operation, and maintenance.
Figure 1 Front view, detectors (SCD and NCD)
Power switch
Status LED
Power switch
Status LED
8355 SCD 8255 NCD
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1
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