Agilent Technologies 1260 Infinity II Bedienungsanleitung

Agilent Technologies

Agilent InfinityLab LC Series

1260 Infinity II Flexible

Pump

User Manual

1260 Infinity II Flexible Pump User Manual

Notices

No part of this manual may be reproduced

in any form or by any means (including

electronic storage and retrieval or transla-

tion into a foreign language) without prior

agreement and written consent from Agi-

lent Technologies, Inc. as governed by

United States and international copyright

laws.

Manual Part Number

G7104-90010

Edition

09/2017

Printed in Germany

Agilent Technologies

Hewlett-Packard-Strasse 8

76337 Waldbronn

Warranty

The material contained in this docu-

ment is provided “as is,” and is sub-

ject to being changed, without notice,

in future editions. Further, to the max-

imum extent permitted by applicable

law, Agilent disclaims all warranties,

either express or implied, with regard

to this manual and any information

contained herein, including but not

limited to the implied warranties of

merchantability and fitness for a par-

ticular purpose. Agilent shall not be

liable for errors or for incidental or

consequential damages in connection

with the furnishing, use, or perfor-

mance of this document or of any

information contained herein. Should

Agilent and the user have a separate

written agreement with warranty

terms covering the material in this

document that conflict with these

terms, the warranty terms in the sep-

arate agreement shall control.

Technology Licenses

The hardware and/or software described in

this document are furnished under a

license and may be used or copied only in

accordance with the terms of such license.

Restricted Rights Legend

If software is for use in the performance of

a U.S. Government prime contract or sub-

contract, Software is delivered and licensed

as “Commercial computer software” as

defined in DFAR 252.227-7014 (June 1995),

or as a “commercial item” as defined in

FAR 2.101(a) or as “Restricted computer

software” as defined in FAR 52.227-19

(June 1987) or any equivalent agency regu-

lation or contract clause. Use, duplication

or disclosure of Software is subject to Agi-

lent Technologies’ standard commercial

license terms, and non-DOD Departments

and Agencies of the U.S. Government will

receive no greater than Restricted Rights as

defined in FAR 52.227-19(c)(1-2) (June

1987). U.S. Government users will receive

no greater than Limited Rights as defined in

FAR 52.227-14 (June 1987) or DFAR

252.227-7015 (b)(2) (November 1995), as

applicable in any technical data.

Safety Notices

CAUTION

A CAUTION notice denotes a

hazard. It calls attention to an

operating procedure, practice, or

the like that, if not correctly per-

formed or adhered to, could

result in damage to the product

or loss of important data. Do not

proceed beyond a CAUTION

notice until the indicated condi-

tions are fully understood and

met.

WARNING

A WARNING notice denotes a

hazard. It calls attention to an

operating procedure, practice,

or the like that, if not correctly

performed or adhered to, could

result in personal injury or

death. Do not proceed beyond a

WARNING notice until the indi-

cated conditions are fully

understood and met.

1260 Infinity II Flexible Pump User Manual 3

In This Guide...

This manual covers the Agilent 1260 Infinity II Flexible Pump (G7104C).

1Introduction

This chapter gives an introduction to the module, instrument overview and

internal connectors.

2 Site Requirements and Specifications

This chapter provides information on environmental requirements, physical

and performance specifications.

3 Using the Module

This chapter explains the operational parameters of the Agilent 1260 Infinity

II Flexible Pump.

4 How to Optimize the Performance of Your Module

This chapter gives hints on how to optimize the performance or use additional

devices.

5 Troubleshooting and Diagnostics

Overview about the troubleshooting and diagnostic features.

6 Error Information

This chapter describes the meaning of error messages, and provides

information on probable causes and suggested actions how to recover from

error conditions.

7 Maintenance

This chapter describes the maintenance of the Agilent 1260 Infinity II Flexible

Pump.

4 1260 Infinity II Flexible Pump User Manual

In This Guide...

8 Parts and Materials

This chapter provides information on parts for maintenance and repair.

9 Identifying Cables

This chapter provides information on cables used with the modules.

10 Hardware Information

This chapter describes the pump in more detail on hardware and electronics.

11 LAN Configuration

This chapter provides information on connecting the module to the controller

software.

12 Appendix

This chapter provides additional information on safety, legal and web.

1260 Infinity II Flexible Pump User Manual 5

Contents

1Introduction 9

Product Description 10

Features 12

Operating Principle 13

Positions of the Multi Purpose Valve 15

Leak and Waste Handling 19

2 Site Requirements and Specifications 25

Site Requirements 26

Physical Specifications 29

Performance Specifications 30

3 Using the Module 33

Magnets 34

Turn on/off 35

Status Indicators 37

Best Practices 38

Flushing the Filter 42

Purging the Pump 44

Solvent Information 46

Solvent Recommendation for Agilent 1290 Infinity and 1290 Infinity II and 1260

Infinity II Flexible Pumps 52

Algae Growth in HPLC Systems 57

Setting up the Pump with the Instrument Control Interface 58

Agilent Local Control Modules 69

4 How to Optimize the Performance of Your Module 71

Delay Volume and Extra-Column Volume 72

How to Configure the Optimum Delay Volume 73

How to Achieve Higher Resolution 75

Using Solvent Calibration Tables 78

6 1260 Infinity II Flexible Pump User Manual

Contents

5 Troubleshooting and Diagnostics 79

User Interfaces 80

Agilent Lab Advisor Software 81

Pump Leak Rate Test 82

System Pressure Test 86

Pump Self Test 88

6 Error Information 93

What Are Error Messages 95

General Error Messages 96

Pump Error Messages 101

7 Maintenance 119

Introduction to Maintenance 121

Warnings and Cautions 122

Overview of Maintenance 124

Cleaning the Module 125

Install Fittings and Capillaries 126

Remove and Install Doors 127

Replace the Pressure Sensor 129

Replace the Inlet Weaver 131

Replace the Inlet Valve 133

Remove the Jet Weaver 134

Install the Jet Weaver 136

Replace the Seal Wash Pump Cartridge 138

Replace the Multi-Channel Gradient Valve (MCGV) 139

Release a Stuck Inlet Valve 141

Remove the Pump Head Assembly 143

Pump Head Maintenance (Tool Free) 146

Install the Pump Head Assembly 160

Replace the Outlet Valve 162

Replace the Multi Purpose Valve 165

Replace Parts of the Multi Purpose Valve 167

Replace the High Pressure Outlet Filter or Filter Frit 168

Install the Inline Filter 170

Remove the Inline Filter 172

Replace Parts of the Inline Filter 173

1260 Infinity II Flexible Pump User Manual 7

Contents

Replace the Seal Wash Sensor 176

Replace the Module Firmware 178

Prepare the Pump Module for Transport 179

8 Parts and Materials 181

Overview of Main Assemblies 182

Flow Connections 184

Pump Heads 186

Multi Purpose Valve 190

Cover Parts 191

Accessory Kit 192

Tool Kit 193

9 Identifying Cables 195

Cable Overview 196

Analog Cables 198

Remote Cables 200

CAN/LAN Cables 204

Agilent Module to PC 205

USB Cables 206

10 Hardware Information 207

Firmware Description 208

Electrical Connections 211

Interfaces 213

Setting the 8-bit Configuration Switch 219

Early Maintenance Feedback 222

Instrument Layout 223

8 1260 Infinity II Flexible Pump User Manual

Contents

11 LAN Configuration 225

What You Have To Do First 226

TCP/IP Parameter Configuration 227

Configuration Switch 228

Initialization Mode Selection 229

Dynamic Host Configuration Protocol (DHCP) 231

Link Configuration Selection 234

Manual Configuration 235

PC and User Interface Software Setup 240

12 Appendix 243

General Safety Information 244

Waste Electrical and Electronic Equipment Directive 250

Radio Interference 251

Sound Emission 252

Agilent Technologies on Internet 253

1260 Infinity II Flexible Pump User Manual

Agilent Technologies

Introduction

Product Description 10

Features 12

Operating Principle 13

Positions of the Multi Purpose Valve 15

Leak and Waste Handling 19

Leak Sensor 22

Waste Concept 23

This chapter gives an introduction to the module, instrument overview and

internal connectors.

10 1260 Infinity II Flexible Pump User Manual

Introduction

Product Description

The new Agilent 1260 Infinity II Flexible Pump improves your everyday

efficiency by combining the performance of a high-pressure mixing UHPLC

pump with the flexibility of a low-pressure mixing UHPLC pump.

The power range of 5 mL/min with a maximum pressure up to 800 bar allows

to run HPLC and UHPLC methods on the same LC system. Intelligent System

Emulation Technology enables the transfer from existing methods from

different LC systems - current Agilent systems as well as instruments from

other manufacturers.

The Agilent Inlet Weaver mixer, active damping, or the optional Agilent Jet

Weaver mixers for additional mixing capacity achieve high analytical

efficiency.

The established multipurpose valve enhances laboratory efficiency by adding

useful functionalities, for example, mixer in/out switch, filter backflush, or

automatic purge.

BlendAssist software simplifies your workflow with accurate buffer/additive

blending.

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