Agilent Technologies InfinityLab LC Series Bedienungsanleitung

Agilent InfinityLab LC Series

Preparative Binary Pumps

User Manual

Preparative Binary Pumps User Manual

Notices

Manual Part Number

D0000602 Rev.B

EDITION 10/2019

No part of this manual may be repro-

duced in any form or by any means

(including electronic storage and retrieval

or translation into a foreign language)

without prior agreement and written con-

sent from Agilent Technologies, Inc. as

governed by United States and interna-

tional copyright laws.

Agilent Technologies

Hewlett-Packard-Strasse 8

76337 Waldbronn

Warranty

The material contained in this document

is provided “as is,” and is subject to being

changed, without notice, in future edi-

tions. Further, to the maximum extent

permitted by applicable law, Agilent dis-

claims all warranties, either express or

implied, with regard to this manual and

any information contained herein, includ-

ing but not limited to the implied warran-

ties of merchantability and fitness for a

particular purpose. Agilent shall not be lia-

ble for errors or for incidental or conse-

quential damages in connection with the

furnishing, use, or performance of this

document or of any information con-

tained herein. Should Agilent and the user

have a separate written agreement with

warranty terms covering the material in

this document that conflict with these

terms, the warranty terms in the separate

agreement shall control.

Technology Licenses

The hardware and/or software described

in this document are furnished under a

license and may be used or copied only in

accordance with the terms of such

license.

Restricted Rights Legend

U.S. Government Restricted Rights. Soft-

ware and technical data rights granted to

the federal government include only

those rights customarily provided to end

user customers. Agilent provides this

customary commercial license in Soft-

ware and technical data pursuant to FAR

12.211 (Technical Data) and 12.212

(Computer Software) and, for the Depart-

ment of Defense, DFARS 252.227-7015

(Technical Data - Commercial Items) and

DFARS 227.7202-3 (Rights in Commer-

cial Computer Software or Computer

Software Documentation).

Safety Notices

CAUTION

notice denotes a

hazard. It calls attention to an

operating procedure, practice, or

the like that, if not correctly per-

formed or adhered to, could result

in damage to the product or loss

of important data. Do not proceed

beyond a

CAUTION

notice until

the indicated conditions are fully

understood and met.

WARNING

A WARNING notice denotes a

hazard. It calls attention to an

operating procedure, practice, or

the like that, if not correctly per-

formed or adhered to, could

result in personal injury or death.

Do not proceed beyond a WARN-

ING notice until the indicated

conditions are fully understood

and met.

Preparative Binary Pumps User Manual 3

In This Guide...

This manual covers the following modules:

•Agilent 1260 Infinity II Preparative Binary Pump (G7161A)

•Agilent 1290 Infinity II Preparative Binary Pump (G7161B)

1Introduction

This chapter gives an introduction to the module and an instrument overview.

2 Site Requirements and Specifications

This chapter provides information on environmental requirements, physical and

performance specifications.

3 Using the Pump

This chapter explains the operational parameters of the module.

4 Optimizing Performance

This chapter gives hints on how to optimize the performance or use additional

devices.

5Troubleshootingand Diagnostics

Overview about the troubleshooting and diagnostic features.

6ErrorInformation

This chapter describes the meaning of error messages, and provides information

on probable causes and suggested actions how to recover from error conditions.

7 Maintenance

This chapter describes the maintenance of the module.

Preparative Binary Pumps User Manual 4

8 Parts and Materials for Maintenance

This chapter provides information on parts for maintenance.

9IdentifyingCables

This chapter provides information on cables used with the modules.

10 Hardware Information

This chapter describes the module in more detail on hardware and electronics.

11 LAN Configuration

This chapter provides information on connecting the module to the Agilent

ChemStation PC.

12 Appendix

This chapter provides addition information on safety, legal and web.

Preparative Binary Pumps User Manual 5

Contents

1Introduction9

G7161A Preparative Binary Pump 10

G7161B Preparative Binary Pump 12

Flow Reduction 14

Pump Principle 15

Leak and Waste Handling 18

2 Site Requirements and Specifications 19

Site Requirements 20

Physical Specifications 24

Performance Specifications 25

3 Using the Pump 31

Magnets 32

Turn on/off 33

Status Indicators 35

Best Practices 36

Purging the Pump 39

Solvent Information 41

Algae Growth in HPLC Systems 49

Agilent Local Control Modules 50

4 Optimizing Performance 51

Delay Volume and Extra-Column Volume 52

How to Achieve Higher Resolution 53

Using Solvent Calibration Tables 56

5Troubleshootingand Diagnostics 57

User Interfaces 58

Preparative Binary Pumps User Manual 6

Agilent Lab Advisor Software 59

Pump Leak Rate Test 60

6ErrorInformation64

What Are Error Messages 65

General Error Messages 66

Module Error Messages 73

7 Maintenance 79

Introduction to Maintenance 80

Warnings and Cautions 83

Overview of Maintenance 85

Cleaning the Module 86

Install Fittings and Capillaries 87

Remove and Install Doors 88

Open and Close Doors 90

Replace the Manifold 91

Replace the Y-Connector (G7161A) 93

Replace the Solvent Selection Valve (G7161B) 94

Replace the Solvent Mixer 96

Replace the Seal Wash Pump 97

Replace the Seal Wash Sensor 99

Replace the Purge Valve 101

Replace the Purge Valve Adapter and the Filter 103

Replace the Inlet Valve Cartridge 106

Release a Stuck Inlet Valve 108

Replace the Outlet Valve 110

Remove the Pump Head Assembly 112

Pump Head Maintenance 113

Install the Pump Head Assembly 117

Replace the Module Firmware 119

Prepare the Pump Module for Transport 120

Preparative Binary Pumps User Manual 7

8 Parts and Materials for Maintenance 122

Overview of Maintenance Parts (G7161A) 123

Overview of Maintenance Parts (G7161B) 124

Flow Connections (G7161A) 125

Flow Connections (G7161B) 126

Purge Valve 127

Pump Heads 128

Accessory Kit 131

HPLC System Tool Kit 132

9 Identifying Cables 133

Cable Overview 134

Analog Cables 136

Remote Cables 138

CAN/LAN Cables 142

Agilent Module to PC 143

USB 144

10 Hardware Information 145

Firmware Description 146

Electrical Connections 149

Interfaces 151

Setting the 6-bit Configuration Switch 158

Early Maintenance Feedback 160

Instrument Layout 161

11 LAN Configuration 162

What You Have to Do First 163

TCP/IP parameter configuration 164

Configuration Switches 165

Initialization Mode Selection 166

Preparative Binary Pumps User Manual 8

Dynamic Host Configuration Protocol (DHCP) 168

Manual Configuration 171

12 Appendix 175

General Safety Information 176

Waste Electrical and Electronic Equipment (WEEE) Directive 183

Radio Interference 184

Sound Emission 185

Agilent Technologies on Internet 186

Preparative Binary Pumps User Manual 9

1Introduction

G7161A Preparative Binary Pump 10

Product Description 10

Features 11

G7161B Preparative Binary Pump 12

Product Description 12

Features 13

Flow Reduction 14

Flow Reduction when Column Switching 14

Flow Reduction for Pump Protection (G7161B only) 14

Pump Principle 15

Leak and Waste Handling 18

Leak Sensor 18

This chapter gives an introduction to the module and an instrument overview.

Preparative Binary Pumps User Manual 10

1Introduction

G7161A Preparative Binary Pump

Product Description

The 1260 Infinity II Preparative Binary Pump is an affordable high-pressure

gradient pump for LC purification. This pump has been designed and tested for

reverse-phase solvents and engineered for continuous use to provide reliable and

rugged performance through a dual-piston, rapid-refill design. It delivers flow

from 1 to 50 mL/min and is ideally suited for a broad range of semi-preparative

applications using conventional columns up to 30 mm id.

Figure 1 Overview of the pump

Status indicator

Purge valve

Leak and waste drain

Power switch

Active seal wash

Solvent mixer

Y-connector

Manifold

Channel B

Channel A

Andere Handbücher für InfinityLab LC Series

Dieses Handbuch passt für folgende Modelle

Inhaltsverzeichnis

Andere Agilent Technologies Wasserpumpe Handbücher

Agilent Technologies

Agilent Technologies TV 301SF Navigator Bedienungsanleitung

Agilent Technologies

Agilent Technologies 1260 Infinity Quaternary LC VL Bedienungsanleitung

Agilent Technologies

Agilent Technologies MS40+ Bedienungsanleitung

Agilent Technologies

Agilent Technologies VHS-4 Bedienungsanleitung

Agilent Technologies

Agilent Technologies SH-110 Bedienungsanleitung

Agilent Technologies

Agilent Technologies TriScroll 610 Bedienungsanleitung

Agilent Technologies

Agilent Technologies G6696A Bedienungsanleitung

Agilent Technologies

Agilent Technologies 1100 Series Bedienungsanleitung

Agilent Technologies

Agilent Technologies MS 120 Major Installations- und Betriebsanleitung

Agilent Technologies

Agilent Technologies TV-401/301/21 NSF Bedienungsanleitung

Agilent Technologies

Agilent Technologies Turbo-V 1K-G Series Bedienungsanleitung

Agilent Technologies

Agilent Technologies TriScroll 620 Series Bedienungsanleitung

Agilent Technologies

Agilent Technologies Varian TriScroll 620 Series Bedienungsanleitung

Agilent Technologies

Agilent Technologies 1100 Series Bedienungsanleitung

Agilent Technologies

Agilent Technologies 1290 Infinity II Bedienungsanleitung

Agilent Technologies

Agilent Technologies PHV K Series Handbuch

Agilent Technologies

Agilent Technologies TPS-mini 9699180 Bedienungsanleitung

Agilent Technologies

Agilent Technologies 1290 infinity Bedienungsanleitung

Agilent Technologies

Agilent Technologies X3500-64000 Bedienungsanleitung

Agilent Technologies

Agilent Technologies VHS-4 Bedienungsanleitung

Agilent Technologies

Agilent Technologies TPS-compact Bedienungsanleitung

Agilent Technologies

Agilent Technologies TV-401/301 MS Bedienungsanleitung

Agilent Technologies

Agilent Technologies MS120 Bedienungsanleitung

Agilent Technologies

Agilent Technologies 1200 series Bedienungsanleitung

Beliebte Wasserpumpe Handbücher anderer Marken

Neptun

Neptun NPHW 5500 Bedienungsanleitung

Sensidyne

Sensidyne Gilian BDX-II Montage- und Bedienungsanleitung

Draper

Draper 47808 Bedienungsanleitung

Trolla

Trolla 12820 Bedienungsanleitung

Sunfab

Sunfab SVH Series Bedienungsanleitung

WilTec

WilTec 50740 Bedienungsanleitung

Fieldmann

Fieldmann FVC 5015 EK Bedienungsanleitung

Everbilt

Everbilt EFSUB5-122HD Bedienungsanleitung

Graco

Graco Husky 3300e Bedienungsanleitung

esotec

esotec 101018 Bedienungsanleitung

moyno

moyno 2000 CC Bedienungsanleitung

Becker

Becker BASIC VASF 2.80/1-0.AC230 Bedienungsanleitung

Sykes AmeriPumps

Sykes AmeriPumps GP100M Fehlerbehebungshandbuch

DUROMAX

DUROMAX XP WX Series Bedienungsanleitung

BRINKMANN PUMPS

BRINKMANN PUMPS SBF550 Bedienungsanleitung

Franklin Electric

Franklin Electric IPS Bedienungsanleitung

Xylem

Xylem e-1532 Series Bedienungsanleitung

Milton Roy

Milton Roy PRIMEROYAL Bedienungsanleitung