Agilent Technologies 1290 infinity Bedienungsanleitung

Agilent Technologies

Agilent 1290 Infinity

Quaternary Pump

User Manual

1290 Infinity Quaternary Pump User Manual

Notices

No part of this manual may be reproduced

in any form or by any means (including

electronic storage and retrieval or transla-

tion into a foreign language) without prior

agreement and written consent from Agi-

lent Technologies, Inc. as governed by

United States and international copyright

laws.

Manual Part Number

G4204-90002 Rev. B

Edition

10/2018

Printed in Germany

Agilent Technologies

Hewlett-Packard-Strasse 8

76337 Waldbronn

Warranty

The material contained in this docu-

ment is provided “as is,” and is sub-

ject to being changed, without notice,

in future editions. Further, to the max-

imum extent permitted by applicable

law, Agilent disclaims all warranties,

either express or implied, with regard

to this manual and any information

contained herein, including but not

limited to the implied warranties of

merchantability and fitness for a par-

ticular purpose. Agilent shall not be

liable for errors or for incidental or

consequential damages in connection

with the furnishing, use, or perfor-

mance of this document or of any

information contained herein. Should

Agilent and the user have a separate

written agreement with warranty

terms covering the material in this

document that conflict with these

terms, the warranty terms in the sep-

arate agreement shall control.

Technology Licenses

The hardware and/or software described in

this document are furnished under a

license and may be used or copied only in

accordance with the terms of such license.

Restricted Rights Legend

If software is for use in the performance of

a U.S. Government prime contract or sub-

contract, Software is delivered and licensed

as “Commercial computer software” as

defined in DFAR 252.227-7014 (June 1995),

or as a “commercial item” as defined in

FAR 2.101(a) or as “Restricted computer

software” as defined in FAR 52.227-19

(June 1987) or any equivalent agency regu-

lation or contract clause. Use, duplication

or disclosure of Software is subject to Agi-

lent Technologies’ standard commercial

license terms, and non-DOD Departments

and Agencies of the U.S. Government will

receive no greater than Restricted Rights as

defined in FAR 52.227-19(c)(1-2) (June

1987). U.S. Government users will receive

no greater than Limited Rights as defined in

FAR 52.227-14 (June 1987) or DFAR

252.227-7015 (b)(2) (November 1995), as

applicable in any technical data.

Safety Notices

CAUTION

A CAUTION notice denotes a

hazard. It calls attention to an

operating procedure, practice, or

the like that, if not correctly per-

formed or adhered to, could

result in damage to the product

or loss of important data. Do not

proceed beyond a CAUTION

notice until the indicated condi-

tions are fully understood and

met.

WARNING

A WARNING notice denotes a

hazard. It calls attention to an

operating procedure, practice,

or the like that, if not correctly

performed or adhered to, could

result in personal injury or

death. Do not proceed beyond a

WARNING notice until the indi-

cated conditions are fully

understood and met.

1290 Infinity Quaternary Pump User Manual 3

In This Guide...

This manual covers the Agilent 1290 Infinity Quaternary Pump (G4204A).

1Introduction

This chapter gives an introduction to the module, instrument overview and

internal connectors.

2 Site Requirements and Specifications

This chapter provides information on environmental requirements, physical

and performance specifications.

3 Installing the Module

This chapter gives information about the preferred stack setup for your

system and the installation of your Agilent 1290 Infinity Quaternary Pump.

4 Using the Module

This chapter explains the operational parameters of the Agilent 1290 Infinity

Quaternary Pump.

5 How to Optimize the Performance of Your Module

This chapter gives hints on how to optimize the performance or use additional

devices.

6 Troubleshooting and Diagnostics

Overview about the troubleshooting and diagnostic features.

7 Error Information

This chapter describes the meaning of error messages, and provides

information on probable causes and suggested actions how to recover from

error conditions.

4 1290 Infinity Quaternary Pump User Manual

In This Guide...

8 Test Functions and Calibrations

This chapter describes the tests for the module.

9 Maintenance

This chapter describes the maintenance of the Agilent 1290 Infinity

Quaternary Pump.

10 Parts and Materials

This chapter provides information on parts for maintenance.

11 Identifying Cables

This chapter provides information on cables used with the Agilent 1200

Infinity Series modules.

12 Hardware Information

This chapter describes the pump in more detail on hardware and electronics.

13 LAN Configuration

This chapter provides information on connecting the module to the controller

software.

14 Appendix

This chapter provides addition information on safety, legal and web.

1290 Infinity Quaternary Pump User Manual 5

Contents

1Introduction 9

Features 10

Overview of the Quaternary Pump 11

Operating Principle 12

Positions of the Multi Purpose Valve 14

System Overview 18

2 Site Requirements and Specifications 21

Site Requirements 22

Physical Specifications 25

Performance Specifications 26

3 Installing the Module 29

Unpacking the Module 30

Optimizing the Stack Configuration 31

Installation Information on Leak and Waste Handling 36

Removing the Transport Foam 40

Installing the Pump 41

Flow Connections to the Pump 43

Installation of Seal Wash Function 47

4 Using the Module 49

Magnets 51

Turn on/off 52

Status Indicators 54

Leak and Waste Handling 55

Best Practices 56

Setting up the Pump with the Instrument Control Interface 61

Flushing the Filter 73

Purging the Pump 75

Solvent Information 77

Solvent Recommendation for Agilent 1290 Infinity and 1290 Infinity II and 1260

Infinity II Flexible Pumps 84

Algae Growth in HPLC Systems 89

6 1290 Infinity Quaternary Pump User Manual

Contents

5 How to Optimize the Performance of Your Module 91

Operational Hints for the Multi Channel Gradient Valve (MCGV) 92

Delay Volume and Extra-Column Volume 93

How to Configure the Optimum Delay Volume 94

How to Achieve Higher Resolution 96

Using Solvent Calibration Tables 99

6 Troubleshooting and Diagnostics 101

Available Tests vs User Interfaces 102

Agilent Lab Advisor Software 103

7 Error Information 105

What Are Error Messages 107

General Error Messages 108

Pump Error Messages 116

8 Test Functions and Calibrations 133

Pump Leak Rate Test 134

System Pressure Test 139

9 Maintenance 141

Introduction to Maintenance 143

Warnings and Cautions 144

Overview of Maintenance 145

Cleaning the Module 146

Installing Fittings and Capillaries 147

Replacing the Pressure Sensor 148

Replacing the Inlet Weaver 151

Replacing the Inlet Valve 153

Replacing the Outlet Valve 155

Removing the Jet Weaver 159

Installing the Jet Weaver 161

Replacing the Seal Wash Pump 163

Replacing the Multi-Channel Gradient Valve (MCGV) 165

Releasing a Stuck Inlet Valve 169

Remove the Pump Head Assembly 172

1290 Infinity Quaternary Pump User Manual 7

Contents

Pump Head Maintenance (Tool Free) 176

Install the Pump Head Assembly 191

Replacing the Multi Purpose Valve 193

Replacing Parts of the Multi Purpose Valve 196

Replacing the Outlet Filter 198

Installing the Inline Filter 200

Removing the Inline Filter 202

Replacing Parts of the Inline Filter 204

Installing the Valve Rail Kit 207

Replacing Module Firmware 208

Preparing the Pump Module for Transport 209

10 Parts and Materials 215

Overview of Main Assemblies 216

Flow Connections 218

Seal Wash Function 219

Pump Heads 220

Multi Purpose Valve 224

Solvent Cabinet 226

Cover Parts 228

Leak Parts 229

Accessory Kit 230

HPLC System Tool Kit 231

11 Identifying Cables 233

Cable Overview 234

Analog cables 236

Remote Cables 238

BCD Cables 241

CAN/LAN Cable 243

RS-232 Cable Kit 244

Agilent 1200 Module to Printer 245

8 1290 Infinity Quaternary Pump User Manual

Contents

12 Hardware Information 247

Firmware Description 248

Electrical Connections 251

Interfaces 253

Setting the 8-bit Configuration Switch 260

Early Maintenance Feedback 264

Instrument Layout 265

13 LAN Configuration 267

What You Have To Do First 268

TCP/IP Parameter Configuration 269

Configuration Switch 270

Initialization Mode Selection 271

Dynamic Host Configuration Protocol (DHCP) 273

Link Configuration Selection 276

Manual Configuration 277

PC and User Interface Software Setup Setup 283

14 Appendix 285

General Safety Information 286

Waste Electrical and Electronic Equipment (WEE) Directive 292

Radio Interference 293

Sound Emission 294

Agilent Technologies on Internet 295

1290 Infinity Quaternary Pump User Manual

Agilent Technologies

Introduction

Features 10

Overview of the Quaternary Pump 11

Operating Principle 12

Positions of the Multi Purpose Valve 14

System Overview 18

Leak and Waste Handling 18

This chapter gives an introduction to the module, instrument overview and

internal connectors.

10 1290 Infinity Quaternary Pump User Manual

Introduction

Features

The G4204A Quaternary Pump is designed for highest performance, GLP

compliance and easy maintenance. It includes the following features:

•Seal wash function for continued high lifetime of pump seals for buffer

applications.

•Optional Jet Weaver for optimum mixing performance with a minimum of

delay volume.

•Automatic purge function for ease of use and unattended preparation of the

system.

•Auto tuning of the delivery cycle for compensation of elasticity and solvent

volume change effects (compressibility, thermal expansion).

•Solvent Calibration Tables for optimum flow accuracy.

•Fast defill function for improved intake and delivery performance.

•Two pistons in series design for increased reliability.

•High resolution piston movement control for smooth and reliable motion.

For specifications, see “Performance Specifications” on page 26.

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