Agilent Technologies 1200 series Bedienungsanleitung
Agilent Technologies
Agilent 1200 Series
Quaternary Pump
User Manual
1200 Series Quarternary P ump User Manual
1200 Series Quarternary Pump User Manual
Notices
© Agilent Technologies, Inc. 2006-2007,
2008
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Manual Part Number
G1311-90011
Edition
11/08
Printed in Germany
Agilent Technologies
Hewlett-Packard-Strasse 8
76337 Waldbronn
Research Use Only
Not for use in Diagnostic Procedures.
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Safety Notices
CAUTION
A CAUTION notice denotes a
hazard. It calls attention to an
operating procedure, practice, or
the like that, if not correctly per-
formed or adhered to, could
result in damage to the product
or loss of important data. Do not
proceed beyond a CAUTION
notice until the indicated condi-
tions are fully understood and
met.
WARNING
A WARNING notice denotes a
hazard. It calls attention to an
operating procedure, practice,
or the like that, if not correctly
performed or adhered to, could
result in personal injury or
death. Do not proceed beyond a
WARNING notice until the indi-
cated conditions are fully under-
stood and met.
1200 Series Quarternary Pump User Manual 3
Contents
Contents
1 Introduction 7
Introduction to the Quaternary Pump 8
Overview of the Hydraulic Path 9
Instrument Layout 16
The Electronics 17
Electrical Connections 18
Agilent 1200 Series Interfaces 20
2 Site Requirements and Specifications 21
Site Requirements 22
Physical Specifications 25
Performance Specifications 26
3 Installing the Pump 29
Unpacking the Quaternary Pump 30
Optimizing the Stack Configuration 33
Installing the Quaternary Pump 36
Connecting Modules and Control Software 39
Flow Connections of the Quaternary Pump 41
Priming and Purging the System 44
4UsingtheQuaternaryPump 49
Hints for Successful Use of the Quaternary Pump 50
Solvent Information 51
Prevent Blocking of Solvent Filters 52
Algae Growth in HPLC Systems 53
5 Optimizing Performance 55
Operational Hints for the Vacuum Degasser 56
Operational Hints for the Multi Channel Gradient Valve (MCGV) 57
When to use the Seal Wash Option 58
When to Use Alternative Seals 59
4 1200 Series Quarternary Pump User Manual
Contents
Optimize the Compressibility Compensation Setting 60
6 Troubleshooting and Test Funct io ns 63
Agilent Lab Advisor Software 64
Overview of the Pump’s Indicators and Test Functions 65
Status Indicators 66
User Interfaces 68
7 Maintenance 69
Introduction to Repairing the Pump 70
Early Maintenance Feedback (EMF) 73
Overview of Repairing the Pump 75
Simple Repairs 77
8 Parts and Materials for Maintenance 105
Overview of Main Assemblies 106
Pump Head Assembly 110
Pump Head Assembly with Seal Wash Option 112
Outlet Ball Valve Assembly 114
Purge Valve Assembly 115
Active Inlet Valve Assembly 116
Accessory Kit G1311-68705 117
Seal Wash Option Kit G1311-68711 118
9 Identifying Cables 119
Cable Overview 120
Analog Cables 122
Remote Cables 125
BCD Cables 130
External Contact Cable 132
CAN/LAN Cables 133
Auxiliary Cable 134
RS-232 Cables 135
10 Appendix 137
General Safety Information 138
1200 Series Quarternary Pump User Manual 5
Contents
The Waste Electrical and Electronic Equipment (WEEE) Directive
(2002/96/EC) 141
Lithium Batteries Information 142
Radio Interference 143
Sound Emission 144
Agilent Technologies on Internet 145
6 1200 Series Quarternary Pump User Manual
Contents
7
1200 Series Quarternary Pump User Manual
Agilent Technologies
1
Introduction
Introduction to the Quaternary Pump 8
Overview of the Hydraulic Path 9
How Does the Pump Work? 11
How Does Compressibility Compensation Work? 14
How Does Variable Stroke Volume Work? 14
Early Maintenance Feedback (EMF) 15
Instrument Layout 16
The Electronics 17
Electrical Connections 18
Agilent 1200 Series Interfaces 20
8 1200 Series Quarternary Pump User Manual
1Introduction
Introduction to the Quaternary Pump
Introduction to the Quaternary Pump
The quaternary pump comprises a solvent cabinet, a vacuum degasser and a
four-channel gradient pump. The four-channel gradient pump comprises a
high-speed proportioning valve and a pump assembly. It provides gradient
generation by low pressure mixing. Degassing is a must for a low-pressure
gradient system therefore the Agilent 1200 Series vacuum degasser is part of
the quaternary pump system. A solvent cabinet provides enough space for four
one-liter bottles. An active seal wash (optional) is available when the
quaternary pump is used with concentrated buffer solutions.
Figure 1 Overview of the Quaternary Pump
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1200 Series Quarternary Pump User Manual 9
Introduction 1
Overview of the Hydraulic Path
Overview of the Hydraulic Path
The quaternary pump is based on a two-channel, dual plunger in-series design
which comprises all essential functions that a solvent delivery system has to
fulfill. Metering of solvent and delivery to the high-pressure side are
performed by one pump assembly which can generate pressure up to 400 bar.
Degassing of the solvents is done in a vacuum degasser and solvent
compositions are generated on the low-pressure side by a high-speed
proportioning valve.
The pump assembly includes a pump head with an active inlet valve which has
an replaceable cartridge, and an outlet valve. A damping unit is connected
between the two plunger chambers. A purge valve including a PTFE frit is
fitted at the pump outlet for convenient priming of the pump head.
An active seal wash (optional) is available when the quaternary pump is used
with concentrated buffer solutions.
10 1200 Series Quarternary Pump User Manual
1Introduction
Overview of the Hydraulic Path
Figure 2 Hydraulic Path of the Quaternary Pump
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14
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