IKA C 2000 basic Bedienungsanleitung

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30 830 01 a ,.$WERKE

,.$®Calorimeter System

C 2000 EDVLF

C 2000 FRQWURO

23(5$7,1*,16758&7,216 (1

86$

Reg.-No. 4343-01

Vers. 04 08.07

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IKA-WERKE C 2000 basic / control Ver. 04 08.07

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Wir erklären in alleiniger Verantwortung, dass dieses Produkt den Bestimmungen

der Richtlinien 89 / 336 / EG und 2006 / 95 EG entspricht und mit folgenden Normen

und normativen Dokumenten übereinstimmt: DIN EN IEC 61 010-1 und DIN EN IEC

61 326-1.

&(±'(&/$5$7,212)&21),50,7< (1

We declare under our sole responsibility that this product corresponds to the regula-

tions 89 / 336 / EEC and 2006 / 95 EEC and conforms with the standards or stan-

dardized documents: DIN EN IEC 61 010-1 and DIN EN IEC 61 326-1.

'e&/$5$7,21'(&21)250,7e&( )5

Nous déclarons sous notre responsabilité que se prodiut est conforme aux régle-

mentations 89 / 336 / CEE et 2006 / 95 CEE et en conformité avec les normes ou

documents normalisés suivant: DIN EN IEC 61 010-1 et DIN EN IEC 61 326-1.

'(&/$5$&,21'(&21)250,'$''(&( (6

Declaramos por nuestra responsabilidad propia que este producto corresponde a

las directrices 89 / 336 / CEE y 2006 / 95 CEE y que cumple las normas o docu-

mentos normativos siguientes: DIN EN IEC 61 010-1 y DIN EN IEC 61 326-1.

&(±',&+,$5$=,21(',&21)250,7¬ ,7

Dichiariamo, assumendone la piena responsabilità, che il prodotto è conforme alle

seguenti direttive 89 / 336 / CCE e 2006 / 95 CCE, in accordo ai seguenti regola-

menti e documenti: DIN EN IEC 61 010-1 e DIN EN IEC 61 326-1.

Artisan Technology Group - Quality Instrumentation ... Guaranteed | (888) 88-SOURCE | www.artisantg.com

IKA-WERKE C 2000 basic / control Ver. 04 08.07

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This symbol identifies information WKDWLVRIDEVROXWHLPSRUWDQFHWRHQVXUH\RXU

KHDOWKDQGVDIHW\ Failure to observe this information may be detrimental to your

health or may result in injuries.

This symbol identifies information WKDWLVRILPSRUWDQWWRHQVXUHSUREOHPIUHH

WHFKQLFDORSHUDWLRQRIWKHGHYLFH Failure to observe this information may result in

damage to the calorimeter system.

This symbol identifies information that is important to ensure problem-free operation

of calorimetric measurements and for working with the calorimeter system. Failure to

observe this information may result in inaccurate measurement results.

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IKA-WERKE C 2000 basic / control Ver. 03 03.04

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2.1 User notes on the Operating Instructions ....................................... 2-1

2.2 Warranty....................................................................................... 2-1

2.3 Warranty claims and liability .......................................................... 2-2

2.4 System properties ......................................................................... 2-2

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3.1 Transportation and storage requirements....................................... 3-1

3.2 Set-up location.............................................................................. 3-1

3.3 Unpacking..................................................................................... 3-2

3.4 Scope of delivery .......................................................................... 3-2

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4.1 C 2000 EDVLF................................................................................. 4-1

4.2 C 2000 FRQWURO .............................................................................. 4-3

4.3 Cooling ......................................................................................... 4-4

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5.1 Determination of gross calorific value ............................................ 5-1

5.2 Corrections ................................................................................... 5-2

5.3 Complete combustion.................................................................... 5-3

5.4 Calibration .................................................................................... 5-4

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6.1 Set-up........................................................................................... 6-1

6.2 Connection oxygen supply............................................................. 6-4

6.3 Connecting peripheral devices....................................................... 6-5

6.4 Display and operating elements..................................................... 6-6

6.5 Turning on the system................................................................... 6-9

6.6 Configuring the system................................................................ 6-12

6.7 Turning off the system................................................................. 6-19

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IKA-WERKE C 2000 basic / control Ver. 03 03.04

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7.1 Notes on calibration ...................................................................... 7-1

7.2 Notes on the sample ..................................................................... 7-2

7.3 Preparing the measurement........................................................... 7-4

7.4 Performing the measurement......................................................... 7-8

7.5 Cleaning the decomposition vessel.............................................. 7-11

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9.1 Post-processing experiments......................................................... 9-1

9.2 Calculating reference states / experiment evaluation...................... 9-4

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11.1 Maintenance menu...................................................................... 11-1

11.2 Inner vessel sieve ....................................................................... 11-2

11.3 Dirt trap in the water supply line .................................................. 11-2

11.4 Maintenance for the water circuit ................................................. 11-3

11.5 Changing the O2seal .................................................................. 11-5

11.6 Changing the O2filling piston....................................................... 11-5

11.7 Decomposition vessels................................................................ 11-6

11.8 Notes on cleaning ....................................................................... 11-6

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12.1 Malfunction with message in the display ...................................... 12-1

12.2 Malfunction without message in the display.................................. 12-5

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13.1 Accessories ................................................................................ 13-1

13.2 Consumables .............................................................................. 13-1

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IKA-WERKE C 2000 basic / control Ver. 04 08.07

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In order to be able to use the appliance properly and safely, every user must first

read the operating instructions and observe the safety instructions contained

therein. Take care of these operating instructions and keep them in a place where

they can be accessed by everyone.

The C 2000 calorimeter system may only be used to determine the gross calorific

value of solid and liquid materials materials in accordance with DIN 51900, BS 1016

T5, ISO 1928, ASTM 5468, ASTM 5865 and ASTM 4809. For this purpose, use only

original IKAdecomposition vessels C 5010, C 5012 and C 62. For further details

please see the operating instructions of the decomposition vessels C 5010, 5012

and C 62.

The maximum amount of energy input into the decomposition vessel must not ex-

ceed -. (Select the weight of the sample accordingly). The permissible oper-

ating pressure of EDU 0SD must not be exceeded. The maximum permissi-

ble operating temperature must not exceed &.

Do not fill the decomposition vessel too full of the sample. Only fill the decomposi-

tion vessel with oxygen up to a maximum pressure of EDU0SD. Monitor the

adjusted pressure on the pressure reducer of your oxygen supply. Perform a leak-

age test before every combustion (please observe the operating instructions of the

decomposition vessels C 5010, C 5012 and C 62, chapter ”Leakage test”).

Many substances tend to combust in an explosive manner (for example because of

the formation of peroxide). This may cause the decomposition vessel to burst.

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Substances of which the combustion behavior is not known must be examined for

their combustion behavior before combustion in the decomposition vessel C 5010, C

5012 or C 62 (danger of explosion). If you are burning XQNQRZQVDPSOHV, leave the

room or NHHSDVDIHGLVWDQFH between you and the calorimeter.

Benzoic acid must only be burned in the form of pellets! Combustible dust and powder

must be compressed into pellets before combustion. Oven-dry dust and powder such

as wood chips, hay, straw, etc. burn in an explosive manner! They must be moistened

first! Readily combustible liquids with a low vapor pressure must not be come in direct

contact with the cotton thread (for example tetramethyl dihydrogen disiloxan)!

In addition, toxic residues of combustion are possible in the form of gasses, ash or

precipitates on the inner wall of the decomposition vessel, for example.

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When handling combustion samples, combustion residues and auxiliary materials,

the appropriate safety requirements must be observed. The following are examples

of substances that may cause dangers:

–corrosive

–easily flammable

–capable of exploding

–contaminated with bacteria

–toxic

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IKA-WERKE C 2000 basic / control Ver. 04 08.07

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When working with oxygen, observe the appropriate requirements.

Danger warning: As a compressed gas, oxygen promotes combustion, supports

combustion intensively and may react violently with combustible substances.

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Keep all gas lines and screw connections that carry oxygen free from grease.

Observe the accident prevention requirements applicable to the activity and the

work station.

Close the main valve on the oxygen supply when work is complete.

Only carry out maintenance work when the system is depressurised.

When using crucibles made of stainless steel, their condition should be carefully

checked after every experiment.

A reduction in the thickness of the material may cause the crucible to burn and may

damage the decomposition vessel. For reasons of safety, crucibles must not be

used any more after a maximum of 25 combustion procedures.

The decomposition vessel is manufactured in accordance with the regulation for

pressure vessels 97/ 23/ EEC. This can be recognized from the &(V\PERO with the

identifying number of the testing station named. The decomposition vessel is a

pressure device of Category III. The decomposition vessel has been subjected to an

EC prototype test. The CE declaration of conformity represents our guarantee to you

that this decomposition vessel complies with the pressure device described in the

EC prototype test certificate. The decomposition vessel has been subjected to a

pressure test at a test pressure of EDU and a leakage test with oxygen at 30 bar.

Decomposition vessels are H[SHULPHQWDXWRFODYHV and must be tested by a SUR

IHVVLRQDOO\WUDLQHGSHUVRQ each time before they are used.

An individual application is understood here to mean a series of experiments that

are performed under roughly the same conditions in terms of pressure and tem-

perature Experiment autoclaves must be operated in special chambers (C 2000,

C 5000).

The decomposition vessel must be subject to repeated tests (internal tests and

pressure tests) by a SHUVRQ ZLWK SURIHVVLRQDO WUDLQLQJ. The intervals between

tests must be determined by the operator based on experience, operating manner

and the material used in the decomposition vessel.

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The WKUHDGLQJ on the body of the decomposition vessel and cap screw in particular

are subject to a high level of mechanical stress and must therefore be monitored

regularly for wear and tear.

The condition of the seals must be checked for functionality and must be ensured by

means of a leakage test (please observe the operating instructions of the decompo-

sition vessels C 5010, C 5012 and C 62, chapter “Leakage test”).

Pressure tests and service tasks on the decomposition vessel must only be per-

formed by SHUVRQVZLWKSURIHVVLRQDOWUDLQLQJ.

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Artisan Technology Group - Quality Instrumentation ... Guaranteed | (888) 88-SOURCE | www.artisantg.com

IKA-WERKE C 2000 basic / control Ver. 04 08.07

3DJH

A person with professional training as defined in these operating instructions is

someone

1. whose training, knowledge and experience gained through practical activities

ensures that that person will perform the tests in a proper manner.

2. who is sufficiently reliable

3. who is not subject to any instructions in terms of testing activity

4. who is equipped with suitable testing equipment if necessary

5. who can provide suitable proof demonstrating compliance with the requirements

listed in 1.

National regulations and laws for operating pressure containers must be observed!

Anyone who operates a pressure container must maintain it in proper condition,

must monitor it and perform necessary maintenance and repair tasks without delay,

and must take measures appropriate for the circumstances to ensure safety.

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GDQJHUWKRVHZRUNLQJZLWKLWRUWKLUGSDUWLHV You can obtain a copy of the pres-

sure vessel regulation from Carl Heymann Verlag or Beuth Verlag.

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Artisan Technology Group - Quality Instrumentation ... Guaranteed | (888) 88-SOURCE | www.artisantg.com

Dieses Handbuch passt für folgende Modelle

Inhaltsverzeichnis

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