Metrohm 882 Compact IC plus Bedienungsanleitung

882 Compact IC plus

882 Compact IC plus – Anion

Manual

8.882.8012EN

Metrohm AG

CH-9101 Herisau

Switzerland

Phone +41 71 353 85 85

Fax +41 71 353 89 01

[email protected]

www.metrohm.com

882 Compact IC plus

882 Compact IC plus – Anion

2.882.0020

Manual

8.882.8012EN 05.2011 zst

Teachware

Metrohm AG

CH-9101 Herisau

[email protected]

Although all the information given in this documentation has been

checked with great care, errors cannot be entirely excluded. Should you

notice any mistakes please send us your comments using the address

given above.

Documentation in additional languages can be found on

http://products.metrohm.com under Literature/Technical documenta-

tion.

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ Table of contents

882 Compact IC plus – Anion ￭￭￭￭￭￭￭￭ III

Table of contents

1Introduction 1

1.1 Instrument description ......................................................... 1

1.2 Intended use ......................................................................... 2

1.3 About the documentation ................................................... 3

1.3.1 Symbols and conventions ........................................................ 3

1.4 Safety instructions ................................................................ 4

1.4.1 General notes on safety ........................................................... 4

1.4.2 Electrical safety ........................................................................ 4

1.4.3 Tubing and capillary connections ............................................. 5

1.4.4 Flammable solvents and chemicals ........................................... 5

1.4.5 Recycling and disposal ............................................................. 5

2Overview of the instrument 7

2.1 Front ...................................................................................... 7

2.2 Rear ........................................................................................ 8

3Installation 10

3.1 About this chapter .............................................................. 10

3.2 Initial installation ................................................................ 10

3.3 Installation diagram ........................................................... 13

3.4 Setting up the instrument .................................................. 15

3.4.1 Packaging .............................................................................. 15

3.4.2 Checks .................................................................................. 15

3.4.3 Location ................................................................................ 16

3.5 Capillary connections in the IC system ............................. 16

3.6 Installations on the rear of the instrument ...................... 19

3.6.1 Transport locking screws ....................................................... 19

3.6.2 Leak sensor ........................................................................... 19

3.6.3 Drainage tubings ................................................................... 20

3.7 Capillary and cable feed-throughs .................................... 22

3.8 Eluent ................................................................................... 24

3.8.1 Connecting eluent bottle ....................................................... 24

3.9 High pressure pump ........................................................... 28

3.9.1 Capillary connections high pressure pump/purge valve ........... 28

3.9.2 Deaerating the high pressure pump ....................................... 30

3.10 Inline filter ........................................................................... 32

3.11 Pulsation absorber ............................................................. 33

Table of contents ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭

IV ￭￭￭￭￭￭￭￭ 882 Compact IC plus – Anion

3.12 Injection valve ..................................................................... 34

3.12.1 Connecting the injection valve ............................................... 34

3.12.2 Mode of operation of the injection valve ............................... 36

3.12.3 Selecting the sample loop ...................................................... 37

3.13 Peristaltic pump .................................................................. 37

3.13.1 Principle of the peristaltic pump ............................................. 37

3.13.2 Installing the peristaltic pump ................................................ 38

3.14 Metrohm Suppressor Module (MSM) ............................... 42

3.14.1 Connecting the suppressor .................................................... 42

3.15 Connecting the instrument ................................................ 45

3.15.1 Connecting the instrument to the PC ..................................... 45

3.15.2 Connecting the instrument to mains supply ........................... 45

3.16 Guard column ..................................................................... 46

3.17 Separation column ............................................................. 47

4Start-up 50

4.1 Initial start-up ..................................................................... 50

4.2 Conditioning ........................................................................ 51

5Handling and maintenance 53

5.1 General notes ...................................................................... 53

5.1.1 Care ...................................................................................... 53

5.1.2 Maintenance by Metrohm Service .......................................... 53

5.1.3 Operation .............................................................................. 54

5.1.4 Shutting down ...................................................................... 54

5.2 Capillary connections ......................................................... 54

5.2.1 Operation .............................................................................. 54

5.3 Door ..................................................................................... 55

5.4 Eluent ................................................................................... 55

5.4.1 Production ............................................................................. 55

5.4.2 Operation .............................................................................. 56

5.5 High pressure pump ........................................................... 56

5.5.1 Protection ............................................................................. 56

5.5.2 Maintenance ......................................................................... 57

5.6 Inline filter ........................................................................... 67

5.6.1 Maintenance ......................................................................... 67

5.7 Injection valve .................................................................... 69

5.7.1 Protection ............................................................................. 69

5.8 Inline sample preparation .................................................. 69

5.9 Rinsing the sample path .................................................... 69

5.10 Peristaltic pump .................................................................. 71

5.10.1 Operation .............................................................................. 71

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ Table of contents

882 Compact IC plus – Anion ￭￭￭￭￭￭￭￭ V

5.10.2 Maintenance ......................................................................... 71

5.11 Metrohm Suppressor Module (MSM) ............................... 73

5.11.1 Protection ............................................................................. 73

5.11.2 Operation Suppressor ........................................................... 73

5.11.3 Maintenance ......................................................................... 74

5.12 Separation column ............................................................. 79

5.12.1 Separating efficiency .............................................................. 79

5.12.2 Protection ............................................................................. 80

5.12.3 Storage ................................................................................. 80

5.12.4 Regeneration ......................................................................... 80

5.13 Quality Management and validation with Metrohm ....... 81

6Troubleshooting 82

6.1 Problems and their solutions ............................................. 82

7Technical specifications 86

7.1 Reference conditions .......................................................... 86

7.2 Instrument ........................................................................... 86

7.3 Leak sensor ......................................................................... 86

7.4 Ambient conditions ............................................................ 86

7.5 Housing ............................................................................... 87

7.6 High pressure pump ........................................................... 87

7.7 Injection valve ..................................................................... 88

7.8 Peristaltic pump .................................................................. 88

7.9 Metrohm Suppressor Module (MSM) ............................... 88

7.10 Mains connection ............................................................... 89

7.11 Interfaces ............................................................................. 89

7.12 Safety specification ............................................................ 90

7.13 Electromagnetic compatibility (EMC) ................................ 90

7.14 Weight ................................................................................. 90

8Conformity and warranty 91

8.1 Declaration of Conformity ................................................. 91

8.2 Quality Management Principles ........................................ 92

8.3 Warranty (guarantee) ......................................................... 93

9Accessories 95

9.1 Scope of delivery ................................................................ 95

9.2 Optional accessories ........................................................ 104

Table of contents ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭

VI ￭￭￭￭￭￭￭￭ 882 Compact IC plus – Anion

Index 107

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ Table of figures

882 Compact IC plus – Anion ￭￭￭￭￭￭￭￭ VII

Table of figures

Figure 1 Front 882 Compact IC plus – Anion ................................................... 7

Figure 2 Rear 882 Compact IC plus – Anion .................................................... 8

Figure 3 Installation diagram 882 Compact IC plus – Anion ........................... 14

Figure 4 Connection of capillaries with pressure screws ................................ 16

Figure 5 leak sensor – plugging in ................................................................. 20

Figure 6 Drainage tubings ............................................................................. 21

Figure 7 Capillary and cable feed-throughs ................................................... 23

Figure 8 Installing eluent bottle attachment .................................................. 24

Figure 9 Mounting aspiration filter ................................................................ 25

Figure 10 Install tubing weighting and aspiration filter .................................... 25

Figure 11 Eluent aspiration tubing fully equipped. ........................................... 26

Figure 12 Eluent bottle – connected ............................................................... 27

Figure 13 Capillary connections high pressure pump/purge valve .................... 28

Figure 14 High pressure pump – Connect inlet ................................................ 29

Figure 15 Deaerate the high pressure pump .................................................... 31

Figure 16 Connecting the inline filter .............................................................. 33

Figure 17 Pulsation absorber – Connection ..................................................... 34

Figure 18 Injection valve – connected ............................................................. 35

Figure 19 Injection valve – Positions ................................................................ 36

Figure 20 Peristaltic pump ............................................................................... 37

Figure 21 Installing the pump tubing .............................................................. 38

Figure 22 Install pump tubing connection with filter ....................................... 39

Figure 23 Install pump tubing connection without filter .................................. 40

Figure 24 Suppressor – connection capillaries ................................................. 42

Figure 25 Pump head – removing the piston ................................................... 58

Figure 26 Components of the piston cartridge ................................................ 59

Figure 27 Tool for piston seal .......................................................................... 60

Figure 28 Removing the piston seal ................................................................. 61

Figure 29 Inserting the piston seal into the tool ............................................... 61

Figure 30 Inserting the piston seal into the pump head ................................... 62

Figure 31 Removing valves .............................................................................. 62

Figure 32 Dismantling valve ............................................................................ 64

Figure 33 Components of the inlet valve and outlet valve ................................ 65

Figure 34 Change filters (of the inline filter) ..................................................... 67

Figure 35 Pump tubing connection – Changing the filter ................................. 72

Figure 36 Parts of the suppressor .................................................................... 74

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