Agilent Technologies 1290 infinity Bedienungsanleitung

Agilent Technologies

Agilent 1290 Infinity

LC Injectors HTC/HTS

User Manual

Agilent 1290 Infinity LC Injectors HTC/HTS User Manual

Notices

No part of this manual may be reproduced

in any form or by any means (including elec-

tronic storage and retrieval or translation

into a foreign language) without prior agree-

ment and written consent from Agilent

Technologies, Inc. as governed by United

States and international copyright laws.

Manual Part Number

G4270-90000

Edition

12/2009

Printed in Germany

Agilent Technologies

Hewlett-Packard-Strasse 8

76337 Waldbronn

Warranty

The material contained in this docu-

ment is provided “as is,” and is sub-

ject to being changed, without notice,

in future editions. Further, to the max-

imum extent permitted by applicable

law, Agilent disclaims all warranties,

either express or implied, with regard

to this manual and any information

contained herein, including but not

limited to the implied warranties of

merchantability and fitness for a par-

ticular purpose. Agilent shall not be

liable for errors or for incidental or

consequential damages in connection

with the furnishing, use, or perfor-

mance of this document or of any

information contained herein. Should

Agilent and the user have a separate

written agreement with warranty

terms covering the material in this

document that conflict with these

terms, the warranty terms in the sep-

arate agreement shall control.

Technology Licenses

The hardware and/or software described in

this document are furnished under a license

and may be used or copied only in accor-

dance with the terms of such license.

Restricted Rights Legend

If software is for use in the performance of a

U.S. Government prime contract or subcon-

tract, Software is delivered and licensed as

“Commercial computer software” as

defined in DFAR 252.227-7014 (June 1995),

or as a “commercial item” as defined in FAR

2.101(a) or as “Restricted computer soft-

ware” as defined in FAR 52.227-19 (June

1987) or any equivalent agency regulation

or contract clause. Use, duplication or dis-

closure of Software is subject to Agilent

Technologies’ standard commercial license

terms, and non-DOD Departments and

Agencies of the U.S. Government will

receive no greater than Restricted Rights as

defined in FAR 52.227-19(c)(1-2) (June

1987). U.S. Government users will receive

no greater than Limited Rights as defined in

FAR 52.227-14 (June 1987) or DFAR

252.227-7015 (b)(2) (November 1995), as

applicable in any technical data.

Safety Notices

CAUTION

A CAUTION notice denotes a

hazard. It calls attention to an

operating procedure, practice, or

the like that, if not correctly per-

formed or adhered to, could

result in damage to the product

or loss of important data. Do not

proceed beyond a CAUTION

notice until the indicated condi-

tions are fully understood and

met.

WARNING

A WARNING notice denotes a

hazard. It calls attention to an

operating procedure, practice,

or the like that, if not correctly

performed or adhered to, could

result in personal injury or

death. Do not proceed beyond a

WARNING notice until the indi-

cated conditions are fully under-

stood and met.

For Research Use Only

Agilent 1290 Infinity LC Injectors HTC/HTS User Manual 3

Contents

1 General Information 5

Safety Information 6

How to Use this Manual 12

2 LC Injector HTC/HTS Operating Instructions 13

Using the Control Terminal 15

Methods 18

Job and Job Queue 21

Utility Functions 25

Logfile 35

Info Functions 36

Setup Functions 40

3 LC Injector HTC/HTS Description and Installation 43

General System Overview 45

Installation 50

Object Positions 87

Injection Valve 105

Interfacing the LC Injector HTC/HTS to other Devices 115

PAL Loader Program 118

Establishing Communication with Computer 119

Special Functions 125

Troubleshooting 146

Replacing Parts 166

Maintaining the LC Injector HTC/HTS System 172

4 Agilent 1290 Infinity LC Injectors HTC/HTS User Manual

Contents

4 Appendices 175

Definition of Terms 176

Conventions of Naming 179

Injection Cycles 180

DLW Principles and Operating Details 184

Software Flow Chart 232

External Connectors 239

Agilent 1290 Infinity LC Injectors HTC/HTS User Manual

Agilent Technologies

General Information

Safety Information 6

How to Use this Manual 12

6 Agilent 1290 Infinity LC Injectors HTC/HTS User Manual

1General Information

Safety Information

General

Considerations

The LC Injector HTC/HTS System User Manual and the corresponding

Addendum for a specific module must be consulted by the user under all

circumstances before a unit is put in use.

Changes or modifications to this unit not expressly approved by the party

responsible for compliance could void the user’s authority to operate the

equipment.

The user shall be made aware that if the equipment is used in a manner not

specified by the manufacturer, the protection provided by the equipment may

be impaired.

When using the LC Injector HTC/HTS System, follow the generally accepted

procedures for quality control and methods development.

When you use the LC Injector HTC/HTS System in the field of

chromatographic analysis and you observe a change in the retention of a

particular compound, in the resolution between two compounds, or in peak

shape, immediately determine the reason for the changes. Until you determine

the cause of a change, do not rely on the separation results.

Electrical

Hazards

Every analytical instrument has specific hazards, so be sure to read and

comply with the following precautions. They will help ensure the safe,

long-term use of your LC Injector HTC/HTS System.

The Installation Category (Over voltage Category) for this instrument is Level

II. The Level II Category pertains to equipment that receives its electrical

power from the local level, such as an electrical wall outlet.

Only use fuses of the type and current rating specified. Do not use repaired

fuses and do not short-circuit the fuse holder.

Agilent 1290 Infinity LC Injectors HTC/HTS User Manual 7

General Information 1

Safety Information

The supplied power cord must be inserted into a power outlet with a

protective earth contact (ground). When using an extension cord, make sure

that the cord also has an earth contact.

Do not change the external or internal grounding connections. Tampering

with or disconnecting these connections could endanger you and/or damage

the LC Injector HTC/HTS System.

The instrument is properly grounded in accordance with these regulations

when shipped. You do not need to make any changes to the electrical

connections or the instrument's chassis to ensure safe operation.

The combination of a LC Injector HTC/HTS System with a LC/MS System does

require the safety measure as described by the LC/MS System manufacturer.

Detailed instructions for the safety grounding on the LC/MS system are

outlined in the corresponding operating/installation manual.

Agilent Technologies recommends to use a grounding cable connected on one

side at the Injection Valve, Loop or any other suitable direct metallic contact

and the other side at an appropriate grounding point at the LC/MS System.

This supplementary grounding measure will support the safety strategy of the

LC/MS System manufacturer.

Do not turn the instrument on if you suspect that it has incurred any kind of

electrical damage. Instead disconnect the power cord and contact a Agilent

Technologies representative for a product evaluation. Do not attempt to use

the instrument until it has been evaluated. Electrical damage may have

occurred if the LC Injector HTC/HTS System shows visible signs of damage,

exposure to any liquids or has been transported under severe stress.

Damage can also result if the instrument is stored for prolonged periods under

unfavorable conditions (e.g. subjected to heat, water, etc.).

8 Agilent 1290 Infinity LC Injectors HTC/HTS User Manual

1General Information

Safety Information

In any case disconnect the power cord(s) from the power supply or from the

different power supplies if optional devices are installed before attempting

any type of maintenance.

Capacitors inside the instrument may still be charged even if the instrument is

turned off.

To avoid damaging electrical parts, do not disconnect an electrical assembly

while power is applied to the LC Injector HTC/HTS system. Once the power is

turned off, wait approximately 30 seconds before you disconnect an assembly.

The instrument includes a number of integrated circuits. These circuits may

be damaged if exposed to excessive line voltage fluctuations and/or power

surges.

Never try to repair or replace any components of the instrument that is not

described in this manual without the assistance of a Agilent Technologies

representative.

There are no operator-serviceable or replaceable parts inside the power

supply(ies) or in the LC Injector HTC/HTS System. If a power supply is not

functioning, contact a Agilent Technologies representative.

The power supply for the LC Injector HTC/HTS Instrument has the symbols

1/0 on the label for the power switch to switch ON/OFF.

Any additional power supply for other devices like, Cooled Stack or a Valve

Module shows the symbols as shown below on the label for the power switch:

The symbols shall warn the user that in a emergency case more than one

power supply has to be turned OFF or more than one power cord has to be

pulled from power supply or from the wall outlet to shut down the complete

LC Injector HTC/HTS System.

Agilent 1290 Infinity LC Injectors HTC/HTS User Manual 9

General Information 1

Safety Information

If the basic LC Injector HTC/HTS System is installed, than a single power

supply is installed only. Turning OFF the power supply or pulling this single

power cord in an emergency case will stop the complete LC Injector HTC/HTS

System.

It is important that the power supply (ies) are in a location where the power

ON and OFF switch is accessible and easy to operate, and where it is possible

to unplug the AC power cord from the power supply/wall outlet in case of

emergency.

Other Hazards

To avoid injury during LC Injector HTC/HTS System operation, keep your

hands away from the syringe.

Do not operate the LC Injector HTC/HTS System without the safety shield. The

safety shield must be installed for safe operation.

To avoid injury, observe safe laboratory practice when you handle solvents,

change tubing, or operate the LC Injector HTC/HTS System. Know the physical

and chemical properties of the solvents you use. See the Material Safety Sheets

from the manufacturer for the solvents in use.

Use caution when working with any polymer tubing under pressure:

•Always wear eye protection when near pressurized polymer tubing.

•Do not use polymer tubing that has been severely stressed or kinked.

•Do not use polymer tubing, in particular not PEEK or Tefzel tubing, with

Tetrahydrofuran (THF), Dimethylsulfoxid (DMSO), chlorinated organic

solvents, concentrated mineral acids, such as Nitric, Phosphoric or Sulfuric

acids, or any related compounds to above listings.

10 Agilent 1290 Infinity LC Injectors HTC/HTS User Manual

1General Information

Safety Information

Do not use vials without a sealing cap, microtiter or deepwell plates without a

plate seal. Vapor phase from organic solvents can be hazardous and

flammable. Acidic vapor phase can cause corrosion to critical mechanical

parts.

Disposal

Do not dispose of this equipment or parts thereof unsorted in municipal

waste. Follow local municipal waste ordinances for proper disposal provisions

to reduce the environmental impact of waste electrical and electronic

equipment (WEEE). European Union customers: Call your local customer

service representative responsible for the PAL System for complimentary

equipment pick-up and recycling.

Lithium battery

An onboard lithium battery buffers the electronic memories, when the

instrument is turned off. Replace it only with the same or equivalent type

recommended by the equipment manufacturer.

Battery: Panasonic VL 2330, soldered directly on the electronic board.

Discharged lithium batteries shall be disposed off locally according to national

waste disposal regulations for batteries.

There are no operator-serviceable parts on the electronic boards. If an

electronic board fails, contact a Agilent Technologies representative.

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