Agilent Technologies InfinityLab LC Series Bedienungsanleitung

1290 Infinity II

Preparative Open-Bed Fraction Collector

Agilent InfinityLab LC Series

User Manual

1290 Infinity II Preparative Open-Bed Fraction Collector User Manual

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1290 Infinity II Preparative

Open-Bed Fraction Collector

User Manual

1290 Infinity II Preparative Open-Bed Fraction Collector User Manual 3

In This Guide

This manual contains technical reference information about the Agilent 1290

Infinity II Preparative Open-Bed Fraction Collector (G7159B).

1Introduction

This chapter gives an introduction to the module and an instrument overview.

2 Site Requirements and Specifications

This chapter provides information on environmental requirements, physical and

performance specifications.

3 Using the Fraction Collector

This chapter explains the essential operational parameters of the module.

4 Preparing the Fraction Collector

This chapter explains the operational parameters of the module.

5Troubleshootingand Diagnostics

This chapter gives an overview about the troubleshooting and diagnostic features

and the different user interfaces.

6ErrorInformation

This chapter describes the meaning of error messages, and provides information

on probable causes and suggested actions how to recover from error conditions.

7 Maintenance

This chapter describes the maintenance of the module.

8 Parts for Maintenance and Repair

This chapter provides information on parts for maintenance and repair.

1290 Infinity II Preparative Open-Bed Fraction Collector User Manual 4

9IdentifyingCables

This chapter provides information on cables used with the module.

10 Hardware Information

This chapter describes the module in more detail on hardware and electronics.

11 Appendix

This chapter provides additional information on safety, legal, and web.

1290 Infinity II Preparative Open-Bed Fraction Collector User Manual 5

Contents

1Introduction8

Intended Use 9

Product Description 10

Features 11

Overview of the Module 12

Fraction Collector Principle 13

Leak and Waste Concept 14

2 Site Requirements and Specifications 16

Site Requirements 17

Physical Specifications 22

Performance Specifications 23

3 Using the Fraction Collector 27

Warnings and Cautions 28

Solvent Information 29

Turn on/off 36

Status Indicators 37

Drawer Status Indicator 38

Exchange Drawers 39

Exchange Containers 41

Replace Inlet/Waste Tubings 43

Configuration and Operation of the Open Bed Fraction Collector 47

Prepare the Module for Transportation 61

1290 Infinity II Preparative Open-Bed Fraction Collector User Manual 6

4 Preparing the Fraction Collector 63

Best Practices 64

Capillary Color Coding Guide 65

Swage Fittings 66

Setting up the Fraction Collector with the Instrument Control Interface 68

Method Parameter Settings 74

Pooling 82

5 Troubleshooting and Diagnostics 83

User Interfaces 84

Agilent Lab Advisor Software 85

6ErrorInformation86

What Are Error Messages 87

General Error Messages 88

7 Maintenance 95

Introduction to Maintenance 96

Warnings and Cautions 97

Cleaning the Module 99

Overview of Maintenance 100

Install and Remove the Top Fume Hood 101

Clean the Leak Pan 103

Replace the Dripping Adapter for the Fraction Valve 104

Replace the Module Firmware 106

8 Parts for Maintenance and Repair 107

Supported Containers 108

List of Recommended Fraction Tubes 109

Fraction Collector Accessory Kit 110

Tubing Kits 111

Top Fume Hood Kit 115

1290 Infinity II Preparative Open-Bed Fraction Collector User Manual 7

9IdentifyingCables116

Cable Overview 117

Analog Cables 119

Remote Cables 121

CAN/LAN Cables 125

RS-232 Cables 126

USB 127

10 Hardware Information 128

Firmware Description 129

Electrical Connections 132

Interfaces 134

Setting the 6-bit Configuration Switch 141

Early Maintenance Feedback 145

Instrument Layout 146

11 Appendix 147

General Safety Information 148

Waste Electrical and Electronic Equipment (WEEE) Directive 154

Radio Interference 155

Sound Emission 156

Agilent Technologies on Internet 157

1290 Infinity II Preparative Open-Bed Fraction Collector User Manual 8

1Introduction

Intended Use 9

Product Description 10

Features 11

Overview of the Module 12

Fraction Collector Principle 13

Leak and Waste Concept 14

Leak Sensor 15

This chapter gives an introduction to the module and an instrument overview.

1290 Infinity II Preparative Open-Bed Fraction Collector User Manual 9

1Introduction

Intended Use

The 1290 Infinity II Preparative Open-Bed Fraction Collector is designed to be

used in combination with other InfinityLab LC modules in a preparative-scale

HPLC system to separate and purify inorganic or organic compounds via

reversed-phase chromatography applications. The module can collect fractions

of desired volume for sample purification or for later analysis.

The product is intended to be used by professional laboratory users.

1290 Infinity II Preparative Open-Bed Fraction Collector User Manual 10

1Introduction

Product Description

The Agilent 1290 Infinity II Preparative Open-Bed Fraction Collector is the ideal

solution that automatically manages high-capacity fraction collection of purified

peaks for semi-preparative and preparative scale purification. Collect milligrams

to multi-gram quantities of sample intuitive with ease. The Agilent 1290 Infinity II

Preparative Open-Bed Fraction Collector features handling a wide variety of

collection vessels with ease and capacity of up to 5.9 L by using 150 x 25 mm (L

x OD). The containers use identification tags to automatically detect the vessel

dimensions. With a novel robotic technology, Y-, Z-, theta-axis probe functionality

minimizes sample carryover between the fractions during movements between

the vessels. The Agilent 1290 Infinity II Preparative Open-Bed Fraction Collector

is optimized for flow rates up to 200 mL/min, and can be easily integrated with

any Agilent solvent delivery module, autosampler, or detector. For

high-throughput applications, you can combine up to three fraction collectors in a

single LC system. Scale up your fraction capacity based on your demand up to a

maximum of 1296 fractions.

Figure 1 Overview of the open-bed fraction collector

Status indicator

Container

Drawer

Power switch

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