Agilent Technologies 4100 Bedienungsanleitung

Agilent Microwave

Plasma Atomic

Emission

Spectrometers

For models 4100, 4200,

and 4210

User’s Guide

2 Agilent Microwave Plasma Atomic Emission Spectrometers User’s Guide

Notices

2013, 2016, 2018

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Agilent Technologies, Inc. as governed

by United States and international

Guide Part Number

G8000-90002

Edition

Fourth edition, July 2018

Agilent Technologies Australia [M] Pty

Ltd

679 Springvale Road, Mulgrave,

Victoria, Australia. 3170

www.agilent.com

Printed in Malaysia

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the manner described in the Agilent

product user guides. Any other use

may result in damage to the product

or personal injury. Agilent is not

responsible for any damages caused,

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(November 1995), as applicable in any

technical data.

Safety Notices

A CAUTION notice denotes a hazard.

It calls attention to an operating

procedure, practice, or the like that, if

not correctly performed or adhered to,

could result in damage to the product

or loss of important data. Do not

proceed beyond a CAUTION notice

until the indicated conditions are fully

understood and met.

A WARNING notice denotes a

hazard. It calls attention to an

operating procedure, practice, or the

like that, if not correctly performed

or adhered to, could result in

personal injury or death. Do not

proceed beyond a WARNING notice

until the indicated conditions are

fully understood and met.

WARNING

CAUTION

Contents

Agilent Microwave Plasma Atomic Emission Spectrometers User’s Guide 3

Contents

1. Safety Practices and Hazards 7

General 7

Verifying Safe State 8

Plasma 9

Heat, Vapors and Fumes 10

Compressed Gas Hazards 10

Dangerous Goods 11

Electrical Hazards 11

Other Precautions 12

Warning Symbols 12

Color Coding 14

CE Compliance 14

Electromagnetic Compatibility 15

EN55011/CISPR11 15

South Korean Class A EMC declaration 16

ICES/NMB-001 16

2. Introduction 17

Site Preparation Requirements 17

User Documentation 17

Conventions 18

Notes and tips 18

Contents

4 Agilent Microwave Plasma Atomic Emission Spectrometers User’s Guide

Specifications 18

Installation category 18

Pollution level 18

Environmental conditions 19

Electrical power supplies 19

Gas supplies 20

Exhaust system 21

MP-AES instrument cooling air supply 22

Drain vessel 22

Personal computer requirements 23

Weights and dimensions 23

3. Installation 25

Agilent MP-AES Instrument Overview 26

Installing the MP Expert Software 28

Hardware Components Replacement 29

Accessories 30

Organic solvents kit 30

External Gas Control Module (EGCM) 31

SPS 3 and SPS 4 Autosampler 31

Advanced Valve System (AVS) 4 31

SVS 1/1+ 32

SVS 2 32

Agilent 4107 Nitrogen Generator 32

Multimode sample introduction system (MSIS) 33

Monochromator air purge 34

4. Operation 35

Analysis Checklist 35

Contents

Agilent Microwave Plasma Atomic Emission Spectrometers User’s Guide 5

Turning On the MP-AES Instrument and Software 36

Preparing for Analysis 37

MP-AES Instrument Wavelength Calibration 38

Creating/Opening a Worksheet 39

Creating a new worksheet 39

Opening an existing worksheet 40

Creating a new worksheet from a template 40

Developing a Method 40

Running Samples 42

Printing a Report 43

Turning Off the MP-AES instrument 43

5. Maintenance, Spare Parts and Troubleshooting 47

Routine Maintenance 48

Cleaning the MP-AES Instrument 49

Cleaning the MP-AES Easy Fit Torch 49

Cleaning the Spray Chamber 50

Checking the Gas Supply Tubing for Leaks 51

Spare Parts 51

Technical Support 52

Troubleshooting 52

Contents

6 Agilent Microwave Plasma Atomic Emission Spectrometers User’s Guide

This page is intentionally left blank.

Safety Practices and Hazards

Agilent Microwave Plasma Atomic Emission Spectrometers User’s Guide 7

1. Safety Practices and Hazards

General 7

Verifying Safe State 8

Plasma 9

Heat, Vapors and Fumes 10

Compressed Gas Hazards 10

Electrical Hazards 11

Other Precautions 12

Warning Symbols 12

Color Coding 14

CE Compliance 14

Electromagnetic Compatibility 15

ICES/NMB-001 16

General

Unless otherwise specified, statements in this manual apply to the

Agilent 4100, 4200, and 4210 MP-AES instruments.

Operation of an Agilent Microwave Plasma Atomic Emission

Spectrometer (MP-AES) involves the use of compressed gases, high

microwave energy and hazardous materials including corrosive fluids

and flammable liquids. Careless, improper or unskilled use of this

instrument can cause death or serious injury to personnel, and/or

severe damage to equipment and property. Only trained personnel

should use this equipment.

Safety Practices and Hazards

8 Agilent Microwave Plasma Atomic Emission Spectrometers User’s Guide

The MP-AES instrument incorporates interlocks and covers that are

designed to prevent inadvertent contact with any potential hazards.

If the MP-AES instrument is used in any manner not specified by

Agilent, this protection may be impaired. It is good practice to

develop safe working habits that do not depend upon the correct

operation of the interlocks for safe operation. It is essential that no

interlock or cover is bypassed, damaged or removed.

The safety practices described below are provided to help the user

operate the MP-AES instrument safely. Read each safety topic

thoroughly before attempting to operate the MP-AES instrument and

always operate the MP-AES instrument in accordance with these

safety practices.

If you are unsure of the effects of any liquid, gas or chemical on the

MP-AES instrument, consult your Agilent field service engineer or

approved representative before use.

If the MP-AES instrument is to be used in conjunction with other

non-Agilent equipment, the safety requirements of any system

incorporating the MP-AES instrument is the responsibility of the

assembler of the system.

Verifying Safe State

The following general safety precautions must be observed during all

phases of operation, maintenance and service of this instrument.

To ensure continued safety of the instrument after maintenance or

service procedures verify the instrument is returned to a safe state

before use. This includes running performance checks to verify the

instruments safety systems are functioning correctly. Check the

general condition of the instrument during operation for wear or

signs of corrosion that are likely to inhibit function or safety.

Failure to comply with these precautions or with specific warnings

elsewhere in this manual violates safety standards of design,

manufacture, and intended use of the instrument. Agilent

Technologies assumes no liability for the customer’s failure to

comply with these requirements.

Safety Practices and Hazards

Agilent Microwave Plasma Atomic Emission Spectrometers User’s Guide 9

Plasma

The plasma is extremely hot (about 6,000 °C, 11,000 °F) and operates

using high levels of microwave energy. The plasma emits high

intensity light. Always wear appropriate eye protection if viewing the

plasma. Close contact with the operating plasma can result in severe

heat burns to the skin, and exposure to microwave radiation can

cause sub-surface skin burns.

Do not operate the plasma if:

the microwave excitation assembly appears to be damaged

foreign material is present in the viewing port (left end of the

microwave excitation assembly) or the torch aperture (vertical

space for the torch)

the space above the chimney is not clear of objects

the MP-AES instrument exhaust system is not connected or

turned on

The microwave excitation assembly is designed to reduce microwave

radiation to safe levels while still permitting easy installation of the

torch and viewing of the plasma. The MP-AES instrument has an

interlock system that is designed to extinguish the plasma if either

the pre-optics window holder is opened or the torch is unloaded

before the plasma has been extinguished. Do not attempt to bypass

the interlock system.

Before opening the pre-optics window holder or unloading the torch,

extinguish the plasma by:

pressing SHIFT and F5 on the keyboard

selecting the ‘Plasma off’ option from the ‘Plasma’ drop-down

arrow on the MP Expert software toolbar

pressing the Plasma Enable switch on the front of the MP-AES

instrument

The torch remains hot for up to five minutes after the plasma is

extinguished. Touching the torch before it has cooled sufficiently may

result in burns. Allow the torch to cool before removing it from the

loader.

Safety Practices and Hazards

10 Agilent Microwave Plasma Atomic Emission Spectrometers User’s Guide

The plasma system has been carefully designed to operate safely and

effectively when using torches and related components that conform

to Agilent’s design criteria. Use of non-approved components in the

MP-AES instrument may render the system inoperative and/or

hazardous. It may also invalidate the warranty on the MP-AES

instrument. Use only torches and related components supplied or

authorized by Agilent.

Heat, Vapors and Fumes

Heat, ozone, vapors and fumes generated by the plasma can be

hazardous, and must be extracted from the MP-AES instrument by

means of an exhaust system. Ensure that an exhaust system of the

appropriate type is fitted (as specified in the site preparation guide).

The system must be vented to the outside in accordance with local

regulations and never within the building. Regularly check the

exhaust system by smoke test to ensure that the exhaust system is

functioning correctly. The exhaust fan must always be switched on

before igniting the plasma.

Compressed Gas Hazards

All compressed gases (other than air) can create a hazard if they leak

into the atmosphere. Even small leaks in gas supply systems can be

dangerous. Any leak (except that of air) can result in an oxygen-

deficient atmosphere which can cause asphyxiation. The storage area

must be adequately ventilated and must comply with the rules and

regulations imposed by the local authorities responsible for such use

in the workplace.

Gas cylinders must be stored and handled strictly in accordance with

local safety codes and regulations. Cylinders must be used and stored

only in a vertical position and secured to an immovable structure or

a properly constructed cylinder stand. Move cylinders only by

securing them to a properly constructed trolley.

If gases are to be plumbed from a remote storage area to the

instrument site, ensure that the local outlets are fitted with stop

valves, pressure gauges and suitable regulators that are easily

accessible to the instrument operator. The gas outlets must be

provided within 1.5 meters (5 feet) of the MP-AES instrument.

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