Agilent Technologies InfinityLab LC Series Bedienungsanleitung

Agilent Technologies

Agilent InfinityLab LC Series

Vialsamplers

User Manual

Agilent InfinityLab LC Series Vialsamplers User Manual

Notices

No part of this manual may be reproduced

in any form or by any means (including

electronic storage and retrieval or transla-

tion into a foreign language) without prior

agreement and written consent from Agi-

lent Technologies, Inc. as governed by

United States and international copyright

laws.

Manual Part Number

G7129-90010 Rev. D

Edition

08/2018

Printed in Germany

Agilent Technologies

Hewlett-Packard-Strasse 8

76337 Waldbronn

Warranty

The material contained in this docu-

ment is provided “as is,” and is sub-

ject to being changed, without notice,

in future editions. Further, to the max-

imum extent permitted by applicable

law, Agilent disclaims all warranties,

either express or implied, with regard

to this manual and any information

contained herein, including but not

limited to the implied warranties of

merchantability and fitness for a par-

ticular purpose. Agilent shall not be

liable for errors or for incidental or

consequential damages in connection

with the furnishing, use, or perfor-

mance of this document or of any

information contained herein. Should

Agilent and the user have a separate

written agreement with warranty

terms covering the material in this

document that conflict with these

terms, the warranty terms in the sep-

arate agreement shall control.

Technology Licenses

The hardware and/or software described in

this document are furnished under a

license and may be used or copied only in

accordance with the terms of such license.

Restricted Rights Legend

If software is for use in the performance of

a U.S. Government prime contract or sub-

contract, Software is delivered and licensed

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or as a “commercial item” as defined in

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software” as defined in FAR 52.227-19

(June 1987) or any equivalent agency regu-

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or disclosure of Software is subject to Agi-

lent Technologies’ standard commercial

license terms, and non-DOD Departments

and Agencies of the U.S. Government will

receive no greater than Restricted Rights as

defined in FAR 52.227-19(c)(1-2) (June

1987). U.S. Government users will receive

no greater than Limited Rights as defined in

FAR 52.227-14 (June 1987) or DFAR

252.227-7015 (b)(2) (November 1995), as

applicable in any technical data.

Safety Notices

CAUTION

A CAUTION notice denotes a

hazard. It calls attention to an

operating procedure, practice, or

the like that, if not correctly per-

formed or adhered to, could

result in damage to the product

or loss of important data. Do not

proceed beyond a CAUTION

notice until the indicated condi-

tions are fully understood and

met.

WARNING

A WARNING notice denotes a

hazard. It calls attention to an

operating procedure, practice,

or the like that, if not correctly

performed or adhered to, could

result in personal injury or

death. Do not proceed beyond a

WARNING notice until the indi-

cated conditions are fully

understood and met.

Agilent InfinityLab LC Series Vialsamplers User Manual 3

In This Book:

This manual covers the following modules:

•Agilent 1260 Infinity II Vialsampler (G7129A)

•Agilent 1290 Infinity II Vialsampler (G7129B)

•Agilent 1260 Infinity II Vialsampler (G7129C)

1Introduction

This chapter gives an introduction to the module and instrument overview.

2 Site Requirements and Specifications

This chapter provides information on environmental requirements, physical

and performance specifications.

3 Using the Module

This chapter provides information on how to use the module.

4 Installation of the Optional Sample Cooler or Thermostat

This chapter describes the installation of the optional sample cooler or

thermostat.

5 Preparing the Module

This chapter explains the operational parameters of the module.

6 Optimizing Performance

This chapter provides information on how to optimize the module.

7 Troubleshooting and Diagnostics

Overview about the troubleshooting and diagnostic features.

4 Agilent InfinityLab LC Series Vialsamplers User Manual

In This Book:

8 Error Information

This chapter describes the meaning of error messages, and provides

information on probable causes and suggested actions how to recover from

error conditions.

9 Maintenance and Repair

This chapter describes the maintenance and the repair of the module.

10 Parts and Materials for Maintenance

This chapter provides information on parts for maintenance.

11 Identifying Cables

This chapter provides information on cables used with the Agilent 1200

Infinity Series modules.

12 Hardware Information

This chapter describes the detector in more detail on hardware and

electronics.

13 LAN Configuration

This chapter provides information on connecting the module to the Agilent

ChemStation PC.

14 Appendix

This chapter provides addition information on safety, legal and web.

Agilent InfinityLab LC Series Vialsamplers User Manual 5

Contents

1Introduction 9

Product Description (G7129A) 10

Features (G7129A) 11

Product Description (G7129B) 12

Features (G7129B) 13

Product Description (G7129C) 14

Features (G7129C) 15

Overview of the Module 16

Operating Principle 18

Leak and Waste Handling 28

2 Site Requirements and Specifications 35

Site Requirements 36

Physical Specifications 40

Performance Specifications 41

Specifications of the Sample Cooler 47

Specifications of the Sample Thermostat 49

Specifications of the Integrated Column Compartment 51

3 Using the Module 53

Magnets 54

Turn on/off 55

Status Indicators 57

Exchange Drawers 58

Install the Integrated Column Compartment 60

Install the Column Shelf 66

Install the External Tray 70

Install a Column (ICC) 72

Remove a Column (ICC) 76

Sample Trays 78

Choice of Vials and Caps 81

Transporting the Sampler with a Sample Cooler or Sample Thermostat Installed 84

Agilent Local Control Modules 86

6 Agilent InfinityLab LC Series Vialsamplers User Manual

Contents

4 Installation of the Optional Sample Cooler or Thermostat 89

Damaged Packaging 90

Install the Sample Cooler or Thermostat 91

Using the Sample Cooler or Thermostat in an Infinity II Sampler 97

5 Preparing the Module 105

Leak and Waste Handling 106

Preparing the Module 107

Solvent Information 108

Capillary Color Coding Guide 114

Installing Capillaries 115

Flow Connections to the Vialsampler 117

Setting up the Vialsampler 119

6 Optimizing Performance 131

Optimization for Lowest Carry-over 132

Fast Injection Cycle and Low Delay Volume 136

Precise Injection Volume 138

Choice of Rotor Seal 140

7 Troubleshooting and Diagnostics 141

Overview of the Module’s Indicators and Test Functions 142

Maintenance Functions 144

Step Commands 153

Test s 155

Troubleshooting 156

Troubleshooting Guide for the Sample Transport Assembly 158

Agilent Lab Advisor Software 161

8 Error Information 163

What are Error Messages 165

General Error Messages 166

Sampler Error Messages 172

Sample Cooler Error Messages 180

Integrated Column Compartment (ICC) Heater Error Messages 183

Agilent InfinityLab LC Series Vialsamplers User Manual 7

Contents

9 Maintenance and Repair 185

Introduction to Maintenance 186

Warnings and Cautions 187

Overview of Maintenance 189

Cleaning the Module 190

Remove and Install Doors 191

Exchange the Needle Assembly 192

Exchange the Needle Seat Assembly 197

Exchange the Sample Loop Assembly 202

Exchange the Rotor Seal 206

Exchange the Metering Seal and Piston 212

Exchange the Gripper Arm 216

Replace the Peristaltic Pump Cartridge 219

Exchange the Wash Port Assembly 222

Replace the Module Firmware 228

10 Parts and Materials for Maintenance 229

Main Assemblies 230

Standard Parts 232

Drawer Assembly 233

External Tray 235

Analytical Head Assembly (40 μL) 236

Analytical Head Assembly (100 µL) 237

2ps 6pt Injection Valve 1300 bar 238

2ps 6pt Injection Valve 800 bar 239

2ps 6pt Injection Valve 600 bar 240

Integrated Column Compartment 241

Cabinet Kit 242

Sample Thermostat 244

Standard Vialsampler Accessory Kit 246

Multi-Draw Kit 248

Additional Part List 249

Column Identifier Kit 2C (G4751A) 250

8 Agilent InfinityLab LC Series Vialsamplers User Manual

Contents

11 Identifying Cables 251

Cable Overview 252

Analog Cables 254

Remote Cables 256

CAN/LAN Cables 260

RS-232 Cables 261

USB 262

12 Hardware Information 263

Firmware Description 264

Electrical Connections 267

Interfaces 269

Setting the 6-bit Configuration Switch 277

Instrument Layout 281

Early Maintenance Feedback (EMF)282

13 LAN Configuration 283

What You Have to Do First 284

TCP/IP parameter configuration 285

Configuration Switches 286

Initialization Mode Selection 287

Dynamic Host Configuration Protocol (DHCP) 289

Manual Configuration 292

PC and Agilent ChemStation Setup 297

14 Appendix 307

General Safety Information 308

Waste Electrical and Electronic Equipment (WEE) Directive 314

Refrigerant 315

Radio Interference 318

Sound Emission 319

Solvent Information 320

Agilent Technologies on Internet 321

Agilent InfinityLab LC Series Vialsamplers User Manual

Agilent Technologies

Introduction

Product Description (G7129A) 10

Features (G7129A) 11

Product Description (G7129B) 12

Features (G7129B) 13

Product Description (G7129C) 14

Features (G7129C) 15

Overview of the Module 16

Operating Principle 18

Sampling Sequence 18

Needle Parkstation 23

Hydraulic Box 24

Transport Assembly 26

Leak and Waste Handling 28

Leak Sensor 32

Waste Guidance 32

Waste Concept 33

This chapter gives an introduction to the module and instrument overview.

10 Agilent InfinityLab LC Series Vialsamplers User Manual

Introduction

Product Description (G7129A)

The Agilent 1260 Infinity II Vialsampler is designed for the reliability, safety,

and ease-of-use needed for routine pharmaceutical tasks and quality control,

as well as for environmental and food analyses. It can house optionally the

integrated column compartment for two LC columns with temperature control

up to 80 °C as well as a sample cooler/sample thermostat for stable

temperatures down to 4 °C or from 4 °C up to 40 °C, all within one module.

Figure 1 Overview of the Vialsampler

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