Agilent Technologies 1290 Infinity II Bedienungsanleitung

Agilent Technologies

Agilent InfinityLab LC Series

1290 Infinity II

MS Flow Modulator

User Manual

MS Flow Modulator User Manual

Notices

No part of this manual may be reproduced

in any form or by any means (including

electronic storage and retrieval or transla-

tion into a foreign language) without prior

agreement and written consent from Agi-

lent Technologies, Inc. as governed by

United States and international copyright

laws.

Manual Part Number

G7170-90000

Edition

09/2017

Printed in Germany

Agilent Technologies

Hewlett-Packard-Strasse 8

76337 Waldbronn

Warranty

The material contained in this docu-

ment is provided “as is,” and is sub-

ject to being changed, without notice,

in future editions. Further, to the max-

imum extent permitted by applicable

law, Agilent disclaims all warranties,

either express or implied, with regard

to this manual and any information

contained herein, including but not

limited to the implied warranties of

merchantability and fitness for a par-

ticular purpose. Agilent shall not be

liable for errors or for incidental or

consequential damages in connection

with the furnishing, use, or perfor-

mance of this document or of any

information contained herein. Should

Agilent and the user have a separate

written agreement with warranty

terms covering the material in this

document that conflict with these

terms, the warranty terms in the sep-

arate agreement shall control.

Technology Licenses

The hardware and/or software described in

this document are furnished under a

license and may be used or copied only in

accordance with the terms of such license.

Restricted Rights Legend

If software is for use in the performance of

a U.S. Government prime contract or sub-

contract, Software is delivered and licensed

as “Commercial computer software” as

defined in DFAR 252.227-7014 (June 1995),

or as a “commercial item” as defined in

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software” as defined in FAR 52.227-19

(June 1987) or any equivalent agency regu-

lation or contract clause. Use, duplication

or disclosure of Software is subject to Agi-

lent Technologies’ standard commercial

license terms, and non-DOD Departments

and Agencies of the U.S. Government will

receive no greater than Restricted Rights as

defined in FAR 52.227-19(c)(1-2) (June

1987). U.S. Government users will receive

no greater than Limited Rights as defined in

FAR 52.227-14 (June 1987) or DFAR

252.227-7015 (b)(2) (November 1995), as

applicable in any technical data.

Safety Notices

CAUTION

A CAUTION notice denotes a

hazard. It calls attention to an

operating procedure, practice, or

the like that, if not correctly per-

formed or adhered to, could

result in damage to the product

or loss of important data. Do not

proceed beyond a CAUTION

notice until the indicated condi-

tions are fully understood and

met.

WARNING

A WARNING notice denotes a

hazard. It calls attention to an

operating procedure, practice,

or the like that, if not correctly

performed or adhered to, could

result in personal injury or

death. Do not proceed beyond a

WARNING notice until the indi-

cated conditions are fully

understood and met.

MS Flow Modulator User Manual 3

In This Guide…

This manual covers the Agilent InfinityLab LC Series 1290 Infinity II MS Flow

Modulator (G7170B)

1Introduction

This chapter gives an introduction to the module.

2 Site Requirements and Specifications

This chapter provides information on environmental requirements, physical

and performance specifications.

3 Installing the Module

This chapter gives information about the installation of the valve drive and the

valve heads.

4 Using the Module

This chapter provides information on how to use the module.

5 Troubleshooting and Diagnostics

Overview about the troubleshooting and diagnostic features.

6 Error Information

This chapter describes the meaning of error messages, and provides

information on probable causes and suggested actions how to recover from

error conditions.

7 Maintenance

This chapter describes the maintenance of the module.

8 Parts and Materials

This chapter provides information on parts for maintenance.

4 MS Flow Modulator User Manual

In This Guide…

9 Identifying Cables

This chapter provides information on cables used with the modules.

10 Hardware Information

This chapter describes the module in more detail on hardware and electronics.

11 Appendix

This chapter provides addition information on safety, legal and web.

MS Flow Modulator User Manual 5

Contents

1Introduction 7

1290 Infinity II MS Flow Modulator 8

Features (G7170B) 9

Leak and Waste (G7170B) 10

Operating Principle 11

2 Site Requirements and Specifications 13

Site Requirements 14

Physical Specifications 17

Performance Specifications 18

3 Installing the Module 19

Unpacking the Module 20

Installation of the MS Flow Modulator 21

4 Using the Module 31

Overview 32

Solvent Information 33

Status Indicator 40

Leak and Waste Handling 41

Configure the Flow Modulator 43

5 Troubleshooting and Diagnostics 47

User Interfaces 48

Agilent Lab Advisor Software 49

6 Error Information 51

What Are Error Messages 52

General Error Messages 53

Module Specific Error Messages 58

6 MS Flow Modulator User Manual

Contents

7 Maintenance 61

Introduction to Maintenance 62

Warnings and Cautions 63

Cleaning the Module 64

Replacing the Fuses of the Infinity Valve Drive 65

Replace Rotor and Stator 67

Replace Valve Heads 70

Replacing the Module Firmware 74

8 Parts and Materials 77

Accessory Kit for the Flow Modulator 78

Optional Parts 80

9 Identifying Cables 81

Cable Overview 82

Analog Cables 84

Remote Cables 86

CAN/LAN Cables 90

Agilent Module to PC 91

USB 92

10 Hardware Information 93

Electrical Connections 94

Interfaces 96

Config Switch Settings of the Infinity Valve Drive 102

11 Appendix 105

General Safety Information 106

Waste Electrical and Electronic Equipment (WEEE) Directive (2002-96-EC) 113

Radio Interference 114

Sound Emission 115

Agilent Technologies on Internet 116

MS Flow Modulator User Manual

Agilent Technologies

Introduction

1290 Infinity II MS Flow Modulator 8

Features (G7170B) 9

Leak and Waste (G7170B) 10

Operating Principle 11

This chapter gives an introduction to the module.

8 MS Flow Modulator User Manual

Introduction

1290 Infinity II MS Flow Modulator

Based on technology in our InfinityLab Quick Change valves, the 1290 Infinity

II MS Flow Modulator facilitates efficient flow control for mass-based fraction

collection on all InfinityLab LC Purification Solutions. The Flow Modulator is

a compact module suitable for flow rates up to 100 mL/min and supports split

ratios between 40:1 and 400000:1 with split frequencies up to 2 Hz.

Figure 1 Overview of the MS flow modulator

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MS Flow Modulator User Manual 9

Introduction

Features (G7170B)

Purification efficiency

•Supports wide range of split modes from 40:1 up to 400000:1 depending on

flow rate

•Enables split frequencies of up to 2 Hz

•Handles flow rates up to 100 mL/min

Instrument efficiency

•Integrates into any InfinityLab LC Purification Solution through CAN-bus

technology

•Supported by Agilent drivers – no additional software or macros required

Laboratory efficiency

•Compact design and easy connection to any InfinityLab LC Purification

Solution saves bench space

•Compatible with all InfinityLab LC Purification Solutions, enabling upgrade

to mass-based fraction collection when needs demand

•Integrates seamlessly in OpenLAB CDS ChemStation for familiar and

reliable operation

10 MS Flow Modulator User Manual

Introduction

Leak and Waste (G7170B)

NOTE

This example shows the leak and waste concept of the module, if installed to a leak tray and attached to

another module.

Alternatively, the module can be installed and integrated to the leak and waste concept of 1290 Infinity II

Preparative Column Compartment.

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