Agilent Technologies 1290 infinity Bedienungsanleitung

Agilent Technologies

Agilent 1290 Infinity

Valve Drive and Valve Heads

User Manual

Agilent 1290 Infinity Valve Drive and Valve Heads

Notices

No part of this manual may be reproduced

in any form or by any means (including elec-

tronic storage and retrieval or translation

into a foreign language) without prior agree-

ment and written consent from Agilent

Technologies, Inc. as governed by United

States and international copyright laws.

Manual Part Number

G1170-90001 Rev. B

Edition

05/2012

Printed in Germany

Agilent Technologies

Hewlett-Packard-Strasse 8

76337 Waldbronn

This product may be used as a com-

ponent of an in vitro diagnostic sys-

tem if the system is registered with

the appropriate authorities and com-

plies with the relevant regulations.

Otherwise, it is intended only for gen-

eral laboratory use.

Warranty

The material contained in this docu-

ment is provided “as is,” and is sub-

ject to being changed, without notice,

in future editions. Further, to the max-

imum extent permitted by applicable

law, Agilent disclaims all warranties,

either express or implied, with regard

to this manual and any information

contained herein, including but not

limited to the implied warranties of

merchantability and fitness for a par-

ticular purpose. Agilent shall not be

liable for errors or for incidental or

consequential damages in connection

with the furnishing, use, or perfor-

mance of this document or of any

information contained herein. Should

Agilent and the user have a separate

written agreement with warranty

terms covering the material in this

document that conflict with these

terms, the warranty terms in the sep-

arate agreement shall control.

Technology Licenses

The hardware and/or software described in

this document are furnished under a license

and may be used or copied only in accor-

dance with the terms of such license.

Restricted Rights Legend

If software is for use in the performance of a

U.S. Government prime contract or subcon-

tract, Software is delivered and licensed as

“Commercial computer software” as

defined in DFAR 252.227-7014 (June 1995),

or as a “commercial item” as defined in FAR

2.101(a) or as “Restricted computer soft-

ware” as defined in FAR 52.227-19 (June

1987) or any equivalent agency regulation

or contract clause. Use, duplication or dis-

closure of Software is subject to Agilent

Technologies’ standard commercial license

terms, and non-DOD Departments and

Agencies of the U.S. Government will

receive no greater than Restricted Rights as

defined in FAR 52.227-19(c)(1-2) (June

1987). U.S. Government users will receive

no greater than Limited Rights as defined in

FAR 52.227-14 (June 1987) or DFAR

252.227-7015 (b)(2) (November 1995), as

applicable in any technical data.

Safety Notices

CAUTION

A CAUTION notice denotes a

hazard. It calls attention to an

operating procedure, practice, or

the like that, if not correctly per-

formed or adhered to, could

result in damage to the product

or loss of important data. Do not

proceed beyond a CAUTION

notice until the indicated condi-

tions are fully understood and

met.

WARNING

A WARNING notice denotes a

hazard. It calls attention to an

operating procedure, practice,

or the like that, if not correctly

performed or adhered to, could

result in personal injury or

death. Do not proceed beyond a

WARNING notice until the indi-

cated conditions are fully under-

stood and met.

Agilent 1290 Infinity Valve Drive and Valve Heads 3

Contents

1 Introduction to the Agilent 1290 Infinity Valve Drive and Valve Heads 7

Overview of the Valve Drive 8

Overview of the Agilent Quick Change Valve Heads 12

Typical Applications 13

Bio-inert Materials 21

Early Maintenance Feedback 23

2 Site Requirements and Specifications 25

Site Requirements 26

Physical Specifications 29

Performance Specifications 30

3 Installing the Module 33

Unpacking the Module 34

Installing the Valve Drive 36

Installing the Valve Heads 42

4 Using the Module 49

Hints for Successful Use 50

Solvent Information 52

Software Configuration 57

5 Troubleshooting and Diagnostics 61

Overview of the Module’s Indicators and Test Functions 62

Module Status Indicator 63

Agilent Lab Advisor Software 64

6 Error Information 65

What Are Error Messages 66

General Error Messages 67

Module Specific Error Messages 72

4 Agilent 1290 Infinity Valve Drive and Valve Heads

Contents

7 Maintenance 75

Introduction to Maintenance 76

Cautions and Warnings 77

Overview of Maintenance 79

Cleaning the Module 80

Replacing Parts of the Valve Head 81

Replacing the Fuses of the Infinity Valve Drive 83

Replacing Valve Heads 86

Replacing the Module Firmware 90

8 Parts and Materials 91

Valve Drive Parts 92

Valve Options Overview 94

Accessory Kit 96

Valve Products 97

Capillary Kits 98

Tubing Kit 106

2 Pos/6 Port Valve Head 600 bar 107

2 Pos/6 Port Ultra High Pressure Valve Head 1200 bar 108

2 Pos/6 Port Valve Head 600 bar (Bio-inert) 109

2 Pos/10 Port Micro Valve Head 600 bar 110

2 Pos/10 Port Ultra High Pressure Valve Head 1200 bar 111

8 Pos/9 Port Valve Head 600 bar 112

8 Pos/9 Port Ultra High Pressure Valve Head 1200 bar 113

Valve Head 4 Column Selector 600 bar (Bio-inert) 114

Valve Head 6 Column Selector 600 bar 115

Valve Head 6 Column Selector 1200 bar 116

12 Pos/13 Port Valve Head 210 bar (Bio-inert) 117

9 Identifying Cables 119

Cable Overview 120

Analog Cables 122

Remote Cables 124

BCD Cables 127

CAN/LAN Cables 129

External Contact Cable 130

Agilent Module to PC 131

Agilent 1290 Infinity Valve Drive and Valve Heads 5

Contents

10 Hardware Information 133

Electrical Connections 134

Interfaces 137

Config Switch Settings of the Infinity Valve Drive 144

11 Appendix 147

General Safety Information 148

The Waste Electrical and Electronic Equipment Directive 151

Radio Interference 152

Sound Emission 153

Agilent Technologies on Internet 154

6 Agilent 1290 Infinity Valve Drive and Valve Heads

Contents

Agilent 1290 Infinity Valve Drive and Valve Heads

Agilent Technologies

Introduction to the Agilent 1290 Infinity

Valve Drive and Valve Heads

Overview of the Valve Drive 8

Overview of the Agilent Quick Change Valve Heads 12

Typical Applications 13

Dual and Multi Column Selection 13

Sample Enrichment and Sample Cleanup 15

Alternating Column Regeneration 18

Solvent Selection 20

Bio-inert Materials 21

Early Maintenance Feedback 23

This chapter gives an introduction to the module, instrument overview and

internal connectors

8 Agilent 1290 Infinity Valve Drive and Valve Heads

1Introduction to the Agilent 1290 Infinity Valve Drive and Valve Heads

Overview of the Valve Drive

The Agilent 1290 Infinity Valve Drive (G1170A) is the latest addition to the

1290 Infinity LC system. This is a valve drive delivered without a specific valve

head. To be used in a HPLC system it is required to add a valve head to this

device. It is compatible with all currently available Agilent Quick Change Valve

heads (see Table 1 on page 12)

It includes the following features:

•Built-in power supply

•Leak handling with a leak pane and a leak sensor underneath the valve

head

•User exchangeable valve heads (Agilent Quick Change valve heads)

•Valve type and pressure detected by RF-ID tag

•Flexible mounting bracket, for left- or right-side mounting on LC stacks or

at the Agilent Column Organizer (G1383A).

Agilent 1290 Infinity Valve Drive and Valve Heads 9

Introduction to the Agilent 1290 Infinity Valve Drive and Valve Heads 1

Overview of the Valve Drive

Figure 1 Mounting Examples for 1290 Infinity Valve Drive

10 Agilent 1290 Infinity Valve Drive and Valve Heads

1Introduction to the Agilent 1290 Infinity Valve Drive and Valve Heads

Overview of the Valve Drive

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