Agilent Technologies 7890B Bedienungsanleitung

Agilent Technologies

Agilent 7890B Gas

Chromatograph

Getting Started

2Getting Started

Notices

No part of this manual may be reproduced in

any form or by any means (including elec-

tronic storage and retrieval or translation

into a foreign language) without prior agree-

ment and written consent from Agilent

Technologies, Inc. as governed by United

States and international copyright laws.

Manual Part Number

G3430-90055

Edition

Second edition, December 2013

First edition, January 2013

Printed in USA and China

Agilent Technologies, Inc.

2850 Centerville Road

Wilmington, DE 19808-1610

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Acknowledgments

Microsoft ® and Windows® are U.S. regis-

tered trademarks of Microsoft Corporation.

Warranty

The material contained in this document is

provided “as is,” and is subject to being

changed, without notice, in future editions.

Further, to the maximum extent permitted

by applicable law, Agilent disclaims all

warranties, either express or implied, with

regard to this manual and any information

contained herein, including but not limited

to the implied warranties of merchantabil-

ity and fitness for a particular purpose.

Agilent shall not be liable for errors or for

incidental or consequential damages in

connection with the furnishing, use, or

performance of this document or of any

information contained herein. Should

Agilent and the user have a separate writ-

ten agreement with warranty terms cover-

ing the material in this document that

conflict with these terms, the warranty

terms in the separate agreement shall

control.

Restricted Rights Legend

If software is for use in the performance of a

U.S. Government prime contract or subcon-

tract, Software is delivered and licensed as

“Commercial computer software” as

defined in DFAR 252.227-7014 (June 1995),

or as a “commercial item” as defined in FAR

2.101(a) or as “Restricted computer soft-

ware” as defined in FAR 52.227-19 (June

1987) or any equivalent agency regulation or

contract clause. Use, duplication or disclo-

sure of Software is subject to Agilent Tech-

nologies’ standard commercial license

terms, and non-DOD Departments and

Agencies of the U.S. Government will

receive no greater than Restricted Rights as

defined in FAR 52.227-19(c)(1-2) (June

1987). U.S. Government users will receive

no greater than Limited Rights as defined in

FAR 52.227-14 (June 1987) or DFAR

252.227-7015 (b)(2) (November 1995), as

applicable in any technical data.

Technology Licenses

The hardware and/or software described in

this document are furnished under a license

and may be used or copied only in accor-

dance with the terms of such license.

Safety Notices

CAUTION

A CAUTION notice denotes a

hazard. It calls attention to an

operating procedure, practice, or

the like that, if not correctly

performed or adhered to, could

result in damage to the product or

loss of important data. Do not

proceed beyond a CAUTION notice

until the indicated conditions are

fully understood and met.

WARNING

A WARNING notice denotes a

hazard. It calls attention to an

operating procedure, practice, or

the like that, if not correctly

performed or adhered to, could

result in personal injury or death.

Do not proceed beyond a

WARNING notice until the

indicated conditions are fully

understood and met.

Getting Started 3

Contents

1 Manuals, Information, Tools and Where to Find Them

GC Manuals, Tools, and Online Help 6

Available manuals 7

Language Versions 9

Online help 10

User Apps 11

Education Opportunities 14

2 Overview of the 7890B GC

The 7890B Gas Chromatograph 16

The inlets 19

The GC column and oven 21

Capillary Flow Technology 22

Detectors 23

The operating panel 24

3NewFeatures

New Features 26

Intelligent instruments 26

Improved Early Maintenance Feedback (EMF) 27

Access to Agilent’s Method Calculators 28

Energy- and Gas-saving features 29

Find parts from your data system 30

FPD+30

Increased detector sensitivity 30

4 Using Hydrogen Carrier Gas

Using Hydrogen Carrier Gas 32

Special considerations 32

Method translation tools 33

4Getting Started

Agilent 7890B Gas Chromatograph

Getting Started

Agilent Technologies

Manuals, Information, Tools and Where

to Find Them

GC Manuals, Tools, and Online Help 6

Language Versions 9

Education Opportunities 14

Manuals, Information, Tools and Where to Find Them

6Getting Started

GC Manuals, Tools, and Online Help

In addition to this manual, Agilent provides several learning products that

explain how to install, operate, maintain and troubleshoot the 7890B GC

system. These manuals can be found on the Agilent GC and GC/MS User

Manuals & Tools DVDs that are included with your GC shipment.

Installing your manuals provides for a much richer user experience by

providing the ability to install the manuals you want, in the language you

want. Install HTML and PDF versions.

Allrights reserved.

Madein USA

Agilent Technologies

GC/GCMS Hardware User Manuals and Videos



Disk 2/3

Toinstall:

1.Insert disk into DVD drive

2.Follow the instructions on the screen.

3.If autoplay is not enabled, double-click

"index_xx.html"on the DVD

where xx is:

en for English

ch for 中文

jpfor 日本語

Version B.01.05

January, 2013

Allrights reserved.

Madein USA

Agilent Technologies

GC/GCMS Hardware User Manuals and Videos



Disk 2/3

Toinstall:

1.Insert disk into DVD drive

2.Follow the instructions on the screen.

3.If autoplay is not enabled, double-click

"index_xx.html"on the DVD

where xx is:

en for English

ch for 中文

jpfor 日本語

Version B.01.05

January, 2013

Select the Instrument Manuals icon

from the GC and GC/MS User Manuals

& Tools DVD and install the suite of

manuals for your system.

Manuals, Information, Tools and Where to Find Them

Getting Started 7

Available manuals

Table 1 7890B GC Learning Products

Learning Product Contents When to use this documentation

Getting Started (this

manual)

Overview of the manuals. Where to find

information. How to install the manuals.

Overview of the GC.

Safety Manual Lists safety and regulatory information.

Precautions for using hydrogen carrier

(or fuel) gas. Precautions for performing

maintenance tasks.

•Before installation, to prepare for a safe

installation process.

•Before maintenance.

GC, GC/MS, and ALS Site

Prep Guide

Requirements for: space and weight for

the lab bench, power, heat dissipation,

exhaust venting, laboratory conditions

(expected local environment), gas and

reagent gas purity, gas supplies, gas

plumbing (including filters, regulator

types, and tubing needs), and cryogenic

cooling supplies (if used).

Recommended supplies to purchase

before installation.

•Before installation, to prepare the laboratory

site.

•Before installation, to find what supplies are

needed for successful installation (such as

gases, installation kits, gas purifiers,

regulators, tubing, fittings, consumable parts,

and so on).

•At any time, to refer to expected requirements

for gas supplies, regulators, cryogenic cooling

supplies, supply pressures, and so on.

Installation and First Startup How to install the GC on the laboratory

bench. Cabling pinouts.

•During installation.

Operation Manual Common keyboard functions. Using the

keyboard to start runs and sequences.

Using the keyboard when connected to

an Agilent data system. Methods and

sequences overview. Startup and

shutdown. How to check GC

performance after installation. Energy

conservation (sleep/wake). Early

Maintenance Feedback. Configuration.

•To learn common operating tasks (making a

run, loading a method, running a series of

samples).

•To learn how to use the GC keyboard when

under data system control.

•Before a short-term or long-term shutdown.

•When starting up the GC after a period of

inactivity.

•Whenever you need to verify performance of

the instrument against factory standards, for

example, after certain maintenance

procedures.

•To learn how to properly configure GC

components, especially when newly installed.

Manuals, Information, Tools and Where to Find Them

8Getting Started

Advanced Operation Manual Procedures and theory of operation not

normally required for daily use:

programming; detailed information about

methods and sequences; inlet (column)

flow and pressure modes; inlet, detector,

valve, oven, and other setpoint details;

and output signal settings.

•When developing methods.

•When running the GC standalone (no data

system).

•To learn details about settings.

Maintaining Your GC Procedures to maintain the GC, including

procedures for all standard inlet and

detector options. Replacement parts

information. Instructions for using Early

Maintenance Feedback (EMF).

•To look up a replacement part or consumable

part.

•Before performing any maintenance on the

GC.

Troubleshooting Procedures for resolving GC issues.

Symptoms and resolutions for resolving

GC or chromatographic or hardware

issues. Procedures to determine whether

an issue is hardware-related,

software-related, or related to other

factors (such as sample preparation).

•When trying to isolate the cause of

unexpected performance issues.

GC Software Familiarization Introduction to the data system control

software user interface for the GC.

Introduces concepts for EMF and

configuration, and other new features.

•To locate settings in the data system user

interface.

Data system help Topics and tasks for creating and editing

methods for the GC.

•To answer questions about using the software

to control the GC.

Table 1 7890B GC Learning Products (continued)

Learning Product Contents When to use this documentation

Manuals, Information, Tools and Where to Find Them

Getting Started 9

Language Versions

Agilent provides the 7890B learning products in several languages.

Table 2 below lists the manuals and the languages available for each

manual format (print, Adobe PDF, or HTML).

Table 2 Languages available for GC manuals

Language

Manual Format

English

Chinese

French

German

Italian

Japanese

Brazilian

Portuguese

Russian

Spanish

Getting Started Print

HTML

PDF

Safety Manual HTML

PDF

Installation and First Startup HTML

PDF

GC, GC/MS, and ALS Site Prep Guide HTML

PDF

Maintaining Your GC HTML

PDF

Troubleshooting HTML

PDF

Operation Manual HTML

PDF

Advanced Operation Manual HTML

PDF

Software Familiarization HTML

9 9

Manuals, Information, Tools and Where to Find Them

10 Getting Started

Online help

In addition to hardware manuals, your GC data system also includes an

extensive online help system with detailed information, common tasks,

and video tutorials on using the software.

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