Agilent Technologies 1290 infinity Bedienungsanleitung

Agilent Technologies

Agilent 1290 Infinity

Flexible Cube

User Manual

1290 Infinity Flexible Cube User Manual

Notices

No part of this manual may be reproduced

in any form or by any means (including elec-

tronic storage and retrieval or translation

into a foreign language) without prior agree-

ment and written consent from Agilent

Technologies, Inc. as governed by United

States and international copyright laws.

Manual Part Number

G4227-90000

Edition

06/2010

Printed in Germany

Agilent Technologies

Hewlett-Packard-Strasse 8

76337 Waldbronn

Warranty

The material contained in this docu-

ment is provided “as is,” and is sub-

ject to being changed, without notice,

in future editions. Further, to the max-

imum extent permitted by applicable

law, Agilent disclaims all warranties,

either express or implied, with regard

to this manual and any information

contained herein, including but not

limited to the implied warranties of

merchantability and fitness for a par-

ticular purpose. Agilent shall not be

liable for errors or for incidental or

consequential damages in connection

with the furnishing, use, or perfor-

mance of this document or of any

information contained herein. Should

Agilent and the user have a separate

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document that conflict with these

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arate agreement shall control.

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closure of Software is subject to Agilent

Technologies’ standard commercial license

terms, and non-DOD Departments and

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receive no greater than Restricted Rights as

defined in FAR 52.227-19(c)(1-2) (June

1987). U.S. Government users will receive

no greater than Limited Rights as defined in

FAR 52.227-14 (June 1987) or DFAR

252.227-7015 (b)(2) (November 1995), as

applicable in any technical data.

Safety Notices

CAUTION

A CAUTION notice denotes a

hazard. It calls attention to an

operating procedure, practice, or

the like that, if not correctly per-

formed or adhered to, could

result in damage to the product

or loss of important data. Do not

proceed beyond a CAUTION

notice until the indicated condi-

tions are fully understood and

met.

WARNING

A WARNING notice denotes a

hazard. It calls attention to an

operating procedure, practice,

or the like that, if not correctly

performed or adhered to, could

result in personal injury or

death. Do not proceed beyond a

WARNING notice until the indi-

cated conditions are fully under-

stood and met.

For Research Use Only

1290 Infinity Flexible Cube User Manual 3

In This Guide...

This manual covers the Agilent 1290 Infinity Flexible Cube (G4227A)

1 Introduction

This chapter gives an introduction to the module, instrument overview and

internal connectors

2 Site Requirements and Specifications

This chapter provides information on environmental requirements, physical

and performance specifications.

3 Installing the Module

This chapter gives information about the preferred stack setup for your system

and the installation of your Flexible Cube.

4 LAN Configuration

This chapter provides information on connecting the module to the Agilent

Data System.

5 Using the Module

This chapter provides information on how to set up the Flexible Cube for an

analysis and explains the basic settings.

6 Optimizing the Autosampler with the Flexible Cube

This chapter provides information on how to optimize the Autosampler and

the Flexible Cube for a minimum carry over and fastest cycle times.

7 Troubleshooting and Diagnostics

This chapter gives an overview about the troubleshooting and diagnostic

features and the different user interfaces.

4 1290 Infinity Flexible Cube User Manual

In This Guide...

8 Error Information

This chapter describes the meaning of error messages, and provides

information on probable causes and suggested actions how to recover from

error conditions.

9 Maintenance and Repair

This chapter describes the maintenance of the module.

10 Parts and Materials for Maintenance

This chapter provides information on parts and material required for the

module.

11 Identifying Cables

This chapter provides information on cables used with the 1290 series of

HPLC modules.

12 Appendix

This chapter provides addition information on safety, legal and web.

1290 Infinity Flexible Cube User Manual 5

Contents

1 Introduction 9

Features 10

Overview of the Module 11

Flexible Cube Principle 12

Early Maintenance Feetback 19

Instrument Layout 20

Electrical Connections 21

Interfaces 23

2 Site Requirements and Specifications 29

Site Requirements 30

Physical Specifications 33

Performance Specifications 34

3 Installing the Module 37

Unpacking the Module 38

Optimizing the Stack Configuration 40

Installing the Module 47

Flow Connections to the Module 49

4 LAN Configuration 51

LAN-Configuration 52

5 Using the Module 53

Setting up the Flexible Cube with Agilent ChemStation 54

6 Optimizing the Autosampler with the Flexible Cube 61

Preparing the Autosampler and Flexible Cube 62

How to Achieve Lowest Carry Over 63

How to Achieve Highest Throughput Using the Flexible Cube 72

6 1290 Infinity Flexible Cube User Manual

Contents

7 Troubleshooting and Diagnostics 73

Overview of the Module’s Indicators and Test Functions 74

Status Indicators 75

User Interfaces 77

Agilent Lab Advisor Software 78

8 Error Information 79

What Are Error Messages 80

General Error Messages 81

Module Spezific Error Messages 88

9 Maintenance and Repair 91

Introduction to Maintenance 92

Warnings and Cautions 93

Overview of Maintenance 95

Cleaning the Module 96

Exchange Flush Pump Inlet Valve 97

Exchange Flush Pump Outlet Valve 100

Exchange Valve Rotor Seal 103

Replacing Module Firmware 107

10 Parts and Materials for Maintenance 109

Capillaries 110

Parts overview 111

Accessory Kits 112

11 Identifying Cables 113

Cable Overview 114

Analog Cables 116

Remote Cables 118

BCD Cables 121

CAN/LAN Cables 123

External Contact Cable 124

Agilent Module to PC 125

1290 Infinity Flexible Cube User Manual 7

Contents

12 Appendix 127

General Safety Information 128

The Waste Electrical and Electronic Equipment (WEEE) Directive

(2002/96/EC) 131

Radio Interference 132

Sound Emission 133

Flow Cell 134

Agilent Technologies on Internet 135

8 1290 Infinity Flexible Cube User Manual

Contents

1290 Infinity Flexible Cube User Manual

Agilent Technologies

Introduction

Features 10

Overview of the Module 11

Flexible Cube Principle 12

Early Maintenance Feetback 19

Instrument Layout 20

Electrical Connections 21

Serial Number Information (ALL) 22

Rear View of the Module 22

Interfaces 23

Overview Interfaces 24

This chapter gives an introduction to the module, instrument overview and

internal connectors

10 1290 Infinity Flexible Cube User Manual

1Introduction

Features

The Agilent 1290 Infinity Flexible Cube introduces an unprecedented

flexibility to the Agilent 1290 Infinity System. It includes options to reduce

Carry Over and will later, with addition of valve pods, be able to convert the

G4226A Autosampler for fixed loop injections or be used as a multipurpose

valve box.

The G4227A Flexible Cube is capable of reducing carry over to a minimum and

maintains that level between the maintenance intervals of the Autosampler.

For specifications, see “Performance Specifications” on page 34.

NOTE This 1290 Infinity Flexible Cube has been introduced as part of the Agilent 1290 Infinity

Liquid Chromatograph.

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