Agilent Technologies 1290 infinity Bedienungsanleitung

Agilent Technologies

Agilent 1290 Infinity

Thermostatted Column

Compartment

User Manual

1290 Infinity TCC User Manual

Notices

2011- 2012, 2013

No part of this manual may be reproduced

in any form or by any means (including elec-

tronic storage and retrieval or translation

into a foreign language) without prior agree-

ment and written consent from Agilent

Technologies, Inc. as governed by United

States and international copyright laws.

Manual Part Number

G1316-90032

Edition

02/2013

Printed in Germany

Agilent Technologies

Hewlett-Packard-Strasse 8

76337 Waldbronn

This product may be used as a com-

ponent of an in vitro diagnostic sys-

tem if the system is registered with

the appropriate authorities and com-

plies with the relevant regulations.

Otherwise, it is intended only for gen-

eral laboratory use.

Warranty

The material contained in this docu-

ment is provided “as is,” and is sub-

ject to being changed, without notice,

in future editions. Further, to the max-

imum extent permitted by applicable

law, Agilent disclaims all warranties,

either express or implied, with regard

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contained herein, including but not

limited to the implied warranties of

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liable for errors or for incidental or

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Safety Notices

CAUTION

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hazard. It calls attention to an

operating procedure, practice, or

the like that, if not correctly per-

formed or adhered to, could

result in damage to the product

or loss of important data. Do not

proceed beyond a CAUTION

notice until the indicated condi-

tions are fully understood and

met.

WARNING

A WARNING notice denotes a

hazard. It calls attention to an

operating procedure, practice,

or the like that, if not correctly

performed or adhered to, could

result in personal injury or

death. Do not proceed beyond a

WARNING notice until the indi-

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stood and met.

1290 Infinity TCC User Manual 3

In This Guide...

This manual covers the Agilent 1290 Infinity Thermostatted Column

Compartment (TCC) (G1316C).

1 Introduction to the Column Compartment

This chapter gives an introduction to the TCC and an instrument overview.

2 Site Requirements and Specifications

This chapter provides information on environmental requirements, physical

and performance specifications.

3 Installing the Module

This chapter provides information on unpacking, checking on completeness,

stack considerations and installation of the module.

4 How to optimize the Column Compartment

This chapter provides information on how to optimize the thermostatted

column compartment.

5 Troubleshooting and Diagnostics

Overview about the troubleshooting and diagnostic features.

6 Error Information

This chapter describes the meaning of error messages, and provides

information on probable causes and suggested actions how to recover from

error conditions.

7 Test Functions and Calibrations

This chapter describes the TCC’s built in test functions.

4 1290 Infinity TCC User Manual

In This Guide...

8 Maintenance

This chapter describes the maintenance tasks for the TCC. If the instrument

needs repair please contact your Agilent service representative.

9 Parts and Materials for Maintenance

This chapter provides information on parts for maintenance.

10 Identifying Cables

This chapter summarizes information on all cables.

11 Hardware Information

This chapter describes the TCC in more detail on hardware and electronics.

12 Appendix

This chapter provides addition information on safety, legal and web.

1290 Infinity TCC User Manual 5

Contents

1 Introduction to the Column Compartment 9

Overview of the Module 10

System Overview 11

Column-Identification System 13

Column Switching Valve (Optional) 15

Bio-inert Materials 21

2 Site Requirements and Specifications 23

Site Requirements 24

Physical Specifications 27

Performance Specifications 28

Valve Specifications 29

Extended Specifications on G1316C 34

Solvent Information 35

3 Installing the Module 39

Unpacking the module 40

Optimizing the Stack Configuration 41

Installing the Column Compartment 46

Installing Valve Heads 50

Installation of Heater Devices 56

Flow Connections of the Column Compartment 60

Installing Capillaries 67

Placing Columns 70

4 How to optimize the Column Compartment 73

Optimizing the Column Compartment 74

Using Additional Heater Devices 75

Delay Volume and Extra-Column Volume 76

How to Configure the Optimum Delay Volume 78

How to Achieve Higher Injection Volumes 79

How to Achieve High Throughput 80

6 1290 Infinity TCC User Manual

Contents

5 Troubleshooting and Diagnostics 81

Overview of the Module’s Indicators and Test Functions 82

Status indicators 83

Available Tests vs User Interfaces 85

Agilent Lab Advisor Software 86

6 Error Information 87

What Are Error Messages 88

General Error Messages 89

TCC Error Messages 93

7 Test Functions and Calibrations 103

Thermostat Function Test 104

Pressure Test 106

Temperature Calibration 107

8 Maintenance 111

Introduction to Maintenance and Repair 112

Cautions and Warnings 113

Overview of Maintenance 115

Cleaning the Column Compartment 116

Changing Column Identification Tags 117

Adding Heater Devices 119

Installing the capillaries 124

Correcting Leaks 131

Replacing Head Parts of Column Switching Valve 133

Replacing Valve Heads 136

Preparing the Column Compartment for Transportation 140

Replacing the Module Firmware 143

9 Parts and Materials for Maintenance 145

Plastic Parts 146

Leak Parts 147

Heater and Cooling Devices 148

Valve Options Overview 152

Accessory Kits 155

1290 Infinity TCC User Manual 7

Contents

10 Identifying Cables 163

Cable Overview 164

Analog cables 166

Remote Cables 168

BCD Cables 171

CAN Cable 173

RS-232 Cable Kit 174

Agilent Module to Printer 175

11 Hardware Information 177

Firmware Description 178

Electrical Connections 181

Interfaces 184

Setting the 8-bit Configuration Switch (without On-board) LAN 190

Early Maintenance Feedback 194

Instrument Layout 195

12 Appendix 197

General Safety Information 198

The Waste Electrical and Electronic Equipment (WEEE) Directive

(2002-96-EC) 201

Lithium Batteries Information 202

Radio Interference 203

Sound Emission 204

Agilent Technologies on Internet 205

8 1290 Infinity TCC User Manual

Contents

1290 Infinity TCC User Manual

Agilent Technologies

Introduction to the Column

Compartment

Overview of the Module 10

System Overview 11

Column-Identification System 13

Column Switching Valve (Optional) 15

Typical Applications 18

Bio-inert Materials 21

This chapter gives an introduction to the TCC and an instrument overview.

10 1290 Infinity TCC User Manual

1Introduction to the Column Compartment

Overview of the Module

The Agilent 1290 Infinity Thermostatted Column Compartment is a stackable

temperature-controlled column compartment for LC. It is available as

standalone module or as a component of an Agilent 1290 Infinity system. It is

used for heating and cooling to meet extreme requirements of retention time

reproducibility.

The main features of the 1290 Infinity Thermostatted Column Compartment

are:

•Peltier heating and cooling from 10 degrees below ambient up to 100 °C

with high heating and cooling speeds for maximum application flexibility

and stability,

•holds up to three 30 cm columns,

•optimized design gives minimum dead volumes and maximum efficiency,

•two independently programmable heat exchangers contribute volumes of

only 3 and 6 μl,

•additional heating devices for low flow rates, which reduce the risk of

additional dispersion,

•it can be supplemented by a kit to install a small heat exchanger with 1.6 μl

delay volume to reduce the delay volume.

•electronic column-identification as standard for GLP documentation of

column type, and major column parameters,

•optional high-quality Quick-Change Valve Heads.

For specifications, see “Performance Specifications” on page 28.

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