Agilent Technologies 1290 infinity Bedienungsanleitung

Agilent Technologies

Agilent 1290 Infinity

Binary Pump

User Manual

Agilent 1290 Infinity Binary Pump User Manual

Notices

No part of this manual may be reproduced

in any form or by any means (including

electronic storage and retrieval or transla-

tion into a foreign language) without prior

agreement and written consent from Agi-

lent Technologies, Inc. as governed by

United States and international copyright

laws.

Manual Part Number

G4220-90007 Rev. B

Edition

10/2018

Printed in Germany

Agilent Technologies

Hewlett-Packard-Strasse 8

76337 Waldbronn

Warranty

The material contained in this docu-

ment is provided “as is,” and is sub-

ject to being changed, without notice,

in future editions. Further, to the max-

imum extent permitted by applicable

law, Agilent disclaims all warranties,

either express or implied, with regard

to this manual and any information

contained herein, including but not

limited to the implied warranties of

merchantability and fitness for a par-

ticular purpose. Agilent shall not be

liable for errors or for incidental or

consequential damages in connection

with the furnishing, use, or perfor-

mance of this document or of any

information contained herein. Should

Agilent and the user have a separate

written agreement with warranty

terms covering the material in this

document that conflict with these

terms, the warranty terms in the sep-

arate agreement shall control.

Technology Licenses

The hardware and/or software described in

this document are furnished under a

license and may be used or copied only in

accordance with the terms of such license.

Restricted Rights Legend

If software is for use in the performance of

a U.S. Government prime contract or sub-

contract, Software is delivered and licensed

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or as a “commercial item” as defined in

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software” as defined in FAR 52.227-19

(June 1987) or any equivalent agency regu-

lation or contract clause. Use, duplication

or disclosure of Software is subject to Agi-

lent Technologies’ standard commercial

license terms, and non-DOD Departments

and Agencies of the U.S. Government will

receive no greater than Restricted Rights as

defined in FAR 52.227-19(c)(1-2) (June

1987). U.S. Government users will receive

no greater than Limited Rights as defined in

FAR 52.227-14 (June 1987) or DFAR

252.227-7015 (b)(2) (November 1995), as

applicable in any technical data.

Safety Notices

CAUTION

A CAUTION notice denotes a

hazard. It calls attention to an

operating procedure, practice, or

the like that, if not correctly per-

formed or adhered to, could

result in damage to the product

or loss of important data. Do not

proceed beyond a CAUTION

notice until the indicated condi-

tions are fully understood and

met.

WARNING

A WARNING notice denotes a

hazard. It calls attention to an

operating procedure, practice,

or the like that, if not correctly

performed or adhered to, could

result in personal injury or

death. Do not proceed beyond a

WARNING notice until the indi-

cated conditions are fully

understood and met.

Agilent 1290 Infinity Binary Pump User Manual 3

In This Guide…

This manual covers the Agilent 1290 Infinity Binary Pump (G4220A).

1Introduction

This chapter gives an introduction to the pump, instrument overview and

internal connectors.

2 Site Requirements and Specifications

This chapter provides information on environmental requirements, physical

and performance specifications.

3 Installing the Module

This chapter gives information about the preferred stack setup for your

system and the installation of your Agilent 1290 Infinity Binary Pump.

4UsingthePump

This chapter explains the operational parameters of the Agilent 1290 Infinity

Binary Pump.

5 Optimizing Performance

This chapter gives hints on how to optimize the performance or use additional

devices.

6 Troubleshooting and Diagnostics

Overview about the troubleshooting and diagnostic features.

7 Error Information

This chapter describes the meaning of error messages, and provides

information on probable causes and suggested actions how to recover from

error conditions.

4 Agilent 1290 Infinity Binary Pump User Manual

In This Guide…

8 Test Functions and Calibrations

This chapter describes the tests for the module.

9 Maintenance

This chapter describes the maintenance of the Agilent 1290 Infinity Binary

Pump.

10 Parts and Materials for Maintenance

This chapter provides information on parts for maintenance.

11 Identifying Cables

This chapter provides information on cables used with the Agilent 1200

Infinity Series modules.

12 Hardware Information

This chapter describes the pump in more detail on hardware and electronics.

13 LAN Configuration

This chapter provides information on connecting the detector to the Agilent

ChemStation PC.

14 Appendix

This chapter provides addition information on safety, legal and web.

Agilent 1290 Infinity Binary Pump User Manual 5

Contents

1Introduction 9

Features 10

Overview of the Binary Pump 11

Pump Principle 12

System Overview 15

2 Site Requirements and Specifications 17

Site Requirements 18

Physical Specifications 21

Specifications 22

3 Installing the Module 25

Unpacking the Module 26

Optimizing the Stack Configuration 27

Installation Information on Leak and Waste Handling 32

Removing the Transport Foam 36

Installing the Pump 37

Flow Connections to the Pump 41

Installation of Seal Wash Function 45

4UsingthePump 47

Magnets 48

Turn on/off 49

Status Indicators 51

Leak and Waste Handling 52

Best Practices 53

Preparing the Binary Pump 58

Algae Growth in HPLC Systems 59

Setting up the Pump with the Instrument Control Interface 60

Purging the Pump 69

Solvent Information 71

Solvent Recommendation for Agilent 1290 Infinity and 1290 Infinity II and 1260

Infinity II Flexible Pumps 78

6 Agilent 1290 Infinity Binary Pump User Manual

Contents

5 Optimizing Performance 83

Delay Volume and Extra-Column Volume 84

How to Configure the Optimum Delay Volume 85

How to Achieve Higher Resolution 87

Using Solvent Calibration Tables 90

6 Troubleshooting and Diagnostics 91

Available Tests vs User Interfaces 92

Agilent Lab Advisor Software 93

7 Error Information 95

What Are Error Messages 97

General Error Messages 98

Pump Error Messages 107

8 Test Functions and Calibrations 123

Introduction 124

Pump Leak Rate Test 125

System Pressure Test 130

9 Maintenance 133

Introduction to Maintenance 135

Warnings and Cautions 137

Overview of Maintenance 138

Cleaning the Module 139

Installing Fittings and Capillaries 140

Replacing the Shutoff Valve Panel 141

Replacing the Pressure Sensor 143

Replacing the Inlet valve 146

Replacing the Outlet Valve 148

Replacing the Solvent Selection Valve (SSV) 151

Changing configuration or replacing the Jet Weaver 153

Replacing the Seal Wash Pump 156

Releasing a Stuck Inlet Valve 157

Remove the Pump Head Assembly 160

Pump Head Maintenance (Tool Free) 163

Agilent 1290 Infinity Binary Pump User Manual 7

Contents

Install the Pump Head Assembly 178

Replacing the Purge Valve Head 180

Replacing Parts of the High Pressure Filter Assembly 183

Installing the Valve Rail Kit 185

Replacing the Main Power Fuses 186

Replacing Module Firmware 188

Preparing the Pump Module for Transport 189

10 Parts and Materials for Maintenance 195

Overview of Maintenance Parts 196

Flow Connections 198

Solvent Cabinet Kit 200

Seal Wash Option 201

Pump Heads 202

Purge Valve 206

Cover Parts 208

Leak Parts 210

Fuses 211

Accessory Kit 212

Tools 213

HPLC System Tool Kit 215

11 Identifying Cables 217

Cable Overview 218

Analog cables 220

Remote Cables 222

BCD Cables 225

CAN/LAN Cable 227

RS-232 Cable Kit 228

Agilent 1200 Module to Printer 229

8 Agilent 1290 Infinity Binary Pump User Manual

Contents

12 Hardware Information 231

Firmware Description 232

Electrical Connections 235

Interfaces 237

Setting the 8-bit Configuration Switch 244

Instrument Layout 248

Early Maintenance Feedback 249

13 LAN Configuration 251

What You Have to Do First 252

TCP/IP parameter configuration 253

Configuration Switch 254

Initialization mode selection 255

Dynamic Host Configuration Protocol (DHCP) 257

Link configuration selection 260

Manual Configuration 261

PC and User Interface Software Setup Setup 267

14 Appendix 269

General Safety Information 270

The Waste Electrical and Electronic Equipment (WEEE) Directive

(2002-96-EC) 273

Radio Interference 274

Sound Emission 275

Agilent Technologies on Internet 276

Agilent 1290 Infinity Binary Pump User Manual

Agilent Technologies

Introduction

Features 10

Overview of the Binary Pump 11

Pump Principle 12

System Overview 15

Leak and Waste Handling 15

This chapter gives an introduction to the pump, instrument overview and

internal connectors.

10 Agilent 1290 Infinity Binary Pump User Manual

Introduction

Features

The Binary pump is designed for highest performance, GLP compliance and

easy maintenance. It includes the following features:

•Seal wash for continued high lifetime of pump seals for buffer applications.

•Solvent selection valve for method flexibility.

•Jet Weaver for optimum mixing performance with a minimum of delay

volume.

•Automatic purge function for ease of use and unattended preparation of the

system.

•Auto tuning of the delivery cycle for compensation of elasticity and solvent

volume change effects (compressibility, thermal expansion, mixing

contraction).

•Solvent selection for optimum flow and composition accuracy.

•Fast defill function for improved intake and delivery performance.

•Two pistons in series design for increased reliability.

•High resolution piston movement control for smooth and reliable motion.

For specifications, see Table 2 on page 22.

NOTE

This Binary pump has been introduced together with the Agilent 1290 Infinity Liquid

Chromatograph.

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