Agilent Technologies InfinityLab LC Series Bedienungsanleitung

1290 Infinity II High-Speed Pumps

Agilent InfinityLab LC Series

User Manual

1290 Infinity II High-Speed Pumps User Manual

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1290 Infinity II High-Speed Pumps User Manual 3

In This Guide…

This manual covers:

•Agilent 1290 Infinity II High-Speed Pump (G7120A)

•Agilent 1290 Infinity II Bio High-Speed Pump (G7132A)

1Introduction

This chapter gives an introduction to the pump and an instrument overview.

2 Site Requirements and Specifications

This chapter provides information on environmental requirements, physical and

performance specifications.

3UsingthePump

This chapter explains the operational parameters of the Agilent 1290 Infinity II

High-Speed Pumps.

4PreparingthePump

This chapter provides information on how to set up the module for an analysis and

explains the basic settings.

5 Optimizing Performance

This chapter gives hints on how to optimize performance or use additional devices.

6Troubleshootingand Diagnostics

Overview about the troubleshooting and diagnostic features.

7 Error Information

This chapter describes the meaning of error messages, and provides information

on probable causes and suggested actions how to recover from error conditions.

1290 Infinity II High-Speed Pumps User Manual 4

8 Maintenance

This chapter describes the maintenance of the Agilent 1290 Infinity II High-Speed

Pumps.

9 Parts and Materials for Maintenance

This chapter provides information on parts for maintenance.

10 Identifying Cables

This chapter provides information on cables used with the modules.

11 Hardware Information

This chapter describes the pump in more detail on hardware and electronics.

12 LAN Configuration

This chapter provides information on connecting the module to the Agilent

ChemStation PC.

13 Appendix

This chapter provides addition information on safety, legal and web.

1290 Infinity II High-Speed Pumps User Manual 5

Contents

1Introduction9

Agilent 1290 Infinity II High-Speed Pump 10

Agilent 1290 Infinity II Bio High-Speed Pump 12

Pump Principle 14

Leak and Waste Handling 16

2 Site Requirements and Specifications 21

Site Requirements 22

Physical Specifications 25

Performance Specifications 27

3UsingthePump33

Magnets 34

Turn on/off 35

Status Indicators 37

Best Practices 38

Purging the Pump 45

Recommendations for Bio-Compatible and Bio-Inert Systems 47

Recommendations for Degassers 49

Solvent Information 50

Solvent Recommendation for Agilent 1290 Infinity and 1290 Infinity II and

1260 Infinity II Flexible Pumps 58

Algae Growth in HPLC Systems 64

Setting up the Pump with the Instrument Control Interface 65

Agilent Local Control Modules 75

4 Preparing the Pump 76

Capillary Coding Guide 77

Installing Capillaries 80

1290 Infinity II High-Speed Pumps User Manual 6

5 Optimizing Performance 85

Delay Volume and Extra-Column Volume 86

How to Configure the Optimum Delay Volume 87

How to Achieve Higher Resolution 88

Using Solvent Calibration Tables 91

6 Troubleshooting and Diagnostics 96

User Interfaces 97

Agilent Lab Advisor Software 98

Pump Leak Rate Test 99

System Pressure Test 104

7 Error Information 106

What Are Error Messages 108

General Error Messages 109

Pump Error Messages 117

8 Maintenance 133

Introduction to Maintenance 135

Warnings and Cautions 138

Overview of Maintenance 140

Cleaning the Module 141

Install Fittings and Capillaries 142

Remove and Install Doors 143

Replace the Shutoff Valve Panel 145

Replace the Pressure Sensor 146

Replace the Solvent Selection Valve (SSV) 148

Change Configuration or Replace the Jet Weaver 150

Replace the Seal Wash Pump 153

Replace the Inlet Valve (G7120A) 154

Replace the Inlet Valve (G7132A) 156

Release a Stuck Inlet Valve 158

Remove the Pump Head Assembly (G7120A) 160

Remove the Pump Head Assembly (G7132A) 163

1290 Infinity II High-Speed Pumps User Manual 7

Pump Head Maintenance (Tool Free) 166

Install the Pump Head Assembly (G7120A) 191

Install the Pump Head Assembly (G7132A) 193

Replace the Outlet Valve (G7120A) 195

Replace the Outlet Valve (G7132A) 198

Replace the Purge Valve Head 200

Replace Parts of the Purge Valve Head 202

Replace Parts of the High Pressure Filter Assembly (G7120A) 203

Replace Parts of the High Pressure Filter Assembly (G7132A) 205

Replace the Module Firmware 207

Prepare the Pump Module for Transport 208

9 Parts and Materials for Maintenance 212

Overview of Maintenance Parts (G7120A) 213

Overview of Maintenance Parts (G7132A) 214

Flow Connections (G7120A) 216

Flow Connections (G7132A) 218

Pump Heads (G7120A) 220

Pump Heads (G7132A) 225

Purge Valve (G7120A) 229

Purge Valve (G7132A) 230

Cover Parts 231

Accessory Kit (G7120A) 232

Accessory Kit (G7132A) 233

HPLC System Tool Kit 234

10 Identifying Cables 235

Cable Overview 236

Analog Cables 238

Remote Cables 240

CAN/LAN Cables 244

Agilent Module to PC 245

USB 246

1290 Infinity II High-Speed Pumps User Manual 8

11 Hardware Information 247

Firmware Description 248

Electrical Connections 251

Interfaces 253

Setting the 8-bit Configuration Switch 258

Early Maintenance Feedback 261

Instrument Layout 262

12 LAN Configuration 263

What You Have to Do First 264

TCP/IP parameter configuration 265

Configuration Switch 266

Initialization mode selection 267

Dynamic Host Configuration Protocol (DHCP) 269

Link configuration selection 272

Manual Configuration 273

PC and User Interface Software Setup Setup 278

13 Appendix 280

General Safety Information 281

Waste Electrical and Electronic Equipment (WEEE) Directive 287

Radio Interference 288

Sound Emission Certification for Federal Republic of Germany 289

Agilent Technologies on Internet 290

1290 Infinity II High-Speed Pumps User Manual 9

1Introduction

Agilent 1290 Infinity II High-Speed Pump 10

Product Description 10

Features 11

Agilent 1290 Infinity II Bio High-Speed Pump 12

Product Description 12

Features 13

Pump Principle 14

Leak and Waste Handling 16

Leak Sensor 19

Waste Concept 20

This chapter gives an introduction to the pump and an instrument overview.

1290 Infinity II High-Speed Pumps User Manual 10

1Introduction

Agilent 1290 Infinity II High-Speed Pump

Product Description

The Agilent 1290 Infinity II High-Speed Pump can enhance your efficiency

through high speed and chromatographic performance.

A low-delay-volume mixer allows you to run fast gradients for narrow-bore

applications for high laboratory efficiency.

The new 1290 Infinity II LC power range has a high instrument efficiency,

allowing you to run any HPLC and UHPLC method.

The full ISET range enables you to transfer existing methods from different

instruments, including current Agilent systems as well as instruments from other

manufacturers.

Active damping, automatic purge valve, new ultralow dispersion kits or low

delay-volume capability, combine to achieve high instrument and analytical

efficiency.

Figure 1 Overview of the High-Speed Pump

Status indicator

Leak drain

Power switch

Pressure sensor

Pump head B

Pump head A

Seal wash pump

Jet weaver

SSV

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