Metrohm 889 Bedienungsanleitung

889 IC Sample Center

Manual

8.889.8001EN

Metrohm AG

CH-9101 Herisau

Switzerland

Phone +41 71 353 85 85

Fax +41 71 353 89 01

[email protected]

www.metrohm.com

889 IC Sample Center

Manual

8.889.8001EN 02/2010 dm

Teachware

Metrohm AG

CH-9101 Herisau

[email protected]

Although all the information given in this documentation has been checked

with great care, errors cannot be entirely excluded. Should you notice any

mistakes please send us your comments using the address given above.

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ Table of contents

889 IC Sample Center ￭￭￭￭￭￭￭￭ III

Table of contents

1Introduction 1

1.1 Instrument description ......................................................... 1

1.1.1 Model versions ........................................................................ 1

1.1.2 Instrument components .......................................................... 2

1.1.3 Intended use ........................................................................... 2

1.2 About the documentation ................................................... 2

1.2.1 Symbols and conventions ........................................................ 2

1.3 Safety instructions ................................................................ 3

1.3.1 General notes on safety ........................................................... 3

1.3.2 Electrical safety ........................................................................ 3

1.3.3 Tubing and capillary connections ............................................. 5

1.3.4 Personnel safety ...................................................................... 5

1.3.5 Flammable solvents and chemicals ........................................... 6

1.3.6 Recycling and disposal ............................................................. 6

2Overview of the instrument 7

2.1 Front and rear ....................................................................... 7

2.2 Opening the device ............................................................... 8

2.3 Interior view ........................................................................ 10

2.4 Interior ................................................................................. 11

2.5 Cooling option .................................................................... 12

3Installation 13

3.1 Setting up the instrument .................................................. 13

3.1.1 Packaging .............................................................................. 13

3.1.2 Checks .................................................................................. 13

3.1.3 Location ................................................................................ 13

3.1.4 Removing the device from the packaging .............................. 13

3.2 Connecting a computer ...................................................... 14

3.3 Connecting pump and column .......................................... 15

3.4 Tubing ................................................................................. 16

3.4.1 Tubing guide ......................................................................... 16

3.5 Outlet tubings ..................................................................... 17

3.6 Rinsing the syringe ............................................................. 18

4Functioning 19

4.1 Injection modes .................................................................. 19

4.2 Syringe and buffer loop ..................................................... 20

Table of contents ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭

IV ￭￭￭￭￭￭￭￭ 889 IC Sample Center

4.3 Full loop injection ............................................................... 21

4.4 Partial loopfill injection ...................................................... 24

4.5 Pickup injection .................................................................. 27

5Handling and maintenance 31

5.1 General ................................................................................ 31

5.2 Care ...................................................................................... 31

5.2.1 Cleaning in general ................................................................ 31

5.3 Maintenance and service ................................................... 32

5.3.1 Sample loop .......................................................................... 32

5.3.2 Replacing the sample needle ................................................. 33

5.3.3 Replacing the air needle ........................................................ 35

5.3.4 Replacing the fuses ................................................................ 36

5.4 Quality Management and validation with Metrohm ....... 37

6Troubleshooting 38

6.1 Error list ............................................................................... 38

6.1.1 Rack unit ............................................................................... 38

6.1.2 Needle unit ............................................................................ 39

6.1.3 Syringe unit ........................................................................... 41

6.1.4 Injection valve unit ................................................................. 42

6.1.5 Cooling unit .......................................................................... 42

6.1.6 Electronics ............................................................................. 43

6.2 Analytical problems ............................................................ 43

6.2.1 Autosampler .......................................................................... 43

7Appendix 46

7.1 Samples and sample vials .................................................. 46

7.2 I/O interface ........................................................................ 46

7.2.1 Properties of the I/O interface ................................................ 47

7.2.2 Pin assignment of the remote interface .................................. 47

8Technical specifications 48

8.1 General ................................................................................ 48

8.2 Sampling .............................................................................. 48

8.3 Analytical characteristics ................................................... 49

8.4 Programming ...................................................................... 49

8.5 Interfaces ............................................................................. 49

8.6 Options (pre-installed) ........................................................ 49

8.7 Mains connection ............................................................... 50

8.8 Safety specifications ........................................................... 50

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ Table of contents

889 IC Sample Center ￭￭￭￭￭￭￭￭ V

8.9 Electromagnetic compatibility (EMC) ................................ 50

8.10 Ambient temperature ......................................................... 51

8.11 Dimensions .......................................................................... 51

9Conformity and warranty 52

9.1 Declaration of Conformity ................................................. 52

9.2 Warranty (guarantee) ......................................................... 53

9.3 Quality Management Principles ........................................ 54

10 Accessories 56

10.1 Scope of delivery 2.889.0010 ............................................ 56

10.2 Scope of delivery 2.889.0020 ............................................ 58

10.3 Optional accessories 2.889.0010 ...................................... 59

10.4 Optional accessories 2.889.0020 ...................................... 60

Index 61

Table of figures ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭

VI ￭￭￭￭￭￭￭￭ 889 IC Sample Center

Table of figures

Figure 1 889 IC Sample Center - front ............................................................. 7

Figure 2 889 IC Sample Center - rear .............................................................. 8

Figure 3 Interior view without covering ......................................................... 10

Figure 4 Interior with sampling device ........................................................... 11

Figure 5 Interior with installed cooling option. .............................................. 12

Figure 6 Unpacking the 889 IC Sample Center .............................................. 13

Figure 7 Connecting pump and column ........................................................ 15

Figure 8 Guiding the rinsing tubing ............................................................... 16

Figure 9 Tubing guide from above ................................................................ 17

Figure 10 Mounting the outlet tubing ............................................................. 17

Figure 11 Mounting the leakage tubing .......................................................... 17

Figure 12 PASA™ injection concept ............................................................... 19

Figure 13 Full loop injection ............................................................................ 21

Figure 14 Replacing the sample needle ........................................................... 33

Figure 15 Pin assignment of I/O socket and plug ............................................. 47

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 1 Introduction

889 IC Sample Center ￭￭￭￭￭￭￭￭ 1

1 Introduction

1.1 Instrument description

The 889 IC Sample Center is a robust Autosampler for high sample through-

put, optimized for the challenges of the modern analytic laboratory. Its

greatest advantages are speed and small sample volumes.

Special features:

￭Control of syringes with high resolution. This enables very high precision

during injections.

￭The control per PC software makes operation readily comprehensible. A

context-sensitive online Help function is available for every window and

every dialog.

￭As a means of enhancing safety, no needle movements are carried out

when the door is open.

￭The optional sample cooling guarantees consistent results.

Standard micro titer plates (high or low form) or sample racks can be used.

The same plates or racks must be present in the left-hand and right-hand

loading drawer.

1.1.1 Model versions

2.889.0010 889 IC Sample Center

With:

￭15 µL injection needle

￭500 µL syringe

￭1000 µL buffer loop

￭100 µL sample loop

2.889.0020 889 IC Sample Center Cool

With:

￭15 µL injection needle

￭500 µL syringe

￭1000 µL buffer loop

￭100 µL sample loop

￭Accessories for cooling the samples

1.2 About the documentation ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭

2￭￭￭￭￭￭￭￭ 889 IC Sample Center

1.1.2 Instrument components

The 889 IC Sample Center has the following components:

￭2 sample racks

Each for 48 vials.

￭Needle arm

With air needle and drives for horizontal and vertical positioning.

￭Injection valve

With six connectors and two switching positions (LOAD and INJECT)

￭Syringe module

For aspirating and transferring the samples.

￭Cooling module (optional)

For cooling the samples.

￭USB connector

For the connection to a PC.

￭I/O interface

For output of an inject marker signal.

1.1.3 Intended use

The 889 IC Sample Center is designed for usage as an automation system

in analytical laboratories.

This instrument is suitable for processing chemicals and flammable samples.

The usage of the 889 IC Sample Center therefore requires that the user has

basic knowledge and experience in the handling of toxic and caustic sub-

stances. Knowledge with respect to the application of the fire prevention

measures prescribed for laboratories is also mandatory.

1.2 About the documentation

Caution

Please read through this documentation carefully before putting the

instrument into operation. The documentation contains information and

warnings which the user must follow in order to ensure safe operation of

the instrument.

1.2.1 Symbols and conventions

The following symbols and styles are used in this documentation:

Cross-reference to figure legend

The first number refers to the figure number, the sec-

ond to the instrument part in the figure.

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