Agilent Technologies 1260 Infinity Bedienungsanleitung

Agilent Technologies

Agilent 1260 Infinity Micro

Degasser

Service Manual

1260 Infinity Micro Degasser Service Manual

Notices

2010, 2013

No part of this manual may be reproduced

in any form or by any means (including elec-

tronic storage and retrieval or translation

into a foreign language) without prior agree-

ment and written consent from Agilent

Technologies, Inc. as governed by United

States and international copyright laws.

Manual Part Number

G1379-90111 Rev. B

Edition

10/2013

Printed in Germany

Agilent Technologies

Hewlett-Packard-Strasse 8

76337 Waldbronn

This product may be used as a com-

ponent of an in vitro diagnostic sys-

tem if the system is registered with

the appropriate authorities and com-

plies with the relevant regulations.

Otherwise, it is intended only for gen-

eral laboratory use.

Warranty

The material contained in this docu-

ment is provided “as is,” and is sub-

ject to being changed, without notice,

in future editions. Further, to the max-

imum extent permitted by applicable

law, Agilent disclaims all warranties,

either express or implied, with regard

to this manual and any information

contained herein, including but not

limited to the implied warranties of

merchantability and fitness for a par-

ticular purpose. Agilent shall not be

liable for errors or for incidental or

consequential damages in connection

with the furnishing, use, or perfor-

mance of this document or of any

information contained herein. Should

Agilent and the user have a separate

written agreement with warranty

terms covering the material in this

document that conflict with these

terms, the warranty terms in the sep-

arate agreement shall control.

Technology Licenses

The hardware and/or software described in

this document are furnished under a license

and may be used or copied only in accor-

dance with the terms of such license.

Restricted Rights Legend

If software is for use in the performance of a

U.S. Government prime contract or subcon-

tract, Software is delivered and licensed as

“Commercial computer software” as

defined in DFAR 252.227-7014 (June 1995),

or as a “commercial item” as defined in FAR

2.101(a) or as “Restricted computer soft-

ware” as defined in FAR 52.227-19 (June

1987) or any equivalent agency regulation

or contract clause. Use, duplication or dis-

closure of Software is subject to Agilent

Technologies’ standard commercial license

terms, and non-DOD Departments and

Agencies of the U.S. Government will

receive no greater than Restricted Rights as

defined in FAR 52.227-19(c)(1-2) (June

1987). U.S. Government users will receive

no greater than Limited Rights as defined in

FAR 52.227-14 (June 1987) or DFAR

252.227-7015 (b)(2) (November 1995), as

applicable in any technical data.

Safety Notices

CAUTION

A CAUTION notice denotes a

hazard. It calls attention to an

operating procedure, practice, or

the like that, if not correctly per-

formed or adhered to, could

result in damage to the product

or loss of important data. Do not

proceed beyond a CAUTION

notice until the indicated condi-

tions are fully understood and

met.

WARNING

A WARNING notice denotes a

hazard. It calls attention to an

operating procedure, practice,

or the like that, if not correctly

performed or adhered to, could

result in personal injury or

death. Do not proceed beyond a

WARNING notice until the indi-

cated conditions are fully under-

stood and met.

1260 Infinity Micro Degasser Service Manual 3

Contents

1 Introduction 5

Introduction to the Micro Vacuum Degasser 6

2 Site Requirements and Specifications 7

Site Requirements 8

Physical Specifications 11

Performance Specifications 12

3 Installing the Micro Vacuum Degasser 13

Unpacking the Micro Vacuum Degasser 14

Optimizing the Stack Configuration 16

Installing the Micro Vacuum Degasser 19

Flow Connections to the Micro Vacuum Degasser 21

Operational Hints for the Micro Vacuum Degasser 24

Transporting the Micro Vacuum Degasser 27

4 Using the Micro Vacuum Degasser 29

When to Use a Micro Vacuum Degasser? 30

Prevent Blocking of Solvent Filters 32

Solvent Information 34

5 Optimizing Performance 41

Increasing the Degasser Performance and Degassing Level 42

6 Troubleshooting and Diagnostics 43

Overview of the Degasser's Indicators 44

Status Indicators 45

Hardware Symptoms 47

7 Maintenance 51

Introduction to Maintenance and Repair 52

4 1260 Infinity Micro Degasser Service Manual

Contents

8Repairs 63

Exchanging Internal Parts 64

Overview of Repair Procedures 65

Overview of Internal Parts 66

9 Parts and Materials for Maintenance 79

Cover Parts 80

Sheet Metal Kit 81

Power and Status Light Pipes 82

Accessory Kit 83

10 Parts for Repair 85

Micro Vacuum Degasser Parts 86

11 Cable overview 89

Overview 90

Remote Cable 92

12 Hardware Information 95

Operating Principle 96

13 Appendix 97

General Safety Information 98

The Waste Electrical and Electronic Equipment "WEEE) Directive

(2002/96/EC) 101

Radio Interference 102

Sound Emission 103

Agilent Technologies on Internet 104

1260 Infinity Micro Degasser Service Manual

Agilent Technologies

Introduction

Introduction to the Micro Vacuum Degasser 6

6 1260 Infinity Micro Degasser Service Manual

1Introduction

Introduction to the Micro Vacuum Degasser

The Agilent 1260 Infinity micro vacuum degasser, model G1379B,

comprises a 4- channel vacuum container, including 4 micro structured

membranes, and a vacuum pump. When the micro vacuum degasser is

switched on, the control circuit turns on the vacuum pump, which is

operated with constant speed and voltage generates a partial vacuum in

the vacuum container. The pressure is measured by a pressure sensor. The

micro vacuum degasser maintains the partial vacuum with the help of a

controlled leak in the degasser’s proportional valve and by varying size of

the controlled leak within the proportional valve, depending on the signal

from the pressure sensor.

The LC pump draws the solvents from their bottles through the special

plastic membranes of the vacuum container. As the solvents pass through

the vacuum chambers any dissolved gas in the solvents permeates through

the membranes into the vacuum container. The solvents will be almost

completely degassed when leaving the outlets of the micro vacuum

degasser.

Figure 1 Overview (only one of the four solvent channels is shown)

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1260 Infinity Micro Degasser Service Manual

Agilent Technologies

Site Requirements and Specifications

Site Requirements 8

Physical Specifications 11

Performance Specifications 12

8 1260 Infinity Micro Degasser Service Manual

2Site Requirements and Specifications

Site Requirements

A suitable environment is important to ensure optimal performance of the

instrument.

Power Considerations

The module power supply has wide ranging capability. It accepts any line

voltage in the range described in Table 1 on page 11. Consequently there

is no voltage selector in the rear of the module. There are also no

externally accessible fuses, because automatic electronic fuses are

implemented in the power supply.

WARNING

Hazard of electrical shock or damage of your instrumentation

can result, if the devices are connected to a line voltage higher than specified.

➔Connect your instrument to the specified line voltage only.

WARNING

The module is partially energized when switched off, as long as the power cord is

plugged in.

Repair work at the module can lead to personal injuries, e.g. electrical shock, when

the cover is opened and the module is connected to power.

➔Always unplug the power cable before opening the cover.

➔Do not connect the power cable to the instrument while the covers are removed.

1260 Infinity Micro Degasser Service Manual 9

Site Requirements and Specifications 2

Site Requirements

Power Cords

Different power cords are offered as options with the module. The female

end of all power cords is identical. It plugs into the power- input socket at

the rear. The male end of each power cord is different and designed to

match the wall socket of a particular country or region.

CAUTION

Inaccessible power plug.

In case of emergency it must be possible to disconnect the instrument from the power

line at any time.

➔Make sure the power connector of the instrument can be easily reached and

unplugged.

➔Provide sufficient space behind the power socket of the instrument to unplug the

cable.

WARNING

Absence of ground connection or use of unspecified power cord

The absence of ground connection or the use of unspecified power cord can lead to

electric shock or short circuit.

➔Never operate your instrumentation from a power outlet that has no ground

connection.

➔Never use a power cord other than the Agilent Technologies power cord designed

for your region.

WARNING

Use of unsupplied cables

Using cables not supplied by Agilent Technologies can lead to damage of the

electronic components or personal injury.

➔Never use cables other than the ones supplied by Agilent Technologies to ensure

proper functionality and compliance with safety or EMC regulations.

10 1260 Infinity Micro Degasser Service Manual

2Site Requirements and Specifications

Site Requirements

Bench Space

The module dimensions and weight (see Table 1 on page 11) allow you to

place the module on almost any desk or laboratory bench. It needs an

additional 2.5 cm (1.0 inches) of space on either side and approximately

8 cm (3.1 inches) in the rear for air circulation and electric connections.

If the bench shall carry a complete HPLC system, make sure that the

bench is designed to bear the weight of all modules.

The module should be operated in a horizontal position.

Condensation

WARNING

Unintended use of supplied power cords

Using power cords for unintended purposes can lead to personal injury or damage of

electronic equipment.

➔Never use the power cords that Agilent Technologies supplies with this instrument

for any other equipment.

CAUTION

Condensation within the module

Condensation will damage the system electronics.

➔Do not store, ship or use your module under conditions where temperature

fluctuations could cause condensation within the module.

➔If your module was shipped in cold weather, leave it in its box and allow it to warm

slowly to room temperature to avoid condensation.

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